Elastomer Classification and Characterization

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1 Recmmended Practice Elastmer Classificatin and Characterizatin Ver 1.0 PCP Run Life Imprvement JIP Participants Prepared by K.L. Kishiuchi, MSc, EIT Reviewed by B.T. Wagg, MSc, PEng Cpyright 2007 C-FER Technlgies September 2007 R004

2 NOTICE 1. This Recmmended Practice was prepared as an accunt f wrk cnducted at C FER Technlgies (1999) Inc. ( C FER ) n behalf f the PCP Run Life Imprvement JIP Participants. All reasnable effrts were made t ensure that the wrk cnfrms t accepted scientific, engineering and envirnmental practices, but C FER makes n ther representatin and gives n ther warranty with respect t the reliability, accuracy, validity r fitness f the infrmatin, analysis and cnclusins cntained in this Recmmended Practice. Any and all implied r statutry warranties f merchantability r fitness fr any purpse are expressly excluded. Any use r interpretatin f the infrmatin, analysis r cnclusins cntained in this Reprt is at the reader s wn risk. Reference herein t any specified cmmercial prduct, prcess r service by trade name, trademark, manufacturer r therwise des nt cnstitute r imply an endrsement r recmmendatin by C FER. 2. The infrmatin cntained in this Recmmended Practice is cnfidential and prprietary t C-FER and may nt be cpied, distributed, referenced r quted withut the prir written apprval f C-FER. 3. Cpyright C-FER All rights reserved. Recmmended Practice Ver 1.0 C-FER File N. R004 (CONFIDENTIAL) i

3 TABLE OF CONTENTS Ntice Acknwledgements Frewrd i iii iv 1. SCOPE ELASTOMER CLASSIFICATION AND CHARACTERISTICS Adpted Elastmer Classificatins and Characteristics Classificatins Characteristics 2 APPENDICES Appendix A Review f ISO Appendix B Sample Table Recmmended Practice Ver 1.0 C-FER File N. R004 (CONFIDENTIAL) ii

4 ACKNOWLEDGEMENTS C-FER wuld like t acknwledge the cntributin f the JIP Participants and PCP vendrs in the develpment f this Recmmended Practice. PCP Vendrs include: Dyna-Drill Technlgies Kudu Industries Inc. / PCM Natinal Oilwell Varc NETZSCH Oilfield Prducts R&M Energy Systems Tierra Alta Weatherfrd Artificial Lift Recmmended Practice Ver 1.0 C-FER File N. R004 (CONFIDENTIAL) iii

5 FOREWORD The bjective f this Recmmended Practice is t prvide a cmmn terminlgy fr the classificatin and characterizatin f PCP elastmers, fr use within the PCP RLI Jint Industry Prject, based n infrmatin cmmnly reprted by PCP vendrs t their clients. There are currently n industry standards fr the classificatin and characterizatin f elastmers fr PCP applicatins. Hwever, the tpic is under discussin by an ISO sub-cmmittee (ISO Petrleum and natural gas industries Dwnhle equipment Prgressing cavity pump systems fr artificial lift Part 1: pumps), and a draft f this standard may be released late in As much as pssible, the classificatins and elastmer characteristics used in this Recmmended Practice have been aligned with the ISO standard where apprpriate. This will reduce the amunt f future wrk needed t make the PCP RLI prject cmpliant with the ISO standard nce it is cmpleted. Fr a review f infrmatin anticipated t be included in the ISO standard, see Appendix A. Fr further detail n the infrmatin prvided by the vendrs, specific values and descriptrs reprted, and a translatin f thse descriptrs and values int the adpted classificatins and characteristics used in this Recmmended Practice, see the C-FER Reprt: Classificatin and Characterizatin f Selected Elastmers, which was issued in cnjunctin with this Recmmended Practice. Recmmended Practice Ver 1.0 C-FER File N. R004 (CONFIDENTIAL) iv

6 1. SCOPE Elastmer selectin plays a key rle in btaining reasnable run-lives f prgressing cavity pumps (PCPs) when prducing a wide range f fluids. Elastmers are knwn t be particularly sensitive t the presence f armatics, H 2 S, CO 2, water and high temperature. In an effrt t understand hw elastmer prperties affect pump run-life fr a given set f perating cnditins, elastmer prperties must first be tracked and included in the Prgressing Cavity Pumping Run-Life Imprvement (PCP RLI) database fr analysis, thrugh investigatins such as the fllwing: Differences in elastmer selectins by different peratrs What elastmers are peratrs using in varius applicatins? What type, r with what main characteristics? Relatin f pump perfrmance t elastmer type and applicatin characteristics Is ne elastmer type r are elastmers with certain characteristics utperfrming thers in specific applicatins? It is acknwledged that vendrs may have different methds fr determining reprted prperties r characteristics. Methds fr testing, evaluating and determining elastmer characteristics are nt cvered by this Recmmended Practice. Recmmended Practice Ver C-FER File N. R004 (CONFIDENTIAL)

7 2. ELASTOMER CLASSIFICATION AND CHARACTERISTICS 2.1 Adpted Elastmer Classificatins and Characteristics Based n infrmatin prvided by the vendrs and recmmendatins carried frward t the Steering Cmmittee (SC), in the PCP RLI JIP, the classificatins and characteristics listed in Sectins and are used fr describing elastmers in the prject database. Appendix B cntains a sample table which may be used fr recrding this data fr a grup f elastmers Classificatins Elastmer Name a unique name given by the pump manufacturer t distinguish amng elastmers within the same elastmer type. Elastmer Type Six grups are used: 1. Medium ACN NBR includes nitrile butadiene rubbers r nitrile rubbers (NBR) with acrylnitrile (ACN) cntent <= 35% 2. High ACN NBR includes NBRs with ACN cntent > 35% 3. Medium ACN HNBR includes highly r fully-saturated hydrgenated nitrile rubbers (HNBR) with ACN cntent <= 35% 4. High ACN HNBR includes HNBRs with ACN cntent > 35% 5. FKM flurcarbn elastmers 6. Other Characteristics General Descriptin (free frmat) infrmatin prvided by the pump vendr. Temperature Limit a single value. This shuld represent the maximum temperature nrmally recmmended fr the elastmer. Chemical Resistance Resistance t each f the fllwing substances are rated: H 2 S CO 2 Armatics Water The fllwing five qualitative descriptrs are used fr rating chemical resistance: 1. Excellent 2. Gd 3. Average Recmmended Practice Ver C-FER File N. R004 (CONFIDENTIAL)

8 Elastmer Classificatin and Characteristics 4. Fair 5. Pr Mechanical Prperties Wear Resistance The fllwing five qualitative descriptrs are used: 1. Excellent 2. Gd 3. Average 4. Fair 5. Pr Hardness (Shre A) a single value. When a range is prvided by the pump vendr, the median value f the range is used. Nte: This Recmmended Practice is nt prescriptive in hw vendrs shuld determine each f the five qualitative descriptrs fr Chemical and Wear Resistance. Vendrs may rank their wn prducts in terms f their relative perfrmance withut cnsidering hw their elastmers cmpare t thse f ther vendrs. Recmmended Practice Ver C-FER File N. R004 (CONFIDENTIAL)

9 APPENDIX A REVIEW OF ISO Review f ISO Elastmer Classificatins and Characteristics The ISO sub-cmmittee tasked with reviewing ISO fr prgressing cavity pumps is cmprised f representatives f many statr manufacturers (including PCM, Netzsch, Centrilift, R&MES and Weatherfrd) and peratrs (CncPhillips, Exxn Mbil, Ttal, Shell, Petrbras, Ameriven and Husky). The new versin f the ISO dcument may include standard methds and nmenclature fr classifying and characterizing elastmers. Infrmatin regarding classificatins and characteristics currently being discussed by the subcmmittee are included in this Recmmended Practice as backgrund infrmatin and t prvide reasning as t why certain classificatins and characteristics have been adpted in this Recmmended Practice. As an fficial draft f the ISO standard had nt been released when this Recmmended Practice was written, this infrmatin may nt reflect the cntents f the final ISO Standard when it is released. Classificatins The fllwing is a list f classificatins prpsed t be used by the ISO sub-cmmittee: Nitrile elastmer (NBR) Medium: ACN cntent <=35% High: ACN cntent >=36% Nte: ther cmpund characteristics, besides ACN cntent, determine elastmer perfrmance Hydrgenated nitrile elastmer (HNBR) Medium: ACN cntent <=35% High: ACN cntent >=36% Flur elastmer (FKM) Other Characteristics (Specificatins) The fllwing is a prpsed list f characteristics, termed specificatins by the ISO subcmmittee, fr use in the standard: Mandatry infrmatin (shuld be available t users) based n standard test prcedures Recmmended Practice Ver 1.0 A.1 C-FER File N. R004 (CONFIDENTIAL)

10 Appendix A Review f ISO Oil and chemical resistance Water and IRM 903 immersin (mass, vlume, hardness, tensile strength changes) Mechanical Prperties Hardness (reprting n instantaneus and 10 secnd delays) Service Temperature Limits (varies accrding t exact elastmer frmulatin and prcessing cnditins, and fr specific applicatin parameters) Optinal infrmatin based n recmmended test prcedures Crude il resistance Mechanical prperties variatin with aging Tear strength, abrasin resistance, cmpressin mdulus Explsive decmpressin resistance Cmpressin set H 2 S resistance Dynamic prperties Bnd retentin Recmmended Practice Ver 1.0 A.2 C-FER File N. R004 (CONFIDENTIAL)

11 APPENDIX B SAMPLE TABLE Vendr Elastmer Name Elastmer Type (ACN Level) General Descriptin and Applicatin Chemical Resistance Temperature Limit ( C) H 2 S CO 2 Armatics Water Mechanical Prperties Wear Resistance Hardness (Shre A) Other Cmments Table B.1 Sample Elastmer Data Table Recmmended Practice Ver 1.0 B.1 C-FER File N. R004 (CONFIDENTIAL)

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