MICRO GC FUSION Micro GC Fusion 3/17/2014 1

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1 MICRO GC FUSION 1

2 Micro GC Fusion The Next Generation Micro GC 2

3 Builds on an Innovative Tradition 3000 Micro GC Micro GC Fusion MTI Micro GC 3

4 Micro GC Fusion Feature Highlight New Chassis Design Aesthetic, transportable design with a small footprint Adopted Expanded Polypropylene 25% weight reduction Better heat insulation Multi-touch control and status display on the instrument Front and/or rear sample inlet(s) Optional integrated sample conditioner 4

5 Micro GC Fusion Feature Highlight Temperature Programming Fast temperature ramping based on resistive column heating technology Ramp rate up to 300 C/min Ramping profile is independently optimized for each module Bench top GC limited to single oven Rapid cool down time reduces cycle time Column Temp Time 5

6 Isothermal vs. Temperature Programming Isothermal runs result in broad, late eluting peaks Fast temperature ramping sharpens peak shape, shortens run time, and purges impurities off the column Example Propane Isothermal, elutes at ~160 seconds Temperature ramping, elutes at ~50 seconds Sharper peak Increased intensity Column: PLOT Q 6

7 Micro GC Fusion Feature Highlight Integrated Sample Conditioner Integrates sample conditioning into the instrument Filters particulates Heats incoming sample to 100 C Reduces sample pressure from up to 1000 psi to between 5 10 psi Automates flushing and sampling operation with electronic valves Optional based on application requirement Factory configured for front sample inlet (quick connect) or rear sample inlet (1/8 SS) 7

8 Micro GC Fusion Feature Highlight Control & Data interface Control through web-based GUI and embedded software No software installation is required Multi-touch LED display Front panel operation Run stored methods Access analysis result Display instrument status Local data storage Store methods and analysis results Wi-Fi connectivity Operate instrument from wirelessly connected computing devices such as laptops or tablets 8

9 Micro GC Fusion Feature Highlight Web-based graphical user interface Intuitive work flow caters to both expert and non-expert chromatographers OS platform independent Runs on Internet browsers Embedded software No installation required No software licensing required 9

10 Micro GC Fusion Advantages Temperature programming More components can be analyzed on a single column Faster analysis for heavier hydrocarbon Better peak resolution Minimize carry over Direct instrument control and status display with multi-touch LED display No external software installation and licensing with webbased software Operate instrument wirelessly using tablet or laptop Integrated sample conditioner eliminates cumbersome external attachment 25% lighter 10

11 MICRO GC FUSION HARDWARE 11

12 Micro GC Fusion Front Multi-touch LED display Illuminated power button Heated and deactivated front sample inlet 12

13 Micro GC Fusion Back Wi-Fi external antenna Carrier gas inlets Rear sample inlet 24VDC power RJ-45 LAN connector Analytical, reference and sample venting connections AUX I/O connector USB data ports 13

14 Micro GC Fusion Modular Architecture Modular architecture allows sample to be analyzed by multiple GC modules in parallel, each with an optimized analytical method to focus on the target compounds Sample Gas Split GC Module B method: Temperature profile #2 Pressure #2 Injection time #2 GC Module A method : Temperature profile #1 Pressure #1 Injection time #1 14

15 Micro GC Fusion MEMS Based GC Module Each Fusion GC module is built on state of the art microelectromechanical systems (MEMS) technology that miniaturizes the injection and detection subsystems, coupled with a resistively heated column to provide fast temperature ramping capability Resistively heated column MEMS based Injector Assembly MEMS based μtcd Assembly 15

16 Micro GC Fusion MEMS Injector Types Variable Volume General analysis from 10 ppm to 100% Variable Large Volume Best for analyses down to 1 ppm Fixed Volume Offers the best precision for components above 500 ppm BackFlush Includes a pre-column to prevent contaminants from entering the analytical column Can be run in a semi-fixed or variable injection mode Minimizes ghost peaks 16

17 Micro GC Fusion Column Support Wall Coated Open Tubular (WCOT) Liquid phase bonded to the surface of the tubing Examples: PDMS, Wax, 1701 Porous Layer Open Tubular (PLOT) Solid particles coated on the surface of the tubing Examples: Molsieve 5A, PLOT U, PLOT Q, Alumina, Carbon PLOT 17

18 Micro GC Fusion μtcd Micro GC Fusion uses a Wheatstone bridge μtcd which is built on the microelectromechanical system (MEMS) technology Thermal conductivity detector (TCD) compares the thermal conductivity of the gas from the reference column vs. the gas from the analytical column The μtcd provides 6 decades (10 6 ) of linear dynamic range, i.e. from low parts-per-million (ppm) to 100% Wheatstone Bridge 18

19 MICRO GC FUSION SOFTWARE 19

20 Web-based Graphical User Interface Micro GC Fusion software is embedded in the instrument. It is controlled through a web-based GUI which can be operated from multi-touch LED front panel display or an external computing device through common web browsers Multi-touch LED display GUI is loaded automatically after system is started Run stored methods, view run results and system status External computing device Full spectrum of instrument control and status Operating system independent, works with common web browsers Connects wirelessly through Wi-Fi No installation or licensing required 20

21 Routine Operation Run Method Run Method Real-time Chrom. View Result Using a predefined analytical method stored on the instrument, simply press the RUN button to perform a sample analysis, view the chromatogram in real time and access the results. 21

22 Method Development 1. Define Sampling Method 2. Run Calibration Sample 3. Perform Calibration Instrument control and calibration screens are available to define and develop analytical method for various applications 22

23 Sequence Definition Advanced sequencing is available to automate sampling process 23

24 Utility Screens System Setup Provides network configuration interface System Status Provides temperature and pressure information for both system and module levels Data Browser Provides quick access to analysis data files stored on Fusion 24

25 MICRO GC FUSION APPLICATIONS 25

26 What Can a Micro GC Fusion Do A gas chromatograph (GC) specifically designed for gas analysis Configurable with 1 or 2 GC modules to address application needs Simple to setup and use Compact footprint ideal for lab, pilot plant, or field applications Fast analysis: secs Lab Pilot plant Field 26

27 Micro GC Fusion Analyses in ppm to % He, H2, O2, N2, CO, CO2 (fixed gases) C1 C12 hydrocarbons C2 C5 olefins Methanol, DME, ethanol, acetaldehyde, formaldehyde (light oxygenates) Benzene, toluene, ethyl benzene, xylenes (VOCs) H2S, SO2, TBM, THT, N2O Plus many, many more components 27

28 Natural Gas Analysis Measures the individual components in natural gas for a variety of applications Composition information used to calculate calorific value (BTU) and density Odorants analysis to comply with natural gas safety regulations Suitable for natural gas samples from wellhead to pipeline quality gas in the field or in the lab 28

29 Standard Natural Gas Analysis One Module Traditionally, the PLOT Q is used for C1-C3 analysis only Using temperature programming, the same module can be used for C1-C8 Plus natural gas analysis Column: PLOT Q Ramp: 45 C 250 C (4 C/s) 29

30 Extended Natural Gas A PDMS (OV-1) module can be added to conduct extended hydrocarbon (C1 C11) analysis for natural gas Column: PDMS Ramp: 50 C 130 C 280 C (2 C/s, 5 C/s) 30

31 Fixed Gas Analysis The Molsieve 5A column analyzes typical fixed gases found in syngas, landfill gas, fuel cell gases, and refinery gases Injector: Backflush Isothermal: 100 C Late backflush Injector: Backflush Ramp: 100 C(10s)-->200 C (2 C/s) Late backflush With temperature programming ethane elutes nearly 3 times faster 31

32 Micro GC Fusion Main Applications Natural Gas Refinery Gas Landfill Gas Dissolved Gas Fixed Gas Catalyst Research Alternative Energy Sulfur Analysis 32

33 Winner of Gas & Instrumentation Magazine 2014 Golden Gas Awards GC Category Award presentation at Pittcon

34 Micro GC Fusion Sensitive. Smart. Easy Going. 34

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