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2 About this Catalogue T his»analytical Supplies«catalogue provides an extensive list of consumables, accessories and spare parts that are essential for the smooth operation of GERSTEL systems for chromatographic analysis. You have the right to demand the highest quality performance from GERSTEL systems and we have compiled this list so that this performance can be maintained throughout the life of your system. Please use only consumables, accessories and spare parts provided by GERSTEL. All GERSTEL products are made to exact specifications. Use of products not approved by GERSTEL can cause system malfunction or damage and may void the system s warranty. If you have any questions please do not hesitate to contact us. The most efficient way is to reach us is through our web site at Your questions can be answered even more quickly by linking to your local sales office through our site. 2

3 Table of contents GRAPHPACK 2M connection technology...4 GRAPHPACK 2M adapters with Swagelok thread, male...6 GRAPHPACK 2M adapters with Swagelok thread, female...7 GRAPHPACK 2M detector adapters...8 GRAPHPACK 2M inlet adapters GRAPHPACK 2M dual column inlet adapter GRAPHPACK 2M MSD adapter GRAPHPACK 2M dual column interface for MSD GRAPHPACK 3D/2 connection technology GRAPHPACK 3D/2 column connector GRAPHPACK 3D/2 column connector with gas connection GRAPHPACK 3D/2 crosspieces GERSTEL Cooled Injection System, CIS...20 GERSTEL Automated Liner Exchange, ALEX...28 GERSTEL MultiPurpose Sampler, MPS GERSTEL MultiPurpose Sampler, MPS GERSTEL Twister Desorption Unit, TDU...48 GERSTEL Twister...52 GERSTEL Thermal Desorption System, TDS...56 GERSTEL Pyrolysis Module, PM GERSTEL Thermal Extractor, TE 1/ GERSTEL Tube Conditioner, TC GERSTEL Column Switching Systems, MCS...70 GERSTEL Preparative Fraction Collector, PFC...72 GERSTEL Olfactory Detector Port, ODP...76 GERSTEL ChemSensor System...78 GERSTEL Approved Supplies...80 Accessories by other leading analytical equipment suppliers...84 Index...85 Page 3

4 GRAPHPACK 2M connection technology For the rapid and economical connection of capillary columns to GC Inlets and Detectors. The components of the GRAPHPACK 2M connection technology are the GRAPHPACK 2M ferrule, the GRAPHPACK 2M adapter and the GRAPHPACK nut. GRAPHPACK 2M ferrule The GRAPHPACK 2M ferrule is a cylindrical metal cartridge packed with graphite. Advantages Rapid and reliable installation/ changing of capillary columns. Rapid mounting and positioning of the ferrules on the capillary column outside the oven. Leak-free connections are achieved without excessive tightening. Connections remain leak-free with temperature cycling. Self-centering of the ferrule on the GRAPHPACK 2M adapter. The capillary column is always centered in the inlet or detector. No damage to column coating. Economical, no more than two ferrules are required for the life of a column. GRAPHPACK 2M Adapter Available for all column outside diameters between 0.2 mm and 0.8 mm. GRAPHPACK nut A slotted nut for securing the column to all GRAPHPACK adapters. 4 GRAPHPACK 2M and GRAPHPACK 3D/2 ferrules are not interchangeable.

5 GRAPHPACK Column OD / ID GRAPHPACK 2M ferrules 1 package (10 units) 0.20 mm / 0.1 mm mm / 0.1 mm mm / 0.20 mm mm / 0.25 mm mm / 0.32 mm mm / 0.53 mm mm / 0.27 mm (for glass) GRAPHPACK 2M plug ferrule 1 package (5 units) 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm GRAPHPACK 2M mounting tool kit For mounting and positioning of GRAPHPACK 2M ferrules on capillary columns. Complete kit Spare parts GRAPHPACK mounting tool for GRAPHPACK 2M ferrules tool body, without insert Column OD Inserts 0.31 mm (red) to 0.45 mm (green) to 0.80 mm (black) GRAPHPACK nut for mounting tool 1 package (5 units) OD = Outside diameter ID = Inside diameter 5

6 GRAPHPACK 2M adapters with Swagelok thread, female For the conversion of GC systems with Swagelok fittings to GRAPHPACK 2M technology. Column OD / ID with 1/4 Swagelok female thread 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm with 1/8 Swagelok female thread 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm with 1/16 Swagelok female thread 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm GRAPHPACK 2M ferrules are not included with the GRAPHPACK detector adapters and must be ordered separately. When using 0.40 mm OD capillaries, use a 0.45 mm OD adapter in combination with a 0.40 mm ferrule.

7 GRAPHPACK GRAPHPACK 2M adapters with Swagelok thread, male For the conversion of GC systems with Swagelok fittings to GRAPHPACK 2M technology. Column OD / ID with 1/4 Swagelok male thread 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm with 1/8 Swagelok male thread 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm with 1/16 Swagelok male thread 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm

8 GRAPHPACK 2M detector adapters For the low-cost conversion of detector connections of various GC manufacturers to GRAPHPACK 2M connection technology. Advantages Economical, only one sealing technology is used for all detectors. No contact with the inside of the detector because of accurate centering. Column OD / ID Agilent Technologies / Hewlett-Packard HP 5890 A and Series II and Agilent 6850/6890 for FID, NPD 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Spare parts Silver seal; 1 package (5 units) Agilent Technologies / Hewlett-Packard HP 5890 A and Series II and Agilent 6850/6890 for TCD, FPD 0.45 mm / 0.32 mm mm / 0.53 mm Chrompack mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Dani Detectors; M mm / 0.20 mm mm / 0.32 mm Spare parts 0.70 mm / 0.53 mm Silver seal; 1 package (5 units) Fisons Series 8000, Trace, Tremetics, CE 5300, CE mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Spare parts Silver seal; 1 package (5 units) GRAPHPACK 2M ferrules are not included with the GRAPHPACK detector adapters and must be ordered separately.

9 GRAPHPACK Column OD / ID O.I. Analytical PID 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm O.I. Analytical PFPD and XSD Spare parts 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Silver seal; 1 package (5 units) Perkin Elmer Spare parts 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Vespel graphite ferrule; 1 package (5 units) Siemens RGC 0202 Spare parts 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Silver seal; 1 package (5 units) Shimadzu 14 A and 17 A Spare parts 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Silver seal; 1 package (5 units) Shimadzu 2010 Spare parts 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Silver seal; 1 package (10 units) Varian 3300 / 3400 / 3500 / 3600 / 3800 / 3900 & Saturn Spare parts 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Silver seal; 1 package (5 units) Spare parts for all GRAPHPACK adapters GRAPHPACK nut; 1 package (5 units)

10 GRAPHPACK 2M inlet adapters For the low-cost conversion of inlet connections of various GC manufacturers to GRAPHPACK 2M connection technology. Advantages Economical, only one sealing technology is used for all inlets. No contact with the inlet liner because of accurate centering. Column OD / ID Agilent Technologies / Hewlett-Packard Split/splitless injector HP 5890 A and Series II and Agilent 6850/ mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Spare parts Silver seal; 1 package (5 units) Agilent Technologies / Hewlett-Packard HP 5890 A and Series II and Agilent 6850/6890 for TCD mm / 0.32 mm mm / 0.53 mm Fisons Series 8000 Split/splitless injector 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Sold without silver seal and nut. Spare parts Silver seal mm OD; 1 package (5 units) Perkin Elmer PSS Injector 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Spare parts Vespel ferrule; 1 package (5 units) When using 0.40 mm OD capillaries, use a 0.45 mm OD adapter in combination with a 0.40 mm ferrule.

11 GRAPHPACK Column OD / ID Perkin Elmer Split/splitless injector 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Spare parts Vespel ferrule 1/4 ; 1 package (5 units) Shimadzu 14 A, 17 A Split/splitless injector 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Spare parts Silver seal; 1 package (5 units) Shimadzu 2010 Split/splitless injector 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Spare parts Silver seal; 1 package (5 units) Valco VICI Valve 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Varian 3300 / 3400 / 3500 / 3600 / 3800 / 3900 & Saturn 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Spare parts Silver seal; 1 package (5 units) Spare parts for all GRAPHPACK adapters GRAPHPACK nut; 1 package (5 units)

12 GRAPHPACK 2M dual column inlet adapter This dual column inlet adapter permits the simultaneous connection of two fused silica capillary columns to one inlet. This allows a sample to be analyzed on two columns simultaneously from a single injection. Adapters are available for GERSTEL inlets as well as for all major GC manufactures. Advantages Reduction in analysis time. Simultaneous analysis using capillary columns with different polarities. No split discrimination due to contact of the capillary column with the inside wall of the inlet liner thanks to column selfcentering design. Column OD / ID GERSTEL Cooled Injection System CIS 3 and CIS mm / 0.20 mm mm / 0.32 mm Spare parts Silver seal; 1 package (5 units)

13 GRAPHPACK Column OD / ID Agilent Technologies / Hewlett-Packard Split/splitless injector HP 5890 A and Series II and Agilent mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Spare parts Silver seal; 1 package (5 units) Fisons Series 8000 Split/splitless injector 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Spare parts Silver seal. 5 mm OD; 1 package (10 units) Silver seal mm OD; 1 package (5 units) Perkin Elmer Split/splitless injector 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Spare parts Vespel ferrule 1/4 ; 1 package (5 units) Carlo Erba CE mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Spare parts Silver seal; 1 package (5 units) Silver seal; 1 package (10 units) When using 0.40 mm OD capillary, use a 0.45 mm OD adapter in combination with a 0.40 mm ferrule. 13

14 GRAPHPACK 2M MSD adapter For the low-cost conversion of MSD connections of various GC manufacturers to GRAPHPACK 2M connection technology. Advantages Economical, only one sealing technology is used for the capillary column. Leak-free at elevated or fluctuating temperatures and under high vacuums. Column OD / ID Agilent Technologies / Hewlett-Packard MSD HP 5971 / 5972, Agilent 5973A / 5973N / 5973 inert, 5975, HP GCD 0.31 mm / 0.20 mm mm / 0.25 mm mm / 0.32 mm Spare parts Silver seal; 1 package (5 units)

15 GRAPHPACK GRAPHPACK 2M dual column interface for MSD For the simultaneous connection of two capillary columns to a single MSD Advantages Use of two different polarity capillary columns with one MSD. Column OD / ID. Hewlett-Packard MSD HP 5971/ mm / 0.20 mm mm / 0.25 mm mm / 0.32 mm Spare parts Vespel ferrule; 1 package (5 units) Interface nut; 1 package (5 units) Agilent Technologies / Hewlett-Packard MSD Agilent/HP 5973A, 5973N, 5973 inert, mm / 0.20 mm mm / 0.25 mm Spare parts Vespel ferrule; 1 package (5 units) Inferface nut; 1 package (5 units)

16 GRAPHPACK 3D/2 connection technology For the rapid, reliable and low-dead-volume connection of two capillary columns with the same or different outside diameter, or of different materials. The components of the GRAPHPACK 3D/2 connection technology are the GRAPHPACK 3D/2 ferrule, the GRAPHPACK 3D/2 connector and the GRAPHPACK 3D/2 screw. Sulfinert All GRAPHPACK 3D/2 components which come into contact with analytes are Sulfinert coated. This offers the optimal surface material for every GC analysis. Sulfinert is the latest in passivation coating technology, the next generation of the well-known Silcosteel coating. The Sulfinert coating is ideal for use in all GC applications such as environmental, flavour and fragrance, off-odors, food and beverage, chemical and petrochemical, pharmaceutical and polymers. Sulfinert is stable over a wide ph range and unlike fused silica coatings, which can dissolve in caustic environments; the Sulfinert coating is stable when sampling caustic amines as well as acidic sulfur compounds. Sulfinert provides for the determination of ultra-low levels of organic compounds and superior inertness for sulfur compounds, simplifying the choice of passivation surface. When working with GERSTEL GRAPHPACK 3D/2 products, there is no need to use different passivation surfaces for different applications or different analytes. GERSTEL GRAPHPACK 3D/2 is offered with only one type of surface passivation: The very best. 1 1 GRAPHPACK 3D/2 ferrule 3 GRAPHPACK 3D/2 screw 2 The GRAPHPACK 3D/2 ferrule is a cylinder metal packed with graphite. Advantages Suitable for high pressures and temperatures as well as high vacuum. Rapid mounting and positioning on the column outside the oven. Leak-free connections are achieved without excessive tightening. Connections remain leak-free with temperature cycling. Self-centering of the ferrule in the connector. 4 The screw secures the capillary column and the GRAPHPACK 3D/2 ferrule in the connector. GRAPHPACK 3D/2 sealing ferrule This is a GRAPHPACK 3D/2 ferrule with a fixed sealing wire for the low dead-volume sealing of an outlet which is not needed on GRAPHPACK 3D/2 crosspieces and switching in use GRAPHPACK 3D/2 connectors Column connectors, crosspieces and switching devices for the connection of two to four capillary columns of the same or different diameters. Advantages No dead volume occurs as the result of an outlet which is not needed. No graphite enters the GRAPHPACK 3D/2 crosspiece or switching device as an appropriate sealing ferrule is available for every column diameter. Advantages Low thermal mass. Low dead-volume. 16 GRAPHPACK 2M and GRAPHPACK 3D/2 ferrules are not interchangeable.

17 GRAPHPACK Column OD / ID GRAPHPACK 3D/2 ferrules 1 package (10 units) 0.20 mm / 0.1 mm mm / 0.1 mm mm / 0.20 mm mm / 0.25 mm mm / 0.32 mm mm / 0.53 mm mm / 0.27 mm (glass capillary) GRAPHPACK 3D/2 screw 1 package (1 units) 0.20 mm / 0.1 mm mm / 0.1 mm mm / 0.20 mm mm / 0.25 mm mm / 0.32 mm mm / 0.53 mm mm / 0.27 mm (glass capillary) GRAPHPACK 3D/2 sealing ferrule for GRAPHPACK 3D/2 crosspieces 1 package (5 units) 0.20 mm / 0.1 mm mm / 0.1 mm mm / 0.20 mm mm / 0.25 mm mm / 0.32 mm mm / 0.53 mm mm / 0.27 mm (glass capillary) 17

18 GRAPHPACK 3D/2 column connector Sulfinert For the connection of two capillary columns with the same or different diameters or of different materials. Column OD / ID Column OD / ID from 0.70 / 0.53 mm to 0.31 mm / 0.20 mm mm / 0.25 mm mm / 0.32 mm mm / 0.53 mm from 0.45 / 0.32 mm to 0.31 mm / 0.20 mm mm / 0.25 mm mm / 0.32 mm from 0.40 / 0.25 mm to 0.40 mm / 0.25 mm from 0.31 / 0.20 mm to 0.31 mm / 0.20 mm GRAPHPACK 3D/2 column connector Sulfinert with gas connection GRAPHPACK 3D/2 column connector with gas connection For the connection of two capillary columns with the same or different diameters or of different materials and the connection of make-up gas. Column OD / ID Column OD / ID Spare parts see page 17 from 0.80 to 0.45 mm / 0.32 mm from 0.70 / 0.53 mm to 0.31 mm / 0.20 mm mm / 0.25 mm mm / 0.32 mm mm / 0.53 mm from 0.45 / 0.32 mm to from 0.40 / 0.25 mm to 0.31 mm / 0.20 mm mm / 0.25 mm mm / 0.32 mm mm / 0.25 mm from 0.31 / 0.20 mm to 0.31 mm / 0.20 mm GRAPHPACK 3D/2 column connectors with or without one gas connection include two GRAPHPACK 3D/2 ferrules.

19 GRAPHPACK GRAPHPACK 3D/2 crosspieces Sulfinert For the connection up to 4 capillary columns with the same or different diameters or of different materials. main column outside diameter GRAPHPACK 3D/2 crosspiece kit contains GRAPHPACK 3D/2 crosspiece GRAPHPACK 3D/2 ferrules Universal bracket for crosspiece GRAPHPACK mounting tool kit 0.31 mm mm mm Spare parts GRAPHPACK 3D/2 crosspiece 0.31 mm mm mm mm Universal bracket for crosspiece GRAPHPACK mounting tool kit for GRAPHPACK 3D/2 column connectors + crosspieces Complete kit Spare parts 2 GRAPHPACK mounting tool tool body without insert Insert for 1.2 mm column mounting depth Color red Insert holder main column outside diameter 0.20 mm to 0.31 mm mm to 0.45 mm mm to 0.80 mm

20 GERSTEL Cooled Injection System, CIS Universal inlet for gas chromatography The GERSTEL CIS is a temperature programmable GC inlet. The CIS offers septumless, cold injection of volumes of up to 1000 µl for liquid samples. The integrated split function enables the CIS to handle ultra-trace concentrations as well as undiluted samples. Programmed linear heating ensures quantitative, discrimination-free transfer of sample components to the GC column for best possible GC analysis results. The CIS is a general purpose, universal GC inlet. When working with Thermal Desorption or Headspace techniques, the CIS is used for enrichment, focusing and quantitative transfer of analytes to the capillary column. An integral part of the CIS is the GERSTEL MAS controller, which can be used to control all GERSTEL modules, thus ensuring easy, cost effective system upgrades. The CIS can be retrofitted to existing Agilent Technologies/HP gas chromatographs. GERSTEL GRAPHPACK technology and septumless sampling head are standard features. A choice of liquid CO2, liquid N2 or Peltier cooling is available. Available CIS models cover the temperature range from 150 to +600 C. Compounds covering a wide boiling range can be efficiently trapped with subsequent discrimation-free analyte transfer to the capillary column. The CIS is compatible with all GERSTEL autosamplers - and with autosamplers from all major manufacturers. 20

21 GERSTEL Cooled Injection System, CIS Septumless sampling head (SLH) for CIS 3 / 4 / 6 (for 23 gauge needles) For manual or auto-injection CIS CIS 4 / CIS Service kit for SLH Complete Contains one unit each of the following items: 1 Plunger Spring Inner-O-Ring (Kalrez ) Outer-O-Ring (Viton ) * * When reordering only complete original package size is available (5 units). 4 SLH cap 23 gauge needles Teflon needle guide for SLH 1 package (10 units) 23 gauge needles Carrier gas connection for SLH 1 4 Complete kit Aluminium seal for SLH 1 package (5 units) Screw 1 package (1 units) Teflon ferrule 1/16 1 package (10 units) Knurled nut 1 package (5 units)

22 Column OD / ID GRAPHPACK 2M adapter for CIS CIS 3 / CIS 4 (silver) 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Spare parts CIS 6 (Stainless steel) 0.31 mm / 0.20 mm mm / 0.32 mm mm / 0.53 mm Silver seal; 1 package (5 units) GRAPHPACK nut; 1 package (5 units) Septum head without septum purge CIS CIS 4 / CIS Septum head with septum purge CIS CIS 4 / CIS Spare parts 2 1 Septum cap Septum for CIS 3/4, white; 1 package (25 units) Teflon ferrule 1/16 ; 1 package (10 units) Knurled nut; 1 package (5 units) Adsorption trap for split outlet 1/16 inlet, 1/16 outlet connection, filled with charcoal

23 GERSTEL Cooled Injection System, CIS Column OD / ID GRAPHPACK 2M dual column injector adapter For the simultaneous connection of two analytical capillary columns to a single CIS inlet mm / 0.20 mm mm / 0.32 mm Spare parts Silver seal; 1 package (5 units) GRAPHPACK nut; 1 package (5 units) On Column kit 1 On Column insert; single CIS CIS 4 / CIS GRAPHPACK 3D ferrule; CIS package (5 units) CIS 4 / CIS GRAPHPACK 2M adapter CIS 3 / CIS CIS GRAPHPACK 2M ferrule; 1 package (10 units) Silver seal; 1 package (5 units) Teflon needle guide (0.47 mm); 1 package (10 units) Cap (0.47 mm)

24 Glass liners for CIS packed * deactivated description / typical use units CIS 3 CIS 4 / CIS 6 ** straight with notch Initial system checkout; user custom-packed liners; hot split/splitless injections baffled General use liquid injection for moderate/high boilers, labile compounds, split injections for SPME ID 1mm for injection with MPS 2 with SPME Option with liquid injection for moderate/high boilers, silanized stable compounds; thermal desorption glass wool cryotrapping of stable compounds with More inert than glass wool; used for trapping quartz wool labile compounds with glass Provides additional surface area compared beads to empty liner with glass beads Trapping volatiles with a wide range of and Carbotrap C boiling points with Tenax TA Trapping of C 5 and higher volatiles ( 50 C minimum temperature) with Carbotrap B Trapping of low boiling volatiles straight with notch Initial system checkout; user custom-packed liners; hot split/splitless injections baffled General use liquid injection for moderate/high boilers, labile compounds, split injections ID 2 mm for special applications with General use liquid injection for moderate/ silanized high boilers, stable compounds; thermal glass wool desorption cryotrapping of stable compounds Quartz liners packed * deactivated description / typical use units CIS 4 / CIS 6 straight with notch For hot split/splitless injection to 650 C baffled General se liquid injection for moderate/ high boilers, labile compounds, split injections to 650 C with Used for trapping labile compounds quartz wool * ** All packed liners use the straight with notch liner. These glass liners are to be used to 450 C only when working with a CIS 6. For higher temperatures than 450 C only quartz liners are allowed!

25 GERSTEL Cooled Injection System, CIS Glass liner kits consisting of: units CIS 3 CIS 4 / CIS 6 ** straight with notch, deactivated baffled, deactivated 2 packed with silanized glass wool, deactivated 2 packed with Tenax 2 packed with Carbopack B 2 GRAPHPACK 3D ferrules for glass liners 1 package (5/10 units) units CIS 3 CIS 4 / CIS 6 ** Kalrez ferrule (not in conjunction with TDS / TDU) units CIS 3 CIS 4 / CIS 6 ** GRAPHPACK 3D mounting tool for glass liners CIS CIS 4 / CIS Cryo tube 2 m CIS 4 / CIS 6 with CIS adapter CIS 4 / CIS 6 1/4 Swagelok

26 Microliter syringes injection type system description µl units manual injection CIS fixed needle manual injection CIS gastight Spare TLL needle

27 GERSTEL Cooled Injection System, CIS Microliter syringes injection / sampler system description µl units manual injection CIS needle-in-needle Autosampler CIS fixed needle HP 7673 / Agilent Autosampler CIS replaceable needle HP 7673 / Agilent Spare needle Autosampler CIS fixed needle, HP 7673 / on-column-injection Agilent

28 GERSTEL Automated Liner EXchange, ALEX For routine GC analysis of samples, that contain large amounts of solid material. Designed for use with the GERSTEL MultiPurpose Sampler, MPS 2 and the GERSTEL Cooled Injection System, CIS. GC inlet liners can be replaced automatically at user-defined intervals in the sequence. A special ALEX liner tray holds up to 98 prepared liners, enabling routine analysis of large numbers of dirty samples. Universal syringe holder Version 2; compatible with ALEX ALEX transportion adapter for CIS 4 Liner 1 units units O ring kit for ALEX transport adapter 1 package (5 4 units)

29 GERSTEL Automated Liner EXchange, ALEX Septa Ice blue, for liquid injection, 5 mm, 1 package (100 units) Allen wrench for transport adapter screws, 4 mm O ring for ALEX sampling head, 1 package (10 units) Glass inserts for ALEX sample tray 10 units units O ring for ALEX sample tray glass inserts 10 units units

30 GERSTEL MultiPurpose Sampler, MPS 2 The GERSTEL MultiPurpose Sampler, MPS 2 is a highly flexible and productive autosampler and sample preparation robot for GC and GC/MS analysis. The MPS 2 can automate everything from sample preparation to sample introduction. The MPS 2 is easily adapted to both new and existing instruments. The system is installed on top of the GC, saving valuable bench space, and is compatible with all standard laboratory GC systems. GERSTEL MASter Software enables integrated control of the MPS 2 and a GC or GC-MS system from one method and one integrated sequence list through the Agilent Technologies ChemStation Software. The GERSTEL MPS PrepStation is a dual-rail/dual robot configuration of the MPS 2 MultiPurpose Sampler. The PrepStation performs fully automated sample preparation and sample introduction. One MPS rail of the MPS PrepStation is an automated liquid sample handler that performs a wide range of sample preparation functions. The second MPS rail enables many automated sample introduction options, including Headspace and SPME depending upon the selected MPS 2 hardware configuration. The GERSTEL PrepBuilder Software enables overlapping sample preparation and GC analysis. While GC separation is in progress, the next sample is being prepared for analysis ensuring maximum productivity. Automated sample preparation steps include: Dilution Derivatization Heating Rinsing Liquid-liquid extraction Standard addition Spiking Agitation Automated sample introduction using a wide range of selectable techniques: Standard liquid injection Large-volume liquid injection Headspace SPME Twister Option Twister back-extraction Membrane assisted solvent extraction Other techniques can be automated using the MPS 2 with special adaptations. MPS 2 30

31 GERSTEL MultiPurpose Sampler, MPS Sample vials and caps for use with the MPS 2, MPS 2L, MPS 2XL and MPS PrepStation 1 Crimp cap vials Sampler Type Vials ml units MPS 2 Clear, colorless glass * Crimp caps with septum for vials If vials need to be reopened and emptied after analysis, magnetic vial caps with aluminum edges (Bi-metal) offer the best solution. The softer edges allow easy crimping and decrimping using a hand-crimper. If steel caps are used, it is recommended to use a bench-top crimper. 3 Sampler Type Caps Vial volume (ml) units MPS 2 Aluminium with septum PTFE red / Silicone / PTFE red, for 8 mm vial * Magnetic, golden with septum PTFE red / Silicone / PTFE red, for 11 mm vial Magnetic, golden, Silicone blue transparent, 10/ PTFE white, 3 mm, for 20 mm vial 10/ Bi-metall, magnetic, red, with septum Silicone blue transparent, PTFE white, 3 mm, for 20 mm vial 10/ Magnetic, with Pharma Fix septum Silicone/PTFE 10/ Delivery times upon request * 31

32 Vials for SPME Special vial with thickened crimp neck for use with 20 mm cap 100 units for SPME and 0.5 mm septa, with imprint»spme«crimp caps for SPME magnetic, golden, with septum For SPME applications, crimp caps of steel with silicone septa are recommended. If the sample is analyzed for silicone, it is recommended to use butyl rubber septa or natural rubber septa. For a leakfree seal, it is recommended to use a bench-top crimper. Sampler Crimp cap with septum: Vial volume (ml) units MPS 2 Silicone creme, PTFE red, 1.5 mm, 55 Shore A, for 20 mm SPME vial Viton, 0.5 mm, 75 Shore A, for 20 mm SPME vial Natural rubber, red-orange / Teflon, 1.3 mm, 55 Shore A, for 20 mm SPME vial Butyl red / PTFE grey, 1.3 mm, 55 Shore A, for 20 mm SPME vial Screw neck vials Sampler Vials Vial volume (ml) units MPS 2 clear, incl. caps and septa, 11 mm clear, for 18 mm screw caps brown, for 18 mm screw caps; without caps and septa clear, for 18 mm screw caps; without caps and septa brown, for 18 mm screw caps; without caps and septa Microliter inserts, clear, for 2 ml screw cap vials Screw caps with septa magnetic, for 18 mm screw cap vials Caps with silicone septa, blue, transparent are recommended as standard. If the sample is analyzed for silicone, it is recommended to use screw-caps with butyl rubber septa or viton septa. Sampler Screw caps with septum Vial volume (ml) units MPS 2 Silicone blue transparent / PTFE white, 1.3 mm, 35 Shore A 10/ Silicone white / PTFE blue, 1.5 mm, 60 Shore A 10/ Viton black, 1.0 mm, 75 Shore A 10/ Butyl red / PTFE grey, 1.6 mm, 55 Shore A 10/

33 GERSTEL MultiPurpose Sampler, MPS Septa for screw caps for 10/20 ml screw cap vials Sampler Septum type units MPS 2 Silicone blue transparent / PTFE white, 1.3 mm, 35 Shore A Silicone white / PTFE blue, 1.5 mm, 60 Shore A Viton black, 1.0 mm, 75 Shore A Butyl red / PTFE grey, 1.6 mm, 55 Shore A Screw cap vials for Twister Back Extraction Sampler Vials Vial volume (ml) units MPS 2 for 10 mm Twisters: screw cap vial 32 x 11.6 mm, clear, for 11 mm screw cap for 10 mm Twisters: insert 31 x 6 mm, clear for 20 mm Twisters: screw cap vial 32 x 11.6 mm, clear, for 11 mm screw cap Screw caps, blue, with septa, 9 mm. With embedded magnetic discs. septum: silicone, white / PTFE, red, 1.0 mm, 55 Shore A. 1 package (100 units) Inserts 2 ml, for Agitator 1 package (6 units) For automated Twister Back Extraction analysis, 2 ml vials are transferred to the agitator. This requires special adaptors inside the agitator * Delivery times upon request * 33

34 Replacement kit for Standard wash station MPS 2 or MPS 2L consisting of: 10 ml 10CV vials (10 units) wash cap Polypropylene Snap Cap (10 units) 20-ST101 Silicone/PTFE Septa (10 units) * Solvent bottle 100 ml includes cap and septum Caps and septa for 100 ml solvent bottle, 1 package (10 units) Crimper for 8 mm crimp caps (0.7 ml vials) * for 11 mm crimp caps (2 ml vials) for 20 mm crimp caps (10/20 ml vials) Decapper for 8 mm crimp caps (0.7 ml vials) * for 11 mm crimp caps (2 ml vials) for 20 mm crimp caps (10/20 ml vials) Delivery times upon request *

35 GERSTEL MultiPurpose Sampler, MPS Bench-top crimper For easy crimping and de-crimping of vials, especially when steel caps are used or when large numbers of samples are analyzed. 1 1 for crimp caps 20 mm Spare parts / Option 2 Crimper head Decapper head Vial guide for crimp caps 8 mm (0.7 ml vials) * 11 mm (2 ml vials) * 13 mm (4 ml vials) * 20 mm (10/20 ml vials) * 8 mm (0.7 ml vials) * 11 mm (2 ml vials) * 13 mm (4 ml vials) * 8 mm (0.7 ml vials) * 11 mm (2 ml vials) * 13 mm (4 ml vials) * 20 mm (10/20 ml vials) * 2 Microliter syringe For MPS 2, MPS 2L and MPS PrepStation, for use with CTC syringe adapter The listed syringes all have 23 Gauge needles (OD = 0.63 mm) and are compatible with the GERSTEL Septumless Head (SLH). Needles have conical tips (type C or AS). 1 OD x L (mm) volume (µl) gastight needle needle dimension units 5 fixed 0.63 x fixed 0.63 x fixed 0.63 x replaceable 0.63 x replaceable 0.63 x Spare needles for 100/250 µl syringe Delivery times upon request * 35

36 Microliter syringes For MPS 2, MPS 2L and MPS PrepStation, for use with the GERSTEL Universal liquid syringe adapter The listed syringes all have 23 Gauge needles (OD = 0.63 mm) and are compatible with the GERSTEL Septumless Head (SLH). Needles have conical tips (type C or AS). needle dimensions volume (µl) gastight needle OD x L (mm) units 1.2 needle-in-needle 0.47 x fixed 0.63 x fixed 0.63 x fixed 0.63 x fixed 0.47 x replaceable 0.63 x replaceable 0.63 x replaceable 0.63 x replaceable 0.63 x replaceable 0.63 x Replacement syringe plungers (gastight) 10 µl syringe with fixed needle µl syringe with replaceable needle µl syringe with replaceable needle µl syringe with replaceable needle µl syringe with replaceable needle Replacement needles 5 µl syringe with replaceable needle µl syringe with replaceable needle /250 µl syringe with replaceable needle µl syringe with replaceable needle On column needle 10 µl syringe with replaceable needle

37 GERSTEL MultiPurpose Sampler, MPS Microliter syringe for MPS 2, MPS 2L, MPS 2XL and MPS PrepStation For use with GERSTEL Universal Headspace Syringe Adapter in combination with heated adapter for liquid injection. The listed syringes all have 23 Gauge needles (OD = 0.63 mm) and are compatible with the GERSTEL Septumless Head (SLH). Needles have conical tips (type C or AS). needle dimensions volume (µl) gastight needle OD x L (mm) units 10 replaceable 0.63 x fixed 0.63 x Replacement needle for 10 µl syringe with needle For use with the GERSTEL Universal Headspace Syringe Adapter The listed syringes all have 23 Gauge needles (OD = 0.63 mm) and are compatible with the GERSTEL Septumless Head (SLH). Needles have conical tips (type H or 5). OD x L (mm) volume [ml] gastight needle needledimension units 1 replaceable 0.63 x replaceable 0.63 x Replacement syringe plungers (gastight) 1 ml headspace syringe ml headspace syringe Replacement needle 1-/2.5 ml headspace syringe

38 Dilutor module for MPS 2, MPS 2 XL and MPS PrepStation MPS 2 Dilutor syringe For use with the MPS Dilutor module volume units MPS Dilutor syringe 1 ml ml ml ml Replacement plunger for MPS Dilutor syringe 1 ml ml ml ml PTFE seal for MPS Dilutor syringe * Solvent bottle for MPS Dilutor; 1000 ml * * * * * MPS 2 Sideport syringe without needle For use with MPS sideport syringe adapter (not compatible with GERSTEL Universal Syringe Adapter) volume units MPS Sideport syringe without needle 20 µl µl Replacement plunger for Sideport syringe 20 µl * 80 µl * Needles Needles for use with MPS 2, MPS 2L, MPS XL and MPS PrepStation. For use with GC injectors. 23s gauge (OD = 0.63 mm) needle for 20 µl syringe gauge (OD = 0.47 mm) needle for 20 µl syringe gauge (OD = 0.63 mm) needle for 80 µl syringe gauge (OD = 0.47 mm) needle for 80 µl syringe gauge needles are compatible with on-column injection. 38 Delivery times upon request *

39 GERSTEL MultiPurpose Sampler, MPS SPME fiber holder Designed for mounting SPME fibers for automated SPME analysis Fibers used for automated SPME analysis have no spring in contrast to fibers for manual SPME. Consequently, there are separate holders for each fiber type. The fibers listed here are designed exclusively for automated SPME analysis using the MPS 2. They are not suitable for manual SPME analysis. For use with the GERSTEL Cooled Injection System, CIS 23 gauge (OD=0.63 mm) fibers and SPME liner are recommended. SPME fiber kits volatiles 100 µm polydimethylsiloxane, non-bonded non-polar semivolatiles 30 µm polydimethylsiloxane, non-bonded 23 gauge (OD=0.63 mm) 1 package (3 units) gauge (OD=0.63 mm) 1 package (3 units) non-polar high molecular weight compounds 7 µm polydimethylsiloxane, bonded 23 gauge (OD=0.63 mm) 1 package (3 units) volatiles, amines, and nitroaromatic compounds 65 µm polydimethylsiloxane/divinylbenzene, partially crosslinked 23 gauge (OD=0.63 mm) 1 package (3 units) volatiles, amines, and nitroaromatic compounds 65 µm polydimethylsiloxane/divinylbenzene, highly crosslinked on StableFlex fiber 23 gauge (OD=0.63 mm) 1 package (3 units) semivolatiles 85 µm polyacrylate, partially crosslinked 23 gauge (OD=0.63 mm) 1 package (3 units)

40 SPME fiber kits gases and low molecular compounds 75 µm carboxen/polydimethylsiloxane, partially crosslinked gases and low molecular compounds 85 µm carboxen/polydimethylsiloxane, highly crosslinked on StableFlexTM fiber alcohols and polar compounds 65 µm carbowax/divinylbenzene, partially crosslinked alcohols and polar compounds 70 µm carbowax/divinylbenzene, highly crosslinked on StableFlexTM fiber 23 gauge (OD=0.63 mm) 1 package (3 units) gauge (OD=0.63 mm) 1 package (3 units) gauge (OD=0.63 mm) 1 package (3 units) gauge (OD=0.63 mm) 1 package (3 units) volatiles and semivolatiles 85 µm polyacrylate, 100 µm polydimethylsiloxane, 7 µm polydimethylsiloxane coating 23 gauge (OD=0.63 mm) 1 package (3 units) flavors 50/30 µm divinylbenzene/carboxen/ polydimethylsiloxane on StableFlex fiber 23 gauge (OD=0.63 mm) 1 package (3 units) flavors 50/30 µm divinylbenzene/carboxen/ polydimethylsiloxane on 2 cm StableFlex fiber 23 gauge (OD=0.63 mm) 1 package (3 units) volatile or polar organics in water 75 µm carboxen/polydimethylsiloxane, 65 µm polydimethylsiloxane/divinylbenzene, 65 µm carbowax/divinylbenzene flavors and odors 100 µm polydimethylsiloxane, 65 µm polydimethylsiloxane/divinylbenzene, 65 µm carboxen/polydimethylsiloxane 23 gauge (OD=0.63 mm) 1 package (3 units) gauge (OD=0.63 mm) 1 package (3 units)

41 GERSTEL MultiPurpose Sampler, MPS SPME Stableflex fiber kit 23 gauge (OD = 0.63 mm), 4 fibers 50/30 Divinylbenzene/Carboxen 65 µm Polydimethylsiloxane/Divinylbenzene 85 µm Carboxen/Polydimethylsiloxane 70 µm Carbowax/Divinylbenze Sample trays for 200 vials 0.7/1 ml (VT 200) * for 98 vials 2 ml ( VT 98) * for 32 vials 10/20 ml ( VT 32) * for 54 vials 2 ml for stack (VT 54) * for 54 vials 2 ml for stack, 6 units (VT 54) * Adapter plate to use a microtiter or deepwell plate in cooled trays * Plastic tray cover for 1 ml vials in Tray * for 2 ml vials in Tray * for deepwell or microtiter plates in cooled trays * Inserts for 2 ml vials for agitator 1 package (6 units) For use with 2 ml vials in combination with the MPS 2 agitator e.g. for Twister Back Extraction * Delivery times upon request * 41

42 GERSTEL MultiPurpose Sampler, MPS 3 MPS 3/3C/3LC are programmable XYZ autosamplers and sample preparation robots for liquid chromatography and LC/MS. The MPS can automate everything from sample preparation to sample introduction. The MPS 3 and MPS 3C are specially designed for High Throughput Screening, HTS. The MPS 3LC is a HPLC autosampler with fixed configuration. These systems set the standard for speed, reliability, accuracy and throughput. GERSTEL MASter Software enables integrated control of the MPS 3 and a LC or LC/MS system. One method and one integrated sequence controls the complete system through the Agilent Technologies ChemStation Software. GERSTEL MASter software is fully integrated into the ChemStation software: All sample parameters are saved as part of ChemStation methods. A single sequence table ties together all sample information, autosampler functions, and data file functions. The GERSTEL PrepBuilder Software enables overlapping sample preparation and GC analysis. While LC separation is in progress, the next sample is being prepared for analysis, ensuring maximum productivity. Automated sample preparation steps include: Standard addition Derivatization Dilution Liquid-liquid extraction Twister Back Extraction Membrane Assisted Solvent Extraction Heating Rinsing Agitation MPS 3LC MPS 3 42

43 GERSTEL MultiPurpose Sampler, MPS 3 Vials and caps for use with MPS 3, MPS 3C and MPS 3LC sampler description volume units MPS 3 Crimp cap vials Crimp cap vial, clear, for 8 mm caps 0.7 ml Crimp cap vial, clear, for 11 mm caps 2 ml * Crimp caps Crimp cap, Aluminium with septum, PTFE red / Silicone / PTFE red, for 8 mm vials 0.7 ml Crimp cap, magnetic, golden with septum, PTFE red / Silicone / PTFE red, for 11 mm vials 2 ml Screw cap vials incl. caps and septa Screw cap vial, clear, incl. 11 mm cap with septum 2 ml Microliter inserts for 2 ml Screw cap vials Inert, clear 100 µl Screw cap vials for Twister Back Extraction for use with 10 mm Twisters Screw cap vial 32 x 11.6 mm, clear, for 11 mm screw cap 1.5 ml Insert 31 x 6 mm, clear, flat bottom 0.2 ml for use with 20 mm Twisters Screw cap vial 32 x 11.6 mm, clear, for 11 mm screw cap 1.1 ml Screw cap 9 mm with magnetic disks, blue, with septum, Silicone white / PTFE red, 1.0 mm, 55 shore A Solvent bottle 100 ml incl. cap and septum * Caps and septa for 100 ml solvent bottle package (10 units) Wash solvent bottle for fast wash station 500 ml * 1000 ml Delivery times upon request * 43

44 Crimper for 8 mm crimp vials (0.7 ml vials) * for 11 mm crimp vials (2 ml vials) Decapper for 8 mm crimp vials (0.7 ml vials) for 11 mm crimp vials (2 ml vials) * Syringe kits with syringe detect, consisting of: plunger holder, syringe adapter and 2 syringes 10 µl µl µl µl µl µl µl * * * * * * * Replacement syringe plunger units 10 µl, gastight µl µl µl µl µl µl µl * * * * * * * * 44 Delivery times upon request *

45 GERSTEL MultiPurpose Sampler, MPS 3 Microliter syringes for MPS 3, MPS 3C and MPS 3LC The needle types 22 and 22S both have the same outer diameter: 0.72 mm OD and a straight needle tip (Type LC or 3). Type 22 and 22S differ only by their internal diameter ( 0.41 mm and 0.15 mm ID respectively); Due to the larger ID, a type 22 needle enables faster syringe filling: Up to 200 µl/sec for type 22 as opposed to µl/sec for the 22S. volume (µl) gastight needle gauge point style units 10 fixed 22S fixed 22S fixed 22S fixed 22S fixed fixed fixed fixed fixed fixed The long-life Microliter syringes are much more durable than standard syringes. This is particularly useful for high-pressure work or when a large number of washcycles are used per sample. Long-life syringe kits Each kit contains a syringe holder, a syringe adapter with syringe type detection and two syringes. volume (µl) gastight needle gauge point style 25 fixed 22S fixed 22S Special long life microliter syringes volume (µl) gastight needle gauge point style units 25 fixed 22S fixed 22S X-type microliter syringes for LC For use with original CTC syringe adapters. X-type syringes provide extremely low carry-over as well as very long life-expectancy. volume (µl) gastight needle gauge point style units 25 fixed 22S fixed 22S fixed

46 Dilutor module for MPS 3, MPS 3C and MPS 3LC MPS Dilutor syringe for MPS 3, MPS 3C and MPS 3LC volume units MPS dilutor syringe 1 ml ml ml ml Replacement syringe plunger 1 ml * for MPS 2.5 ml * dilutor syringe 5 ml * 10 ml * PTFE ferrule for MPS dilutor syringe * Dilutor solvent bottle 1000 ml * MPS sideport syringe without needle For use with MPS sideport-syringe adapter (not compatible with GERSTEL Universal Syringe Adapter) volume units MPS sideport syringe 20 µl µl Replacement plunger for sideport syringes 20 µl µl Replacement needles for MPS sideport syringes for use with MPS 3 and MPS 3C, for use with LC injection valves 22 gauge (OD = 0.72mm) needle for 20 µl syringe gauge (OD = 0.72 mm) needle for 80 µl syringe * * 46 Delivery times upon request *

47 GERSTEL MultiPurpose Sampler, MPS 3 Sample loops for VICI HPLC-valve 1/16 ; includes nuts and ferrules µl µl * 50 µl * 100 µl * 500 µl * 1000 µl * 1 for VICI HPLC-valve, Typ DC6WK and DC10WK; includes nuts and ferrules 200 µl * 250 µl * MPS 3 2 µl µl µl µl µl µl for Cheminert Injection-valve 20 µl µl µl µl µl Sample trays for 200 x 0.7/1 ml vials (VT 200) * for 98 x 2 ml vials (VT 98) * for 32 x 10/20 ml vials (VT 32) * for 54 x 2 ml vials for stack (VT 54) * for 54 x 2 ml vials for stack, pack with 6 units (VT 54) * Adapter plate to use a microtiter- or a deepwell plate in cooled trays Plastic tray cover for 1 ml vials tray * for 2 ml vials tray * for deepwell or microtiter plates in cooled trays * Delivery times upon request * 47

48 GERSTEL Twister Desorption Unit, TDU The GERSTEL Twister Desorption Unit is a thermal desorption accessory designed for use with the GERSTEL Twister. The TDU is based on the same technology as the proven GERSTEL Thermal Desorption System, TDS, but is optimized for desorption of Twisters stir bars. In combination with the GERSTEL MultiPurpose Sampler, MPS 2, automated analysis of up to 196 Twisters can be performed in a single sequence. Recommended Kit consists of: Glass inserts kit O ring kit for transportation adapters (100 units) Twister transportation adapters (10 units) GRAPHPACK-3D ferrules (10 units) Twisters, film thickness 0.5 mm, length 10 mm (10 units) GERSTEL-Twister desorption Liner (100 units) system TDU / CIS TDU / CIS

49 GERSTEL Twister Desorption Unit, TDU Transportation adapter for GERSTEL Twister desorption liner 1 package (10 units) package (100 units) Transportation adapter for liquid injection 1 package (10 units) O-ring set for transportation adapter 1 package (10 Sets) package (100 Sets) Twister desorption liner 1 package (100 units) Glass inserts for Twister sample tray 1 package (100 units) O-ring for glass inserts for Twister sample tray 1 package (10 units) package (100 units)

50 Glass liners for CIS 3/4 in combination with TDU packing deactivated description/use units CIS 3/3 S CIS 4 silanized 1 mm ID, straight glass wool standard glass liner empty straight with notch Initial system checkout; user custom-packed liners; hot split/splitless injections empty baffled General use liquid injection for moderate/high boilers, labile compounds, split injections empty 2 mm ID For special applications silanized General use liquid injection for glass wool moderate/high boilers, stable compounds; glass wool thermal desorption cryotrapping of stable compounds quartz wool More inert than glass wool; used for trapping labile compounds Tenax TA Elimination of water (40 C most effective); Trapping of C 5 and higher volatiles (-50 C minimum temperature) Carbotrap B Trapping of low boiling volatiles Glass liner kit CIS/TDU included glass liners units (each) units (each) CIS 3 CIS 4 CIS 3 CIS 4 empty (baffled) packed with silanized glass wool 4 2 packed with Tenax TA 2 2 packed with Carbopack B mm ID, packed with silanized glass wool 2 Note The CIS glass liners listed in the above tables are designed for use only in combination with a TDU. For all other analyses using a CIS use only the inlet liners listed on page

51 GERSTEL Twister Desorption Unit, TDU GRAPHPACK 3D ferrules for glass liners 1 package (5/10 units) units CIS 3 CIS 4/CIS 6 * Mica coated for improved sealing units CIS 3 CIS 4/CIS 6 * GRAPHPACK 3D mounting tool for glass liners Note The GRAPHPACK 3D mounting tool is designed for use only with glass liners used in combination with a TDU. (see page 50) TDU/CIS TDU/CIS Septum for transportation adapter for liquid injection 1 package (100 units) Allen wrench for transportation adapter screws, 5 mm

52 GERSTEL Twister The GERSTEL Twister looks just like a conventional magnetic stir bar, except for the polydimethylsiloxane (PDMS) coating. While stirring the aqueous or polar liquid sample, the Twister efficiently extracts organic compounds into the PDMS phase. After stirring, the Twister is transferred to a GERSTEL Thermal Desorption System. Thermal desorption ensures efficient and quantitative transfer of analytes to the GC column and lowest detection limits. Thermally labile analytes can be desorbed using a liquid solvent for subsequent LC determination or for Large Volume Injection GC. Due to the large volume of PDMS on the Twister and due to the stirring effiency, it provides much greater capacity and much lower detection limits than SPME. Book»New Concepts in Sorption Based Sample Preparation for Chromatography«by H.A. Baltussen, 241 pages GERSTEL Twister for Stir Bar Sorptive Extraction (SBSE) with polydimethylsiloxane phase (PDMS) film thickness 0.5 mm, length 10 mm 10 units units film thickness 1 mm, length 10 mm 10 units units film thickness 0.5 mm, length 20 mm 10 units units film thickness 1 mm, length 20 mm 10 units units

53 GERSTEL Twister GERSTEL Twister kit Set of Twisters for Stir Bar Sorptive Extraction (SBSE) with polydimenthylsiloxane (PDMS) phase. film thickness 0.5 mm, 10 mm length (4 units) film thickness 1.0 mm, 10 mm length (2 units) film thickness 0.5 mm, 20 mm length (2 units) film thickness 1.0 mm, 20 mm length (2 units) Desorption tubes for use with TDS, TDS A2 or Tube Conditioner, TC 1/2 for Twisters with film thickness up to 1 mm, tube 6 mm OD, 4.5 mm ID, 1 package (10 units) Forceps Vials 1 2 ml vial with screw cap and septum, 1 package (100 units) ml vial 1 package (100 units) ml vial 1 package (100 units)

54 Twister Headspace Sorptive Extraction (HSSE), analyte extraction and concentration from the vapor phase using the GERSTEL Twister. HSSE is a concentration technique that is much more sensitive than traditional static headspace analysis. A Twister is placed in an open adapter inside a closed headspace vial. The Twister is placed in the vapor phase above the sample such that analytes are extracted by, and concentrated into, the PDMS phase of the Twister. Sorptive extraction and concentration of organic compounds provides lower detection limits when combined with a GERSTEL TDS or TDU system for thermal desorption GC or GC/MS analysis. TWISTER headspace vials 20 ml 1 package (100 units) Inserts for 20 ml Twister headspace vials 20 ml 1 package (100 units) Crimp caps for 10/20 ml vial (100 units) * Septa for 10/20 ml vial (100 units) * 54 Delivery times upon request *

55 GERSTEL Twister Twister Back Extraction Option for the MPS 3 consists of: 1.5 ml vials with caps and 200 µl inserts (100 units Opening lock for the Agitator (1 unit) Twister Back Extraction sequence software (1 unit) Requires, but does not include, GERSTEL MPS 3 with GERSTEL MASter software Crimper for 20 mm crimp caps (10/20 ml vials) Decapper for 20 mm crimp caps (10/20 ml vials) Mechanical crimper for 20 mm crimp caps Spare parts see page

56 GERSTEL Thermal Desorption System, TDS The GERSTEL Thermal Desorption System, TDS 3 is a highly optimized system for thermal desorption of Volatile Organic Compounds (VOCs) and Semi-Volatile Organic Compounds (SVOCs) followed by cryofocusing and GC analysis. Thermal desorption is a powerful concentration technique providing extremely low limits of detection. VOCs and SVOCs from gas-phase samples are trapped and concentrated on an adsorbent bed in a TDS tube by pumping a volume of the gas-phase sample through the tube. Solid and liquid samples can be placed in the TDS tube for direct thermal extraction or dynamic headspace of VOCs and SVOCs. In the TDS 3, analytes are thermally desorbed from the TDS tube using heat and a controlled flow of inert gas. Following primary desorption, analytes are concentrated on a second and smaller trap prior to GC or GC/MS determination. The GERSTEL Cooled Injection System, CIS functions as a cryotrap for the TDS 3, focusing and concentrating the compounds to be determined, and then transferring them to the capillary column in a narrow band for optimal GC separation using rapid, programmed heating. With the addition of the TDS A the TDS 3 becomes a fully automated thermal desorption system capable of unattended, automated analysis of up to 20 samples. A separate TDS system, the TDS G on-line, is designed for continuous on-line analysis of VOCs and SVOCs in air and gas streams. TDS A2 TDS 3 TDS G 56

57 GERSTEL TDS family TDS tube adapter for GERSTEL TDS 3 Allows 1/4 OD x 3.5 L desorption tubes to be used with the TDS 3 (stainless steel tubes only) Vespel cone Vespel cone for TDS Tube adapter 1 unit set (21 units) package (5 units) Screw driver SW 1.5 for TDS tube adapter Spare parts for TDS 2/3 septum head for liquid injection Special needle for 10 µl syringe, length 115 mm 1 package (5 units) Ice blue septa 5 mm 1 package (100 units) SLH adapter for spiking TDS tubes CIS CIS 4/ Special needle for 10 µl syringe, length 81 mm package (2 units) Supply kit for TDS 2/3 calibration adapter includes 5 glass tubes with GP 3D ferrules and 5 teflon ferrules SLH / CIS SLH / CIS

58 1 Desorption tubes 6 mm OD, for use with all GERSTEL TDS systems. Each tube has a unique serial number for identification and traceability packing conditioned description units 1 2 Tenax TA 60/80 Tenax GR glass tube glass tube Chromosorb 106 glass tube Carbosieve glass tube Carbotrap 300 multibed, glass tube Carbotrap 300 multibed, glass tube Tenax TA 60/80 1 Tenax GR 1 Chromosorb Carbosieve 1 Carbotrap B 100 mg Carbotrap C 200 mg Tenax TA 60/80 in storage container, glass tube Tenax TA 60/80 in storage container, SS tube Tenax GR in storage container, glass tube Tenax GR in storage container, SS tube Carbosieve in storage container, glass tube Carbosieve in storage container, SS tube Carbotrap 300 in storage container, glass tube Carbotrap 300 in storage container, SS tube Carbotrap 349 in storage container, glass tube Carbotrap 217 in storage container, glass tube Tenax / Carboxene in storage container, glass tube empty glass tube empty glass tube empty glass tube with glass frit empty glass tube with glass frit

59 GERSTEL TDS family GERSTEL TDS adsorbent overview Graphitized Carbon Blacks Carbotrap/Carbopack Unlike activated charcoals, which are porous, graphitized carbon blacks (GCBs), such as Carbotrap and Carbopack, are generally non-porous. Consequently, the entire surface of these materials is available for interactions that depend solely on dispersion (London) forces. These adsorbents offer excellent thermal stability, which ensures minimal bleed at thermal desorption temperatures, and their coarse 20/40 and 40/60 mesh particle size prevents high pressure drop across the tube. Hydrophobic properties minimize sample displacement by water, enabling you to obtain accurate samples despite high humidity. Trapped compounds can be desorbed by solvent or thermal desorption at virtually 100% desorption efficiency. Carbopack B is essentially the same adsorbent as Carbotrap; the only difference is the mesh size (60/80 mesh for Carbopack B vs. 20/40 mesh for Carbotrap). Both have a specific surface area of 100 m 2 /g. Carbopack B is often used in narrow bore tubes (1-2 mm ID), for sample refocusing or for very low flow sampling (e.g., <20 ml/min). This adsorbent is especially suited for trapping and thermally desorbing compounds in the range from C5 to C20 (depending on the size and structure of the molecule). Carbopack C is essentially the same adsorbent as Carbotrap C; the only difference is the mesh size (60/80 mesh for Carbopack C vs. 20/40 mesh for Carbotrap C). Both have a specific surface area of 10 m 2 /g. Carbopack C is often used in narrow bore tubes (1-2 mm ID), for sample refocusing or for very low flow sampling (e.g., <20 ml/min). This adsorbent is especially suited for trapping and thermally desorbing compounds in the range from C9 to C30 (depending on the size and structure of the molecule). Carbopack X, unlike most GCBs, is porous. Its surface area of 240 m 2 /g gives it greater adsorption strength than other GCBs, hence it is a unique bridge between GCBs and carbon molecular sieves. Carbopack Y, with a surface area of 24 m 2 /g, bridges the characteristics of Carbopack B and Carbopack C. Carbon Molecular Sieves A carbon molecular sieve is the carbon skeletal framework remaining after the pyrolysis of a polymeric precursor. These materials are primarily used for collecting very small molecules (e.g., chloromethane, vinyl chloride, and Freon compounds). The size and shape of the analyte molecule and the size and shape of the pores in the adsorbent particle determine how well the analyte is adsorbed and desorbed. Carbosieve S-III A large surface area (approximately 820 m2/g) and Å pores, make Carbosieve S-III excellent for trapping small airborne molecules, such as chloromethane. The pure carbon framework permits thermal desorption of analyte molecules without loss. Carboxen Carboxen carbon molecular sieves are highly hydrophobic, ensuring accurate sampling at high humidity. Carboxen 1000 is for low volume sampling of very volatile compounds, such as vinyl chloride. Its large surface area and optimized microporosity enable it to efficiently adsorb and desorb smaller molecules, providing excellent chromatography without a need for cryogenic cooling. This 60/80 mesh adsorbent is used primarily in narrow bore tubes that are desorbed directly into the chromatographic column. Carboxen 1003 has a large surface area and hydrophobic surface characteristics, which provide a combination of efficient adsorption/desorption and good hydrophobicity. Porous Polymers Tenax TA is a porous material based on 2,6-diphenylene oxide polymer. It is used to trap volatile and semivolatile compounds and has an upper temperature limit of 350 C. The material has a low affinity for water and methanol. When sampling for very volatile analytes with Tenax TA, a carbon molecular sieve is typically is used as a backup. Tenax GR is a composite material containing 30% graphite carbon and 70% Tenax TA. Compared to Tenax TA, it has a higher retention volume for most compounds and is twice as dense. Like Tenax TA, it has a low affinity for water and methanol and has an upper temperature limit of 350 C. Chromosorb 106 is a styrenedivinlybenzene poymer used to trap small molecules. It has a surface area of 750 m2/g and an upper temperature limit of 250 C. Its usefulness is somewhat limited since it produces relatively high levels of background. Multi-bed Adsorbent Tubes Multi-bed adsorbent tubes contain a series of two or three different adsorbents beds packed in order of increasing strength from the sampling end of the tube. A combination of adsorbents enables the analyst to cover a wide range of compounds in a single analysis. The first adsorbent is the weakest, retaining only higher boiling analytes while allowing smaller compounds to pass to the following adsorbent(s). The first adsorbent bed retains analytes that may get irreversibly trapped on the subsequent, stronger adsorbent(s). During thermal desorption of the multi-bed adsorbent tube, the gas flow direction is reversed ensuring that higher boiling analytes will not have to pass through the strong adsorbent beds, where they would be retained. Multi-bed adsorbent tubes enable the analyst to combine the benefits of multiple adsorbents in a single analysis while eliminating effects such as irreversible trapping and loss of larger molecules. Carbotrap 300 is a multi-bed tube comprised of Carbopack C, Carbopack B and Carbosieve S-III. Carbotrap 349 is a multi-bed tube comprised of Carbopack Y, Carbopack B and Carboxen Carbotrap 217 is a multi-bed tube comprised of Carbotrap B and Carboxen

60 Sorption tubes 1 packing conditioned description units PDMS 1 6 mm OD, glass tube, for gaseous samples 2 Supplies for desorption tubes OD description units 3 Storage Container 6 mm 2 single End cap set 6 mm 3 stainless steel, with PTFE seals End caps 6 mm stainless steel, with PTFE seals Storage end caps 1/4 3.5 long, brass TDS empty tubes 1/4 3.5 long, stainless steel Diffusion caps 1/4 3.5 long, stainless steel for TDS tubes Screens Tweezer for handling TDS tubes O-rings for TDS A sample magazine 1 package (10 units) Sealing plugs for TDS A/A2 sample magazine 1 package (10 units)

61 GERSTEL TDS family Spare parts for TDS 2/3 locking cone O-ring set for TDS 2/3 locking cone manual Inner O-ring for TDS 2/3-TDS A/A2 locking cone, 1 package (5 units) Fixing nut for inner O-ring for TDS 2/3 locking cone Spare parts for TDS A/A2 locking cone 1 1 Service kit for TDS A/A2 locking cone Fixing nut for inner O-ring for TDS A locking cone Inner O-ring for TDS 2/3/TDS A/A2 locking cone 1 package (5 units) Spindel O-ring 1 package (5 units) Spindel safety catch 1 package (5 units)

62 Direct interface for 0.7 mm OD transfer line System for transfer line OD units TDS 2/3 with CIS mm TDS 2/3 with CIS mm TDS 2/3 TDS G with CIS 3s 0.70 mm TDS 2/3 with CIS 3s Tremetics 0.70 mm Transfer lines for TDS 2/3 with CIS 3/CIS 4, length 5 m Version deactivated OD/ID ProSteel 0.67 mm/0.53 mm Silcosteel 0.74 mm/0.45 mm Sulfinert 0.74 mm/0.45 mm Transfer line kit for TDS 2/3 with CIS 3/CIS 4, length 1 m Version deactivated OD units ProSteel 0.67 mm 1 GRAPHPACK 2M ferrule Silcosteel 0.74 mm 1 GRAPHPACK 2M ferrule Sulfinert 0.74 mm 1 GRAPHPACK 2M ferrule Direct interface for 0.45 mm OD transfer line System OD units TDS 2/3 with CIS mm TDS 2/3 with CIS mm TDS 2/3 TDS G with CIS 3s 0.45 mm TDS 2/3 with CIS 3s Tremetics 0.45 mm Transfer line for TDS 2/3 with CIS 3/CIS 4, length 5 m Version deactivated OD Fused Silica 0.45 mm Transfer line kit for TDS 2/3 with CIS 3/CIS 4, length 1 m Version deactivated OD units Fused Silica 0.45 mm 1 GRAPHPACK 2M ferrule

63 GERSTEL TDS family GRAPHPACK 2M adapter for TDS 2/3, for 0.45 mm OD transfer line for TDS 2/3 and TDS G, for 0.7 mm OD transfer line Silver seal for GRAPHPACK 2M adapter for TDS 2/3 and TDS G 1 package (5 units) Spare parts for TDS G GRAPHPACK Micro screw single, 0.70 mm GRAPHPACK Micro ferrule 0.70 mm; 1 package (10 units) Adapter for GRAPHPACK Micro screw in conjunction with Valco Vici valve 1/ GRAPHPACK 2M injector adapter for Valco Vici valve, 1/16"

64 GERSTEL Pyrolysis Module, PM 1 Manual Pyrolysis module for the TDS. Sample tubes for GERSTEL Pyrolysis Module PM1 1 package (10 units) package (50 units)

65 GERSTEL Pyrolysis module, PM 1 Pyrolysis TDS tube for GERSTEL Pyrolysis Module, 6.0 mm OD; 5.0 mm ID Note for use with Pyrolysis Module only Quartz glass 1 units Borosilicate glass 10 units Spare parts O-ring set for TDS 2/3 manual locking cone Inner O-ring for TDS 2/3 locking cone 1 package (5 units) Fixing nut for inner O-ring for TDS A/A2 locking cone

66 GERSTEL Thermal Extractor, TE 1/2 The GERSTEL Thermal Extractor TE 2 enables the analyst to extract volatile and semi-volatile organic compounds from liquid or solid samples, trapping the compounds on a TDS tube for further analysis. For aldehyde analysis, analytes can be trapped on a DNPH tube for subsequent liquid elution and LC analysis. The GERSTEL TE 2 has a larger inner diameter than normal TDS tubes. Larger sample volumes can be analyzed to obtain lower detection limits. A larger, more representative sample volume also ensures better results when analyzing inhomogenous samples. The GERSTEL TE 2 is completely independent of the TDS system, eliminating the risk of system contamination when analyzing unknown samples. O-ring set for tube holder complete set of inner and outer O-rings Inner O-ring for tube holder 1 package (5 units)

67 GERSTEL Thermal Extractor, TE 1 Empty tubes for GERSTEL TE 1 package (5 units) Inner O-ring for TE tube holder Kalrez (1 units) PTFE ferrule for TDS desorption tube 1 package (5 units) Desorption tubes for TDS 2/3 and TDS A/A2 see pages Screens for TE tube 1 package (10 units)

68 GERSTEL Tube Conditioner, TC 1/2 For simultaneous conditioning of up to ten TDS tubes or up to 50 Twister s (5 Twisters per TDS tube). Tube conditioning is performed under a flow of inert gas at elevated temperatures. The gas flow to each tube is independently controlled allowing full loading flexibility. The GERSTEL TC 2 operates independently of the analytical system, eliminating the risk of system contamination and ensuring maximum productivity. 68

69 GERSTEL Tube Conditioner, TC 1/2 O-ring set for TC 1/2 tube holder 1 package (1 sets) TDS desorption tubes for 1 mm film thickness Twisters; tube 6 mm OD x 4.5 mm ID 1 package (10 units)

70 GERSTEL Column Switching Systems, MCS The GERSTEL MultiColumn Switching System, MCS enables the combination of different capillary columns in one system for improved separation of complex samples. The system enables venting of solvent and low-boiling compounds, improved overall separation, targeted separation of a particular section of a chromatogram on a separate column, and accurate effluent splitting between detectors such as MSD, FID, FPD and the GERSTEL Olfactory Detection Port, ODP.! Important note Column switching devices are available only for customers with a GERSTEL column switching system. GRAPHPACK 3D/2 column switching device for MCS 2, Sulfinert pre-column OD (mm) main column OD (mm) GRAPHPACK 3D/2 mounting tool kit for column switching device For the rapid creation of low-dead-volume connections when using GRAPHPACK 3D/2 column switching device. Suitable for all capillary columns with outside diameters between 0.2 mm and 0.8 mm. complete kit GRAPHPACK mounting tool tool body without insert For GRAPHPACK 3D/2 ferrules and GRAPHPACK 2M ferrules see GRAPHPACK section beginning with page 16.

71 GERSTEL Multi Column Switching Systems, MCS Insert for 1.5 mm column mounting depth Color: gold Insert holder Column OD 0.20 mm to 0.31 mm mm to 0.45 mm mm to 0.80 mm GRAPHPACK 3D/2 ferrule kit for MCS Fixing nut for column switching device Restriction capillary deactivated column OD / column ID / length units 0.40 mm / 0.05 mm / 0.4 m mm / 0.05 mm / 5 m mm / 0.05 mm / 10 m

72 GERSTEL Preparative Fraction Collector, PFC The GERSTEL PFC is used for purification and collection of compounds or compound classes following separation by capillary gas chromatography. Compounds are automatically and selectively collected in up to six different traps that can be heated or cooled depending on the needs for the type of compounds. Highly accurate switching between the traps enable the analyst to collect and accumulate compounds with high purity and high yield from up to 150 GC runs. A seventh trap is available to collect all compounds not collected in the main traps. These compounds can be saved for further analysis or for conducting subtraction studies of key compounds. 72

73 GERSTEL Preparative Fraction Collector, PFC GRAPHPACK 3D/2 mounting tool kit for switching device For the rapid creation of low-dead-volume connections when using the PFC switching device. Suitable for all capillary columns with outside diameters 0.45 mm. complete kit Spare parts GRAPHPACK mounting tool single, without insert Insert for 3.0 mm mounting depth Color: silver Insert holder Column OD 0.45 mm GRAPHPACK 3D/2 sealing ferrule 1 package (5 units) Column OD (mm)

74 GRAPHPACK 3D/2 ferrule kit for PFC GRAPHPACK 3D/2 switching device for PFC, Sulfinert complete! Important note Switching devices are available only for customers with a GERSTEL Preparative Fraction Collector GRAPHPACK 3D/2 effluent splitter for FID, Sulfinert for HP 5890 II, Agilent 6890 column OD 0.70 mm Replacement Fixing nut Restriction capillary deactivated, 0.40 mm OD, 0.05 mm ID length 80 mm (5 units) m (1 unit) m (1 unit) Silicone tubing for PFC for connecting component traps to solenoid valve length 10 m

75 GERSTEL Preparative Fraction Collector, PFC Trap adapter for traps 1 µl 100 µl 1 unit Sample traps 1 1 µl 1 package (10 units) package (50 units) µl 1 package (10 units) package (50 units) Teflon ferrules for sample traps ID 3.0 mm; for traps 1 µl and 100 µl 1 package (10 units) Sample traps, coiled 1 µl 1 package (10 units) Teflon ferrules for sample traps 1 package (10 units) ID 1.8 mm for 1 µl, coiled traps Transfer capillary for connecting FID effluent splitter to PFC switching device, deactivated OD 0.45 mm L = 870 mm 1 package (5 units) Capillary for sample trap for connecting switching device to component traps, deactivated OD 0.45 mm 180 mm (5 units) m (1 unit) m (1 unit)

76 GERSTEL Olfactory Detector Port, ODP 2 The GERSTEL ODP allows olfactory detection of compounds by the human nose. Olfactory detection is performed in parallel to GC detection with FID, FPD or MSD detectors as compounds elute from the GC column. The effluent is split as it leaves the column, arriving simultaneously at the nose and at the detector, enabling the analyst to gain additional information on odor-active compounds. Using a headset with a microphone coupled to voice recognition software, the analyst can insert spoken comments directly into the chromatogram for peak annotation and into the analysis report. 1 Nose cones for use with ODP 1/2 with humidifier for use with ODP 1/2 without humidifier GRAPHPACK 3D/2 column connector with 1/16 gas connection, Sulfinert Column OD from 0.80 mm OD to 0.45 mm Silicone tubing for connecting nose cone and humifidier vial length 2 m

77 GERSTEL Olfactory Detection Port, ODP 2 Humidifier vial GRAPHPACK 3D/2 crosspiece kit, Sulfinert for Agilent GC detectors, allows simultaneous detection at the nose and the GC detectors. Includes: GRAPHPACK adapter for MSD and FID or TCD main column OD splitter/restrictor capillary OD 0.31 mm 0.40 mm mm 0.40 mm mm 0.40 mm GRAPHPACK 3D/2 crosspiece, Sulfinert 1 main column OD 2 splitter/restrictor capillary OD mm 0.40 mm mm 0.40 mm mm 0.40 mm GRAPHPACK 2M detector adapter MSD HP 5971/5972 GCD Series G 1800 A HP 5890 A and Series II and Agilent 6850/ Spare parts GRAPHPACK nut for all GRAPHPACK adapters; 1 package (5 units) Splitter/restrictor capillaries OD/ID length units 0.36 mm / 0.10 mm 1 m mm / 0.10 mm 5 m m mm / 0.20 mm 10 m mm / 0.15 mm 2 m mm / 0.15 mm 5 m

78 GERSTEL ChemSensor Systems For classification of compound groups or sample groups based on chemometric analysis with or without chromatography separation. Three-dimensional data (intensity, mass fragment and retention time) obtained with a mass selective detector MSD is reduced to two dimensions, enabling fast and reliable classification of samples. Introduction techniques used are Headspace and SPME. MSD spare parts CI Filament for the Agilent 5973/5975 MSD; 1 package (2 units) * 78 Delivery times upon request *

79 GERSTEL ChemSensor Systems GERSTEL ChemSensor interface spare parts Transfer capillary ID = 0.1 mm, OD = 0.36 mm, l = 1 m GRAPHPACK 2M ferrule for column OD 0.4 mm; 1 package (10 units) GRAPHPACK 2M blind plug 1 package (10 units) GRAPHPACK nut 1 package (5 units) Direct interface for ChemSensor CIS 4 Plus Silver seal for direct interface; 1 package (5 units) GRAPHPACK 2M MSD adapter for Hewlett-Packard or Agilent Technologies 5971/5972/5973/5973 N/5973 Inert/5975 MSD, for column OD 0.4 mm Silver seal for GRAPHPACK 2M MSD adapter 1 package (5 units) Vials and crimp caps for the ChemSensor ml Crimp cap vial clear, with flat bottom for 20 mm caps for use with the Agilent Technologies 7694 Headspace Autosampler Crimp caps Aluminum crimp caps with safety closure, Silicone / PTFE septum, for 20 mm vials 1 package (100 units) package (5 units)

80 GERSTEL approved supplies Beside our own supplies for GERSTEL systems we offer a wide range of supplies from other manufacturers. These products have been tested by us and have our approval for ensuring proper operation with GERSTEL systems. SS capillary 1/8", 1 m Cu tubing 1/8", 1 m Swagelok SS adapter complete with nuts and ferrules 1 unit 1/16" SW, complete /8" SW, complete /4" SW, complete /16" to 2 mm Swagelok set consisting of nut, ferrule, and back ferrule 1 unit 1/4" SS /8" SS /16" SS package (10 units) 1/4" MS /8" MS /16" MS Tube adapter for VICI actuator 1 package (2 units)

81 GERSTEL approved supplies Tools Set of mandrels 1 package (5 units) Magnifying glass (plastic) 10x Diamond file Open end wrenches complete set; 6 units, sw SW SW SW SW SW SW

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