Pre-installation guide for analytical systems User manual HPLC

Transcription

1 Pre-installation guide for analytical systems User manual HPLC

2 For your own safety, read the manual and always observe the warnings and safety information on the device and in the manual! 1 Manuel en français: Si jamais vous préfériez un manuel en français pour ce produit, veuillez vous contacter le support technique (Technical Support) par ou par fax avec le no. de série. Merci beaucoup. Technical Support: Phone: (9-17h, Central European Time) Fax: support@knauer.net Languages: German, English Publisher: KNAUER Wissenschaftliche Geräte GmbH Hegauer Weg 38 D Berlin Phone: Fax: Internet: info@knauer.net Version information: Article number: V6802 Version number: 3.1 Last update: 2017/06/19 Original edition

3 2 The information in this document is subject to change without prior notice. For latest version of the manual, check our website: Copyright: This document contains confidential information and may not be reproduced without written content of KNAUER Wissenschaftliche Geräte GmbH. KNAUER Wissenschaftliche Geräte GmbH 2017 All rights reserved. AZURA is a registered trademark of KNAUER Wissenschaftliche Geräte GmbH.

4 Table of contents Table of contents 3 Overview Storing unopened shipping boxes Installation site requirements Ambient conditions Space requirements of the HPLC system Analytical AZURA HPLC systems Individual devices System layout examples Power supply Universal AC/DC switching power adapter Power cable Power connection Minimum computer requirements KNAUER ClarityChrom /KNAUER ClarityChrom Prep OpenLAB CDS EZChrom Edition KNAUER PurityChrom Thermo ScientificTM DionexTM ChromeleonTM 7.2 CDS KNAUER Mobile Control Uninstalling software, KNAUER drivers and extensions Settings for sleep function Technical data Checklist Index

5 4 Overview Overview This manual describes how to prepare for installing an analytical AZURA System. It contains information on the following: intermediate storage of shipping boxes system set-up installation site requirements dimensions of analytical systems power supply characteristic data of individual modules computer requirements for software Storing unopened shipping boxes The shipping boxes are supplied on a pallet sized 80 x 120 cm. In your planning, include the following information for immediate storage of this pallet. sufficient space storage temperatures must be in the temperature range 4 40 C, F Installation site requirements The HPLC system will be set up, installed and commissioned by KNAUER or a company authorized and contracted by KNAUER. KNAUER recommends inviting future users to be present while setting up and commissioning the module so that they can become familiar with the analyzer and how to handle it. Ambient conditions humidity: below 90 % (non-condensing) temperature range: 4 40 C; F Space requirements of the HPLC system Only if the requirements for ambient conditions of the operating environment are met, can the intended use be ensured. Details on the operating conditions can be found in the Technical Data section.

6 Installation site requirements 5 Device defect The device overheats at exposure to sunlight and insufficient air circulation. Device failures are very likely. Set up the device in such a way that it is protected against exposure to direct sunlight. Keep at least 15 cm clear at the rear and 5 10 cm at each side for air circulation. Space requirements At least 5 cm if another device is set up on one side At least 10 cm if further devices are set up on both sides At least 15 cm on the rear panel for the fan. Leave the power plug on the rear of the device accessible to be able to disconnect the device from the mains. General requirements Position the device on a level and even surface. Protect the device against direct exposure to sunlight. Set up the device at a location not exposed to air drafts (A/C systems). Do not set up the device near other machines that cause floor vibrations. The leak sensor may malfunction if the device is placed on an inclined surface. Use a level to check that the device is in horizontal position. Earth quake regions If the device is set up in a region where earth quakes are common, secure the device at the two fixing points 1. The fixing points are situated on both sides of the device.

7 6 Analytical AZURA HPLC systems 1 Fig. 1 Fixing points on the device Analytical AZURA HPLC systems Individual devices Systems for analytical applications typically consist of the following devices: solvent tray gradient pump (quaternary, binary, or isocratic) with degasser, mixing chamber, and pressure sensor autosampler or manual valve analytical column column thermostat detector System layout examples Examples for set-up of an AZURA HPLC system: 1 detector (example) 2 pump (example) 3 solvent tray 4 column thermostat 5 autosampler Fig. 2 AZURA system, horizontal setup

8 Power supply 7 1 solvent tray 2 pump (example) 3 detector (example) 4 column thermostat 5 autosampler Power supply Universal AC/DC switching power adapter The modules are equipped with an universal AC/DC switched-mode power adapter rated for V AC. Power cable Power cables are part of the delivery and come in numbers matching the destination. The cables are available for the following destinations: EU, USA, Switzerland, UK Power connection Fig. 3 AZURA system, vertical setup Prerequisites for power connection: The electrical power supply at the installation site must be connected directly to the nearest main power line. The power must be free from ripple, residual current, voltage peaks and electromagnetic interference. The connectors for the mains voltage are grounded accordingly. The modules receive sufficient power and reserve capacity. The number of sockets corresponds to the number of devices in the system. Multi-outlet power strip with ON/OFF switch for individual system modules and additionally required modules.

9 8 Minimum computer requirements Electronic defect Damage to the electronics if the device is turned on while connecting or interrupting the power connection. Switch off the device beforehand. Minimum computer requirements KNAUER ClarityChrom /KNAUER ClarityChrom Prep Operating system CPU Memory (RAM) Graphics/resolution Drive Free disc space 1 Connections 2 Windows 10, 32/64 bit Windows 8, 32/64 bit Windows 7, 32/64 bit Windows Vista (SP2), 32/64 bit Windows XP (SP3) Pentium 2 GHz Windows XP: 512 MB MB for each addtl. system or PDA detector up to 10 Hz data rate Windows 10 / 8 / 7 / Vista: 2 GB MB for each addtl. system or PDA detector up to 10 Hz data rate For all: 4 GB for PLATINblue PDA-1 and AZURA DAD 6.1L / 2.1L Separate graphics card recommended if more than 1 system is to be controlled DVD ROM (12x) 20 GB available, 80 GB for PLATINblue PDA-1 and AZURA DAD 6.1L / 2.1L USB for the licence dongle COM or USB and/or LAN for device control (depends on device type) 1. At high data transfer rates of the PDA detector, files with up to 100 MB file size may be created. 2. For every device that you want to connect via serial port, a separate COM port is required. You may use a USB-to-COM adapter to increase the number of ports. OpenLAB CDS EZChrom Edition For the OpenLAB Distributed Systems license, you need a Shared Services Server. For Distributed Systems licenses, the Shared Services server must be installed on a separate computer with Windows Server operating system.

10 Minimum computer requirements 9 Prerequisite Microsoft.NET Framework 3.5 with SP1 and Windows Installer 4.5 (for SQL Installation with Shared Services Server) must be installed. Operating system Windows 8.1, 32/64 bit (EZChrom Edition Workstation, EZChrom Edition Client) Windows Server 2008 (R2, SP1) (Shared Services Server, EZChrom Edition Client) Windows 7 (SP1), 32/64 bit (EZChrom Edition Workstation, EZChrom Edition Client) CPU 3 GHz Dual-Core Memory (RAM) 4 GB (32 bit) 6 GB (64 bit) Graphics/resolution separate graphic card for > 1 system Drive DVD ROM (12x) Free disc space GB Connections 2 100/1000 Mbit LAN Adapter LAN, COM or USB for device control (depends on device type) KNAUER PurityChrom 5 Operating system CPU Memory (RAM) Windows 10, 32/64 bit Windows 8, 32/64 bit Windows 7, 32/64 bit Windows Vista (SP2), 32/64 bit Windows XP (SP3) 2GHz 512 MB (Windows XP) 1.5 GB (Windows 8/7/Vista: 32 bit) MB for a PDA-Detector MB for every additional system 2 GB (Windows 8/7/Vista: 64 bit) + 4 GB for DAD 6.1L Graphics/resolution Drive DVD ROM (12x) Free disc space 1 20 GB Connections 2 USB for the licence dongle LAN, COM or USB for device control (depends on device type)

11 10 Uninstalling software, KNAUER drivers and extensions Thermo Scientific TM Dionex TM Chromeleon TM 7.2 CDS Operating system CPU Memory (RAM) Graphics/resolution drive Free disc space 1 Connections 2 KNAUER Mobile Control 4.0 Uninstalling software, KNAUER drivers and extensions To uninstall chromatography software and device drivers, use the Windows Control Panel (CONTROL PANEL > UNINSTALL A PROGRAM). Settings for sleep function Windows 8.1, 64 bit (Professional Edition) Windows 7 (SP1), 64 bit (Professional/Ultimate Edition) Using of 32 bit versions is not recommended. Windows Vista (SP2), 32 bit (Business/Ultimate Edition), using of Windows Vista is not recommended. 3 GHz Intel Core 2 Duo 3GB , 32 bit colours DVD ROM (12x) 60 GB USB for the licence dongle LAn for device control Operating system Only for Windows 10: CPU 1.5 GHz Dual-Core Memory (RAM) 1 GB without data acquisition, 2 GB with data acquisition Graphics/resolution Drive - Free disc space MB Connections 2 LAN, Wifi for download of installation data and device control When you are working with the chromatography software, disable the sleep function. Going to CHANGE ADVANCED POWER SETTINGS and DEVICE MANAGER, change the following settings to NEVER: Turn off the screen all hardware settings as hard drive, USB, netword adapter

12 Technical data 11 Hibernate mode In case hibernate mode is active during data collection, the run is interrupted and no more data is collected. Deactivate the option ALLOW THE COMPUTER TO TURN OFF THIS DEVICE TO SAVE POWER in the power management of the network adapter. The power management is customized by the network-adapter producer and can not always be changed. Set the WINDOWS UPDATES settings to manual. In case you allow automatic installation for WINDOWS UPDATES, the computer boots automatically. Booting interrupts data collection. Technical data For technical data about external devices, please refer to the website of the producer. Device Weight in kg Dimensions (W H D) in mm Solvent tray E 2.1L P 6.1L HPG P 6.1L LPG P6.1L isocratic AS 6.1L AS 6.1L cool/ heat version CT RID 2.1L UVD 2.1L DAD 6.1L DAD 2.1L MWD 2.1L ASM 2.1L about 14 (depending on configuration) V 2.1S (without valve) Power consumption in W

13 12 Checklist Checklist Transportation and storage There must be enough space available for storing the shipping pallet. HPLC System set-up A lab table with adequate carrying capacity and dimensions is available. The power supply and cable are available. The power supply and cable comply with the requirements. Ambient conditions at installation site The installation site complies with the requirements with respect to equipment, temperature, humidity, vibration and high frequency emissions. Computer and Operating System The computer complies with the requirements or is delivered by KNAUER.

14 Index A AC/DC switching power adapter 7 air humidity 4 ambient conditions 4 C checklist 12 computer requirements 8 D dimensions 11 drivers 10 E electromagnetic interference 7 H hibernate mode 11 HPLC systems 6 I individual devices 6 installation site 5 L line voltage 7 N network adapter 11 O operating environment 4 overview 4 P power disconnect 5 plug 5 power cable 7 Power connection 7 power consumption 11 power strip 7 R residual current 7 S shipping box 4 sleep 10 Index 13 software 10 Space requirements 4 space requirements 5 system layout 6 system set-up 4 T Technical Data 11 temperature range, storage temperature 4 U uninstalling 10 V voltage peaks 7 voltage supply 7 W weight 11 Windows Updates 11 AZURA Pre-Installation Guide, V6802

15 KNAUER manuals online: KNAUER 2017 KNAUER Wissenschaftliche Geräte GmbH Hegauer Weg Berlin Phone: Fax: Internet: