Operating manual Conductivity measuring cell to be installed in pipelines ba55321de02 10/2010
Copyright Weilheim 2010, WTW GmbH Reprinting - even as excerpts - is only allowed with the explicit written authorization of WTW GmbH, Weilheim. Printed in Germany. 20 ba55321de02 10/2010
Contents - Contents 1 General information............................... 22 2 Safety........................................... 23 2.1 Authorized use.................................... 23 2.2 General safety instructions........................... 24 3 Installation....................................... 25 3.1 General information................................. 25 3.2 Installation in stainless steel adapter.................... 25 3.2.1 Installation in EST-LRD weld-in socket........... 25 3.2.2 Installation in adaptor socket, ADA-3/4 NPT....... 26 3.2.3 Installation in adaptor socket, ADA-G 1 Zoll........ 27 3.3 Installation in plastic adaptor.......................... 28 3.3.1 Installation in glueing socket, ADA-LF-DN 20...... 28 3.3.2 Installation in ADA-LF-DN 20 glueing socket, using the ADA-DN 25... -DN 50 distance sleeves... 29 4 Maintenance, cleaning, disposal..................... 31 4.1 Aging of the measuring cell........................... 31 4.2 Cleaning......................................... 31 4.3 Disposal.......................................... 31 5 Recommended accessories......................... 32 6 What to do if....................................... 32 7 Technical data.................................... 33 ba55321de02 10/2010 21
General information 1 General information Structure of the -... 1 Cable with plug 2 Enclosure 3 Current electrode (ring, 2x) 4 Potential electrode (inside, 2x) 5 Temperature sensor in graphite enclosure The principle of the measurement method makes it possible to avoid influences from primary or secondary polarization effects, which ensures a high degree of measuring accuracy. A modern epoxy sealing technique reduces the chances of breakage of the sensor in the rough industrial environment. 22 ba55321de02 10/2010
Safety 2 Safety This operating manual contains basic instructions that you must follow during the commissioning, operation and maintenance of the measuring cell. Consequently, all responsible personnel must read this operating manual before working. The operating manual must always be available within the vicinity of the measuring cell. Target group Safety instructions The conductivity measuring cell was especially designed for the use in waste water treatment plants with heavily loaded waste water. Thus, we assume that the operators are familiar with the necessary precautions to take when dealing with chemicals as a result of their professional training and experience. Safety instructions in this operating manual can be recognized by the warning symbol (triangle) in the left column. The signal word (e. g. "CAUTION") indicates the level of the danger: Warning indicates instructions that must be followed precisely in order to prevent serious dangers to persons. CAUTION indicates instructions that must be followed precisely in order to avoid slight injuries or damage to the instrument or the environment. Other labels Note indicates notes that draw your attention to special features. Note indicates cross-references to other documents, e.g. operating manuals. 2.1 Authorized use The technical specifications as given in chapter 7 TECHNICAL DATA must be observed. Only the operation and running of the measuring cell according to the instructions given in this operating manual is authorized. Any other use is considered to be unauthorized. ba55321de02 10/2010 23
Safety 2.2 General safety instructions The conductivity measuring cell left the factory in a safe and secure technical condition. Function and operational safety The failure-free function and operational safety of the conductivity measuring cell is only guaranteed if the generally applicable safety measures and the special safety instructions in this operating manual are followed during its use. The smooth functioning and operational safety of the conductivity measuring cell can only be guaranteed under the environmental conditions that are specified in chapter 7 TECHNICAL DATA. The temperature range specified for using the conductivity measuring cell (chapter 7 TECHNICAL DATA) has to be observed. Protect the conductivity measuring cell, particularly against frost or overheating. 24 ba55321de02 10/2010
Installation 3 Installation 3.1 General information Warning Installation may only be carried out by trained specialists. Incorrect installation and its consequences are not covered by the manufacturer's warranty. Observe the local technical regulations for pressure vessels. 3.2 Installation in stainless steel adapter 3.2.1 Installation in EST-LRD weld-in socket Usage Weld-in socket (1.4571 stainless steel) to be welded into stainless steel pipes. EST-LRD Flow direction Welding the adapter Observe the following points: Because of the tapered NPT screw thread, the thread opening of the adaptor has to point outwards. Install the adaptor in such a way that the medium flows through the slot of the LDR 325 in the flow direction. CAUTION Only authorized specialists are allowed to weld the adaptor and cut pipes! ba55321de02 10/2010 25
Installation Screwing in the conductivity measuring cell 1 Wrap the thread of the with Teflon sealing tape. 2 Screw the measuring cell into the welded adaptor, EST-LRD. 3.2.2 Installation in adaptor socket, ADA-3/4 NPT Usage NPT adaptor socket (1.4571 stainless steel) to increase the 1/2" NPT thread of the to 3/4". ADA-3/4 NPT Installation 1 Wrap the thread of the with Teflon sealing tape. 2 Screw the adaptor on the thread of the measuring cell; the thread opening of the adaptor points upwards. 3 Tighten the adaptor using a size 24 mm fork wrench. 4 Screw the measuring cell with the adaptor into the corresponding pipe cutout. 26 ba55321de02 10/2010
Installation 3.2.3 Installation in adaptor socket, ADA-G 1 Zoll Usage Adaptor socket (1.4571 stainless steel) for installation in a 1" pipe thread. ADA-G 1 Zoll Installation 1 Wrap the thread of the with Teflon sealing tape. 2 Install the adaptor in the pipe thread up to the stop; the thread opening of the adaptor points upwards. 3 Tighten the adaptor using a size 41 mm fork wrench. 4 Screw in the measuring cell with the ADA-G 1 Zoll adaptor. ba55321de02 10/2010 27
Installation 3.3 Installation in plastic adaptor General information The plastic adaptor is glued into a PVC pipe, preferably into a 90 T-piece or 90 crosspiece. Note Before applying the PVC glue (e. g. Tangit, Henkel company) to the adaptor, thoroughly clean and degrease the contact surfaces. Allow the glue to harden according to the manufacturer's instructions. 3.3.1 Installation in glueing socket, ADA-LF-DN 20 Usage Socket (steel reinforced PVC) to be glued into PVC pipe ends with a nominal diameter of DN 20. ADA-LF-DN 20 DN 20 Installation 1 Apply glue around the front outside part of the ADA-LF-DN 20 glueing socket. 2 Insert the glueing socket into the T-piece up to the stop while slightly rotating it, so that the glue is distributed evenly between the contact surfaces. 3 Allow the glue to harden. 28 ba55321de02 10/2010
Installation 4 Wrap the thread of the with Teflon sealing tape. 5 Tightly screw the measuring cell into the glueing socket. 3.3.2 Installation in ADA-LF-DN 20 glueing socket, using the ADA-DN 25... -DN 50 distance sleeves Usage With the aid of the PVC distance sleeves, ADA-DN 25... ADA-DN 50, the ADA-LF-DN 20 glueing socket can be glued into pipe ends with a bigger nominal diameter. ADA-LF-DN 20 ADA-DN 32 (ADA-DN 25, ADA-DN 40, ADA-DN 50) Note All ADA-DN 25... ADA-DN 50 distance sleeves are installed according to the same principle. ba55321de02 10/2010 29
Installation Installing the glueing socket and distance sleeve. 1 Apply glue around the front outside part of the ADA-LF-DN 20 glueing socket. 2 Insert the glueing socket into the distance sleeve up to the stop while slightly rotating it, so that the glue is distributed evenly between the contact surfaces. 3 Allow the glue to harden. 4 Apply PVC glue around the front outside part of the distance sleeve. 5 Insert the distance sleeve into the T-piece up to the stop while slightly rotating it, so that the glue is distributed evenly between the contact surfaces. 6 Allow the glue to harden. 7 Wrap the thread of the with Teflon sealing tape. 8 Tightly screw the measuring cell into the glueing socket. 30 ba55321de02 10/2010
Maintenance, cleaning, disposal 4 Maintenance, cleaning, disposal Warning Contact with the sample can lead to danger to the user! Depending on the type of sample, suitable protective measures must be taken (protective clothing, protective goggles, etc.). CAUTION For all maintenance work, disconnect the conductivity measuring cell from the instrument! 4.1 Aging of the measuring cell Normally, the conductivity measuring cell does not age. Special measuring mediums (e.g. strong acids and bases, organic solvents) or temperatures that are too high may considerably reduce its lifetime or lead to damage. No warranty claims can be made for mechanical damage or any failure caused by these types of measuring mediums. 4.2 Cleaning CAUTION Especially before measuring low conductivity values, we recommend to clean the measuring cell thoroughly. Before measuring, thoroughly rinse the conductivity measuring cell with deionized water. Contamination Cleaning agents Reaction time at room temperature Water-soluble Deionized water Any substances Fats and oils Warm water and household dishwashing Any solution In the case of heavy Maximum of 5 minutes contamination: Methylated spirits Lime and hydroxide deposits Acetic acid (10 %) Any 4.3 Disposal We recommend to dispose of the measuring cell as electronic waste. ba55321de02 10/2010 31
Recommended accessories 5 Recommended accessories Stainless steel adaptor sockets Model Order no. EST-LRD 303209 ADA-3/4 NPT 303201 ADA-G 1 Zoll 303202 PVC glueing socket Model Order no. ADA-LF-DN 20 303203 PVC distance sleeves Model Order no. ADA-DN 25 303204 ADA-DN 32 303205 ADA-DN 40 303206 ADA-DN 50 303207 6 What to do if... Error symptom Cause Remedy No temperature displayed Measurement does not function Measurement provides implausible measured values Temperature sensor defective Return the conductivity measuring cell Conductivity measuring cell not connected Connect the conductivity measuring cell Instrument setting incorrect Correct instrument setting Conductivity measuring cell not connected Connect the conductivity measuring cell Instrument setting incorrect Correct the instrument setting Conductivity measuring cell not connected Conductivity measuring cell is heavily contaminated Connect the conductivity measuring cell Clean the conductivity measuring cell Cable or electrodes are damaged Return the conductivity measuring cell Instrument setting incorrect Correct the instrument setting Measuring range exceeded Select different measuring range 32 ba55321de02 10/2010
Technical data 7 Technical data General features Measuring principle Four-electrodes measurement Cell constant 0.475 cm -1 ±1.5 % Temperature sensor Integrated NTC 30 (30 k at 25 C / 77 F) Dimensions (in mm) Materials Enclosure Stainless steel 1.4571 Front part of the sensor Epoxy, black Conductivity electrodes Graphite Thermistor enclosure Graphite Cable screw joint Brass, nickel-plated Cable PUR Connection cable Lengths 1.5 m, 3 m and 7 m Diameter 8.8 mm Smallest allowed bend radius Fixed installation: 90 mm Flexible use: 180 mm Plug type Screw plug, 7 poles (IP 65) Pressure resistance (20 C / 68 F) Measuring cell: screw-in length Enclosure, cable screw joint, cable Cable plug IP 68 (10 6 Pa or 10 bar) IP 67 (2 x 10 5 Pa or 2 bar) IP 65 (when plugged in) ba55321de02 10/2010 33
Technical data The meets the requirements according to article 3(3) of the directive, 97/23/EC ("pressure equipment directive"). Measurement conditions Storage conditions Characteristic data on delivery Conductivity measuring range Temperature range Max. admissible overpressure Minimum depth of immersion Operating position Recommended storing method Storage temperature Temperature response behavior Precision of the temperature sensor 1 S/cm... 2 S/cm, Resolution corresponding to meter -5... 80 C (100 C) 23... 176 F (212 F) 10 6 Pa (10 bar) 36 mm Any In air 0... 50 C (32... 122 F) t 99 (99 % of the final value display after) <20s ± 0.2 K Wiring diagram Probe 7 pin plug with cable Shield Thermistor NTC Thermistor NTC Current electrode (ring) Potential electrode Potential electrode Current electrode (ring) 34 ba55321de02 10/2010
Technical data Pin assignment 3 4 2 7 5 1 6 Top view of the plug Pin Assignment Voltage Max. current 1 2 3 4 5 6 7 Potential electrode (u2) Potential electrode (u1) Current electrode (i1) Shield NTC (30 kohm) Current electrode (i2) NTC (30 kohm) < 1.3 V < 1.3 V < 1.3 V --- < 4.5 V < 1.3 V < 4.5 V < 0.5 ma < 0.5 ma < 0.5 ma --- < 0.5 ma < 0.5 ma < 0.5 ma CAUTION All voltages must be protective low voltages or safety extra low voltages without shock-hazard according to IEC 1010 or UL3101. All currents to the probe must not exceed 8 A even in case of a shortcircuit. ba55321de02 10/2010 35
Wissenschaftlich-Technische Werkstätten GmbH Dr.-Karl-Slevogt-Straße 1 D-82362 Weilheim Germany Tel: +49 (0) 881 183-0 +49 (0) 881 183-100 Fax: +49 (0) 881 183-420 E-Mail: Info@WTW.com Internet: http://www.wtw.com