EasyMax Product Catalog

EasyMax Product Catalog EasyMax Family EasyMax 102 Sets EasyMax 402 Sets Reactors Accessories Peripherals Software EasyMax Synthesis Workstations Complete More Successful Experiments

Table of Contents General Introduction 2 4 EasyMax 102 and 402 Basic and Advanced Standard Set 5 EasyMax Thermostat Systems 6 9 Optional Accessories for EasyMax 102 and 402 10 11 Temperature Sensors 12 Available Adapters 13 15 EasyMax 102 and 402 Reactors Overview 16 17 8 ml Glass Reactor Set 18 19 10 ml Glass Reactor Set 20 21 25 ml Glass Reactor Set 22 23 50 ml Glass Reactor Set 24 25 50 ml Glass Cover Set 26 29 5-Port 50 ml One-Piece Glass Reactor Set 30 33 100 ml Glass Reactor Set 34 35 100 ml Glass Reactor Set for EasyMax 402 36 37 100 ml High Workup Volume Glass Reactor Set 38 39 100 ml Glass Cover Set 40 43 100 ml PTFE Cover Set Standard Taper Joints 44 47 100 ml PTFE Cover Set for ParticleTrack and ReactIR 48 50 100 ml PTFE Cover Set for PVM V819, ParticleTrack, and ReactIR 51 53 5-Port 100 ml One-Piece Glass Reactor Set 54 57 400 ml Glass Reactor Set 58 59 400 ml Glass Cover Set 60 62 400 ml PTFE Cover Set 63 64 PTFE Lid Adapter Set for PTFE Covers 65 67 50 ml Pressure Reactor 68 70 2

Glossary of Terms Used 100 ml Pressure Reactors 71 73 50 ml and 100 ml Pressure Reactor Accessories 74 75 Overhead Stirrer Set 76 77 Overhead Stirrer Accessories 78 Magnetic Drive Sets 79 80 Magnetic Drive Accessories 81 83 Available Glass Stirrers 84 Available Stirrers Shafts 85 86 Available Stirrers Blades 87 88 Optional Accessories 89 Dosing Unit SP-50 Set 90 93 Dosing Unit SP-50 Syringes 94 3-Way Dosing Adapter Set 95 96 Accessories and Peripherals 97 99 Upgrade Kit EasyMax HFCal 100 101 Startet Kit EasyMax HFCal 102 EasyMax Basic Upgrade Sets 103 icontrol Software for EasyMax 104 Glossary of Terms Used ReactIR = Mid-IR spectroscopy ETFE = Ethylene tetrafluoroethylene FFKM = Perfluoro-elastomer FPM = Fluoro-elastomer PA = Polyamide ParticleTrack = FBRM technology PBT = Polybutylene terephthalate PE = Polyethylene PEEK = Polyetheretherketone PP = Polypropylene POM = Polyoxymethylene PTFE C25 PTFE GF25 PU PVC PVDF PVM SAN VQM = Polytetrafluoroethylene, 25% carbon = Polytetrafluoroethylene, 25% glass = Polyurethane = Polyvinylchloride = Polyvinylidene Fluoride = Particle Vision and Measurement = Styrene acrylonitrile = Silicone rubber 3

General Introduction EasyMax 102 and 402 Chemistry Made Easy Run reactions without an ice bath, oil bath, heating mantle or cryostat. Touch screen provides control of reaction parameters at all times, including changing preprogramed conditions when unattended. Explore new reaction conditions and innovative chemistry by setting temperature to any point from 40 C to 180 C. Interchangeable sleeves and reactors provide flexibility at volumes from 0.5 ml to 400 ml. Record all reaction conditions, making it easy to export data or repeat identical experiments. Incorporating Heat Flow Calorimetry into synthesis workstations allows scientists to perform safety screening. Optimal Usability EasyMax is a personal parallel synthesis workstation developed for organic chemists and engineers. It has two vessels that operate independently from each other. Because of the unique solid state thermostat principle, oil baths, ice baths and cryostats are not needed, control is done via an easy-to-use touchscreen which even allows for preprogramming and unattended execution of reaction steps Increase Your Application Range The EasyMax allows researchers to perform innovative chemistry or explore reaction conditions and by setting any temperature from 40 C to 180 C. Many reactors types can be chosen in the volume range from 0.5 ml to 400 ml. All important reaction data is displayed on the touch screen and optional data export is available after experiment are completed. Increased Personal Safety Personal safety is ensured by controlling all parameters via remote touchscreen without opening the hood. Active temperature control allows chemists to run exothermic reactions without significant temperature increase, and formation of unstable byproducts is avoided by holding temperature constant while dosing. Basic and Advanced Configurations With the Basic configuration, EasyMax 102 or 402 includes touchscreen control capabilities. Expanded functionality such as PC control, programmed task sequences, and software integration, are available with the Advanced configuration. Several software packages upgrade EasyMax 102/402 Basic to Advanced configurations. 4

EasyMax 102 and 402 Basic and Advanced EasyMax 102 and 402 Basic and Advanced EasyMax 102 Basic Ease-to-use Touchscreen control with basic functionalities 0.5 ml to 150 ml reaction volume 40 C to 180 C EasyMax 402 Basic Ease-to-use Touchscreen control with basic functionalities 15 ml to 400 ml reaction volume 40 C to 180 C EasyMax 102 Advanced Ease-to-use Touchscreen control with extended functionalities 0.5 ml to 150 ml reaction volume 40 C to 180 C icontrol Office License (one year) ic Data Center License (one year) EasyMax 402 Advanced Ease-to-use Touchscreen control with extended functionalities 15 ml to 400 ml reaction volume 40 C to 180 C icontrol Office License (one year) ic Data Center License (one year) 5

EasyMax Thermostat Systems EasyMax 102 Thermostat System Reactor zones with solid state thermostat technology Touchscreen eliminates training and learning curve Local data logging system for traceability and reproducibility 51161711 EasyMax thermostat system consisting of Order Number Product Description Quantity EasyMax 102 reactor block 1 51161873 EasyMax touchscreen 1 11132570 Protective cover for EasyMax touchscreen 1 51191728 Pen for EasyMax touchscreen 1 USB memory stick for data export 1 51161187 PVC industrial hose for coolant, 15 bar 2 51191125 PVC hose, soft, for reflux condenser 1 51161186 PVC hose for purge gas 1 51192239 PVC industrial hose for purge gas, 18 bar 1 51191916 Reducing connector for purge gas tubing 1 51190324 Quick connect coupling for purge gas inlet 3 51161827 Flowmeter set 1 51192126 Hose clamp for PVC tube 4 51191915 Flow indicator for coolant 1 EasyMax 102 reactor block Powder-coated stainless steel with FEP/PFA coated cover plate Heating/Cooling Solid state thermostat Temperature Mode Jacket control, reaction mixture control, distillation (constant or ramp) Temperature Range 40 C to 180 C, jacket temperature (Tj) Stirring Type Built-in magnetic and overhead stirring Stirring Speed 50 rpm to 1000 rpm 380 mm x 410 mm x 280 mm (w, d, h), 380 mm x 410 mm x 500 mm (w, d, h with overhead stirrer) Weight 16 kg, including touchscreen 6

EasyMax Thermostat Systems EasyMax 402 Thermostat System Reactor zones with solid state thermostat technology Touchscreen eliminates training and learning curve Local data logging system for traceability and reproducibility 30084210 EasyMax thermostat system consisting of Order number Product description Quantity EasyMax 402 reactor block 1 51161873 EasyMax touchscreen 1 11130821 Protective cover for EasyMax touchscreen 1 51191728 Pen for EasyMax touchscreen 1 USB memory stick for data export 1 51161187 PVC industrial hose for coolant, 15 bar 2 51191125 PVC hose, soft, for reflux condenser 1 51161186 PVC hose for purge gas 1 51192239 PVC industrial hose for purge gas, 18 bar 1 51191916 Reducing connector for purge gas tubing 1 51190324 Quick connect coupling for purge gas inlet 3 51161827 Flowmeter set 1 51192126 Hose clamp for PVC tube 4 51191915 Flow indicator for coolant 1 51191235 Identification clips for adhesive labels, 10 pcs in a set 1 EasyMax 402 reactor block Powder-coated stainless steel with FEP/PFA coated cover plate Heating/Cooling Solid state thermostat Temperature Mode Jacket control, reaction mixture control, distillation (constant or ramp) Temperature Range 40 C to 180 C, jacket temperature (Tj) Stirring Type Overhead stirring Stirring Speed 50 rpm to 1000 rpm 420 mm x 360 mm x 280 mm (w, d, h), 420 mm x 360 mm x 500 mm (w, d, h with overhead stirrer) Weight 20 kg, including touchscreen 7

EasyMax Thermostat Systems 51161883 EasyMax touchscreen PA, aluminum 195 mm x 135 mm x 60 mm (w, d, h) 11132570 Protective cover for EasyMax touchscreen Barex resin 51191728 Pen for EasyMax touchscreen Length 140 mm USB 2.0 memory stick for data export Memory 2 GB 55 mm x 15 mm x 6 mm available on special request only 51161187 PVC industrial hose for coolant PVC Pressure Range 15 bar Ø 8/14 mm, length 2.5 m available on special request only 51191125 PVC hose, soft, for reflux condenser PVC Ø 8/12 mm, length 5 m available on special request only 51161186 PVC hose for purge gas PVC Ø 4 mm, length 2 m available on special request only 51192239 PVC industrial hose for purge gas PVC Pressure Range 18 bar Ø 4/10 mm, length 2 m available on special request only 8

EasyMax Thermostat Systems 51191916 Reducing connector for purge gas tubing PP Temperature Max. 30 C For tubes with inner Ø 7 mm to 11 mm; 4 mm to 7 mm available on special request only 51161827 Flowmeter set for water and gas, including lab bar holder and water/gas inlet adapter Stainless steel, acrylic, brass Temperature Max. 65 C Quantity 1 gas flowmeter, 1 water flowmeter, 1 adapter for gas inlet Ø 4.8 mm 1/8 (for tubes inner Ø 4 mm), and 1 adapter for water inlet Ø 9.6 mm 1/4 (for tubes inner Ø 8/12mm) in a set 51190324 Quick connect coupling for purge gas inlet Stainless steel For tubes with inner Ø 4 mm 51192126 Hose clamp for PVC tube Stainless steel Ø 14 mm to 9.5 mm available on special request only 51191915 Flow indicator for coolant SAN Temperature Max. 30 C For tubes with inner Ø 6 mm to 9 mm available on special request only 9

Optional Accessories for EasyMax 102 and 402 Optional Accessories EasyMax 102 and 402 103472 Lab bar 300 x 14 mm Stainless steel, 1.4301 Ø 14 mm x 300 mm 51161099 Lab bar 600 x 14 mm Stainless steel, 1.4435 Ø 14 mm x 600 mm 51161803 Accessories holder set for two-piece reactor to be attached to the lab bar of the EasyMax system for stirrer motor (ST14), for condensor (ST14), for Tr sensor (ST10) Stainless steel, PTFE GF25 Aperture 2 x ST14, 1 x ST10 Quantity 2 pcs in a set 51161804 Accessories holder set for one-piece reactor to be attached to the lab bar of the EasyMax system for stirrer motor (ST19), for condensor (ST19), for Tr sensor (ST10) Stainless steel, PTFE GF25 Aperture 2 x ST19, 1 x ST10 Quantity 2 pcs in a set 30015271 Flowmeter for water Stainless steel, acrylic, brass Temperature Max. 65 C 100 mm, 0.8 L/min to 9 L/min 30015272 Flowmeter for gas Stainless steel, acrylic, brass Temperature Max. 65 C 100 mm, 1 L/min to 10 L/min 10

Optional Accessories for EasyMax 102 and 402 51161802 Bubble counter set Bubble counter glass (for tubes inner Ø 4 mm), magnetic holder, and gas regulation valve Ø 6 mm to 1.8 PET, borosilicate glass, PA Temperature 40 C to 180 C Quantity 2 of each in a set 51161778 Purge set SP-50 Quick connect coupling for purge gas inlet (for tubes inner Ø 4 mm), PVC tube for gas inlet (inner Ø 4 mm, length 2 m), reducing connector for purge gas tubing (for tubes inner Ø 7 mm to 11 mm and 4 mm to 7 mm) Stainless steel, PVC, PP Temperature PP max 30 C Quantity 1 of each in a set available as a set only Optional Accessories EasyMax 402 51162886 Accessories holder set to be attached to the lab bar of the EasyMax 402 system for stirrer motor (ST24), for Ø 12 mm probes (ST19), for Ø 6 mm probes (ST14) Stainless steel, PTFE GF25 Quantity 2 pcs in a set 11

Temperature Sensors Temperature Sensors EasyMax 102 and 402 51161730 Pt100 temperature sensor Stainless steel, FEP-coated Temperature Max. 200 C Sensor Ø 3.2 mm, length 175 mm Note: Use 51160200 adapter for ST7 port. Use 51161728 adapter for ST10 port. Use 30125685 adapter for ST14 port. Use 30125686 adapter for ST19 port. 30111612 Temperature sensor Stainless steel, FEP-coated Temperature Max. 200 C Sensor Ø 3.2 mm, length 250 mm Note: Use 51160200 adapter for ST7 port. Use 51161728 adapter for ST10 port. Use 30125685 adapter for ST14 port. Use 30125686 adapter for ST19 port. 30099798 Temperature sensor Glass Ø 6 mm, 260 mm Note: Use 51162720 adapter for ST14 port. Use 51162713 adapter for ST19 port. 30090590 Temperature sensor Alloy C-22 Ø 6.35 mm, 260 mm Note: Use 51162720 adapter for ST14 port. Use 51162713 adapter for ST19 port. 12

Available Adapters Available Adapters EasyMax 102 and 402 51161728 Adapter ST10/19 with 1 UNF 1/4 28 port PTFE GF25 UNF 1/4, inner Ø 3.2 mm 51191515 Nut for UNF 1/4 28 threads ETFE Inner Ø max. 3.2 mm Quantity 4 pcs in a set 51160200 Adapter ST7/16 with 1 UNF 1/4 28 port PTFE GF25 UNF 1/4, inner Ø 3.2 mm 51191514 Ferrule for tubing and sensors of outer Ø 3.2 mm Quantity ETFE Inner Ø max. 3.2 mm 4 pcs in a set 30125685 Adapter ST14/23 with 1 UNF 1/4 28 port PTFE 30125686 Adapter ST19/26 with 1 UNF 1/4 28 port PTFE 13

Available Adapters 51161821 Adapter PTFE for ParticleTrack probe, ST19/14 PTFE O-ring needed 51191857 Ø 14 mm 51191857 O-Ring for 51161821 ParticleTrack probe adapter FFKM Ø 13.95 mm x 2.62 mm, AS no. 113 51161817 Adapter PTFE for ReactIR probe, ST14-9.5mm PTFE O-ring needed 51192091 Ø 3/8 9.525 mm 51192091 O-Ring for 51161817 ReactIR probe adapter FFKM Ø 9.19 mm x 2.62 mm, AS no. 110 51161509 Adapter ST19/ST14 PTFE GF25 ST14, inner Ø 12 mm 14

Available Adapters 51162720 PTFE adapter, eccentric including 51162716 sealing ring PTFE GF25 Inner Ø 6 mm, ST14 Can also be used for Ø 1/4 6.35 mm inserts 51162716 Sealing ring for 51162720 and 51162713 PTFE adapters PTFE Inner Ø 6 mm Can also be used for Ø 1/4 6.35 mm inserts 51162713 PTFE adapter, eccentric including 51162716 sealing ring PTFE GF25 Inner Ø 6 mm, ST19 Can also be used for Ø 1/4 6.35 mm inserts 51162880 PTFE adapter, eccentric including 51162879 sealing ring PTFE GF25 Inner Ø 14 mm, ST14 51162879 Sealing ring for 51162880 PTFE adapter PTFE Inner Ø 14 mm 15

EasyMax 102 and 402 Reactors Overview 8 ml glass reactors with receptacle, Page 18 10 ml glass reactors with receptacle, Page 20 50 ml pressure reactor Page 68 25 ml glass reactors with receptacle Page 22 Receptacle for 50 ml reactor Page 24 and 68 50 ml glass reactor Page 24 Receptacle for 50 ml reactor Page 32 5-port 100 ml one-piece glass reactor Page 30 100 ml pressure reactor Page 71 50 ml glass cover Page 26 100 ml glass cover Page 40 Configure and Customize EasyMax Reactors The EasyMax 102 is designed to hold reactors and vials from 8 ml to 100 ml. 16 EasyMax 102

EasyMax 102 and 402 Reactors Overview 5-port 100 ml one-piece glass reactor Page 54 Receptacle for 100 ml reactor Page 36 Receptacle for 100 ml high workup volume reactor, page 38 400 ml glass reactor Page 58 100 ml glass reactor, page 34 100 ml high workup volume reactor, page 38 400 ml glass cover Page 60 400 ml PTFE cover Page 63 100 ml PTFE cover Standard taper joints Page 44 100 ml PTFE cover for ParticleTrack and ReactIR Page 48 100 ml PTFE cover for PVM V819, ParticleTrack and ReactIR, Page 51 The EasyMax 402 is designed to hold reactors from 100 ml to 400 ml. EasyMax 402 17

8 ml Glass Reactor Set EasyMax 8 ml Glass Reactor Set EasyMax 10 ml glass reactor set consisting of 30207789 8 ml glass reactor set The 8 ml reactor set provides the possibility to screen ten reactions from 0.5 ml to 8 ml scale in two different temperature zones. Order Number Product Description Quantity 30210021 Reagent vial with 14-425 thread, 8 ml, 100 pcs in a set 1 30210022 Screw cap, solid top with 14-425 thread, 100 pcs in a set 1 30133675 Receptacle for 5 x 8 ml reagent vials 1 51191324 Magnetic stir bar 4 18

8 ml Glass Reactor Set 30210021 Reagent vial with 14-425 thread, 8 ml Borosilicate glass Ø 16.2 mm, height 61 mm Quantity 100 pcs in a set 30210022 Screw cap, solid top with 14-425 thread Polypropylene, PTFE/Si Temperature Max. 180 C Quantity 100 pcs in a set 30133675 Receptacle 5 x 8 ml reagent vials thermostat sleeve Aluminium anodized 51191324 Magnetic stir bar PTFE-coated Ø 7 mm, length 10 mm 19

10 ml Glass Reactor Set EasyMax 10 ml Glass Reactor Set EasyMax 10 ml glass reactor set consisting of 51161714 10 ml glass reactor set The 10 ml reactor set provides the possibility to screen eight reactions from 1 ml to 5 ml scale in two different temperature zones. Order Number Product Description Quantity 51161285 Reagent tube, Ø 18 mm x 180 mm with GL18 thread, 10 pcs in a set 1 51161635 Receptacle for 4 x 10 ml reagent tubes 1 51191324 Magnetic stir bar 4 51191400 Screw cap GL18, with aperture, 10 pcs in a set 1 51191399 Septum-Set GL18, 10 pcs in a set 1 20

10 ml Glass Reactor Set 51161285 Reagent tube 10 ml with GL18 thread including GL18 screw cap with PTFE sealing Working Volume Quantity Borosilicate glass Max. 5 ml Ø 18 mm, height 180 mm 10 pcs in a set 51161635 Receptacle 4 x 10 ml reagent tubes thermostat sleeve Aluminium anodized 51191400 Screw cap GL18, with aperture PBT Temperature Max. 200 C Aperture Ø 11 mm Quantity 10 pcs in a set 51191399 Silicone rubber seal (septum) for use with screw cap GL18 Quantity Silicone rubber VQM Outer Ø 12 mm, thickness 2 mm 20 pcs in a set 51191324 Magnetic stir bar PTFE-coated Ø 7 mm, length 10 mm 21

25 ml Glass Reactor Set EasyMax 25 ml Glass Reactor Set EasyMax 25 ml glass reactor set for screening consisting of 51161854 25 ml glass reactor set for screening The 25 ml reactor provides the possibility to increase the screening functionality in six reactions from 3 ml to 25 ml in two different temperature zones. Order Number Product Description Quantity 51161853 Reagent tube 25 ml GL18, glass, 6 pcs in a set 1 51161634 Receptacle 3 x 25 ml, aluminium 1 51192096 Magnetic stir bar 5 mm x 15 mm 3 51191400 Screw cap GL18 6 51191399 Septum-Set GL18, 20 pcs in a set 1 22

25 ml Glass Reactor Set 51161853 Reagent tube 25 ml with GL18 thread Borosilicate glass Working Volume Max. 25 ml Outer Ø 22 mm, height 120 mm Quantity 6 pcs in a set 51161634 Receptacle 3 x 25 ml reagent tubes Thermostat sleeve Aluminium anodized 51191400 Screw cap GL18, with aperture PBT Temperature Max. 200 C Aperture Ø 11 mm Quantity 10 pcs in a set 51191399 Silicone rubber seal (septum) for use with screw cap GL18 Quantity Silicone rubber VQM Outer Ø 12 mm, thickness 2 mm 20 pcs in a set 51192096 Magnetic stir bar PTFE-coated Ø 5 mm, length 15 mm 23

50 ml Glass Reactor Set EasyMax 50 ml Glass Reactor Set 51161712 50 ml glass reactor set The 50 ml reactor set has a starting volume of 25 ml, Working Volume of 50 ml, and Nominal Volume of 70 ml for work up. Both magnetic and overhead stirring possibilities are available. EasyMax 50 ml glass reactor set consisting of A special sleeve with window provides visibility into the mixture. Order Number Product Description Quantity 51161255 50 ml round-bottom reactor 1 51161288 Reactor holder for 50 ml reactor 1 51161716 Receptacle for 50 ml reactor 1 51160675 Reactor clamp for 50 ml reactor 1 51161718 Fixing ring for receptacle 1 51191416 O-Ring for 50 ml glass reactor 1 51191919 Magnetic stir bar, cross-shaped 1 24

50 ml Glass Reactor Set 51161255 50 ml glass reactor Working Volume Borosilicate glass Max. 50 ml Temperature 40 C to 180 C Inner Ø 36 mm, height 74.5 mm, wall 1.5 mm 51161288 Reactor holder for 50 ml glass reactor or 50 ml glass cover PE 51161716 Receptacle for 50 ml reactor Thermostat sleeve Aluminium anodized 51160675 Reactor clamp for 50 ml reactor PTFE C25 51161718 Fixing ring for receptacle PTFE C25 51191416 O-Ring for 50 ml glass reactor FFKM Ø 36.14 mm x 2.62 mm, AS no. 127 51 191 919 Magnetic stir bar, cross-shaped PTFE-coated Ø 25 mm, height 10 mm 25

50 ml Glass Cover Set EasyMax 50 ml Glass Cover Set EasyMax 50 ml glass cover set consisting of 51161713 50 ml glass cover set The 50 ml glass cover set with six openings is built for multiple applications including dosing, reflux, ph measurement, ReactIR, or turbidity. Order Number Product Description Quantity 51160817 Glass cover for 50 ml reactor 1 51190878 Glass stopper ST14/23 1 51191167 Glass stopper ST10/19 2 51190877 Glass stopper ST7/16 1 51190879 Clamp ST7 1 51191505 Keck clamp ST14 1 51191504 Keck clamp ST10 2 51190318 Screw cap GL14, closed 2 51191170 Silicone rubber seal (septum) 1 51190317 Screw cap GL14, with aperture 5 51103947 Silicone rubber sealing ring, outer Ø 12 mm, aperture 6 mm 1 51191515 Nut for UNF 1/4 28 threads, 4 pcs in a set 1 51191514 Ferrule for tubing outer Ø 3.2 mm, 4 pcs in a set 1 51160200 Adapter ST 7/16 with 1 UNF 1/4 28 port 1 51190319 Plastic hose, straight 2 51161728 Adapter ST10/19 with 1 UNF 1/4 28 port 1 51191267 Glass adapter ST14/23 GL14 1 51160813 Reflux condenser for ST10 port 1 26

50 ml Glass Cover Set ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser ST14 ST10/19 ST14/23 Overhead stirrer ST10/19 Tr sensor, FEP-coated stainless steel Ø 3.2 mm ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser ST14 ST7/16 Tr sensor, dosing tubes 51160817 Glass cover for 50 ml reactor, 7 ports 1 x ST7/16, 2 x ST10/19, 2 x GL14, center ST14/23 Borosilicate glass Temperature 40 C to 180 C Inner Ø 36 mm 51190878 Glass stopper ST14/23 Glass 51191167 Glass stopper ST10/19 Glass 51190877 Glass stopper ST7/16 Glass 27

50 ml Glass Cover Set 51191505 Keck clamp ST14 POM 51191504 Keck clamp ST10 POM 51190879 Clamp ST7 Stainless steel 51191267 Glass adapter ST14/23-GL14 Glass Height 54 mm 51191515 Nut for UNF 1/4 28 threads ETFE Inner Ø max. 3.2 mm Quantity 4 pcs in a set 51191514 Ferrule for tubing and sensors of outer Ø 3.2 mm Quantity ETFE Inner Ø max. 3.2 mm 4 pcs in a set 51190318 Screw cap GL14, closed with PTFE sealing PBT Temperature Max. 200 C 51191170 Silicone rubber seal (septum) for screw cap GL14 Silicone rubber VQM Ø 12 mm, thickness 2 mm 28

50 ml Glass Cover Set 51190317 Screw cap GL14, with aperture PBT Temperature Max. 200 C Aperture Ø 9.5 mm 51103947 Silicone rubber sealing ring with vulcanized-on PTFE washers for GL14 caps and sensors with outer Ø 6 mm Silicone rubber VQM, PTFE-coated Ø 12 mm, aperture 6 mm 51161728 Adapter ST10/19 with 1 UNF 1/4 28 port PTFE GF25 UNF 1/4, inner Ø 3.2 mm 51160200 Adapter ST7/16 with 1 UNF 1/4 28 port PTFE GF25 UNF 1/4, inner Ø 3.2 mm 51190319 Plastic hose, straight with silicone rubber seal, for screw cap GL14 PP, VQM For tube inner Ø 6 mm to 9 mm 51160813 Reflux condenser for ST10 port with GL14 connectors for coolant and septum Borosilicate glass 29

5-Port 50 ml One-Piece Glass Reactor Set 5-Port 50 ml One-Piece Glass Reactor Set 51161838 5-port 50 ml one-piece glass reactor set The one piece reactor meets round bottom flask requirements so that standard lab material and handling can be used. The reactor has a starting volume of 10 ml, maximum Working Volume of 50 ml and a Nominal Volume of 100 ml. Magnetic and overhead stirring (only with dedicated glass stirrer and blade) are available. EasyMax 5-port 50 ml one-piece glass reactor set consisting of Order Number Product Description Quantity 51161792 5-port 50 ml one-piece glass reactor 1 51161813 Glass stirrer shaft for 50 ml one-piece reactor 1 51161814 Half-moon stirrer blade 1 51190791 Magnetic stir bar 13 x 30 mm 1 51161816 Reactor holder for 50 ml reactor 1 51161815 Reducing part for 50 ml 1 51161822 Non-height adjustable stirrer adapter, ST19, including sealing ring 1 71517 Glass stopper ST19/26 3 51190878 Glass stopper ST14/23 1 51191167 Glass stopper ST10 1 51191429 Keck clamp ST19 3 51191505 Keck clamp ST14 1 51191504 Keck clamp ST10 1 51191515 Nut for UNF 1/4 28, 4 pcs in a set 1 51191514 Ferrule for tubing and sensors of outer Ø 3.2 mm, 4 pcs in a set 1 51161728 Adapter ST10/19 with 1 UNF 1/4 28 1 30

5-Port 50 ml One-Piece Glass Reactor Set ST19/26 ParticleTrack probe S/G400 Ø 14 mm ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser ST14 ST19/26 ParticleTrack probe S/G400 Ø 14 mm ST19/26 Overhead stirrer ST10/19 Tr sensor, FEP-coated stainless steel Ø 3.2 mm 51161792 50 ml one-piece glass reactor, 5-ports 1 x ST10/19, 1 x ST14/23, 2 x ST19/26, center ST19/26 Glass Working Volume Max. 50 ml Temperature 40 C to 180 C inner Ø 43 mm, height 150 mm, wall 2.5 mm 51161813 Glass stirrer shaft for 100/50 ml one-piece reactor Glass Ø 8 mm, length 192 mm 51161814 Half-moon stirrer blade PTFE 15 mm x 26 mm 51161816 Reactor holder for 50 ml reactor PE 31

5-Port 50 ml One-Piece Glass Reactor Set 51161815 Receptacle for 50 ml reactor Thermostat sleeve Aluminium anodized 51190791 Magnetic stir bar 13 x 30 mm PTFE-coated Ø 13 mm x 30 mm *Note: Certain solvents like Methylene-chloride, DMSO, and THF may cause swelling in PEEK. We recommend to use the optional PTFE stirrer adapter 51161835 (see page 78) as an alternative to avoid breakage of the glass port. 51161822 Non-height adjustable stirrer adapter* ST19, including sealing ring PEEK adapter, PTFE/FPM sealing ring Available only as a set with sealing ring 51191375 51191375 Sealing ring for stirrer adapter BOLA-sealing PTFE/FPM 71517 Glass stopper ST19/26 Glass 51190878 Glass stopper ST14/23 Glass 51191167 Glass stopper ST10/19 Glass 32

5-Port 50 ml One-Piece Glass Reactor Set 51191429 Keck clamp ST19 POM 51191505 Keck clamp ST14 POM 51191504 Keck clamp ST10 POM 51191515 Nut for UNF 1/4 28 thread ETFE Inner Ø max. 3.2 mm Quantity 4 pcs in a set 51191514 Ferrule for tubing and sensors of outer Ø 3.2 mm Quantity ETFE Inner Ø max. 3.2 mm 4 pcs in a set 51161728 Adapter ST10/19 with 1 UNF 1/4 28 port PTFE GF25 UNF 1/4, inner Ø 3.2 mm 33

100 ml Glass Reactor Set EasyMax 100 ml Glass Reactor Set 51161708 100 ml glass reactor set The 100 ml reactor set has a starting volume of 15 ml, Working Volume of 100 ml and Nominal Volume of 150 ml for work up. EasyMax 100 ml glass reactor set consisting of Both magnetic and overhead stirring possibilities are available. Order Number Product Description Quantity 51161620 100 ml glass reactor 1 51161676 Reactor holder for 100 ml reactor 1 51191913 O-ring for 100 ml reactor 1 51161670 Clamp chain for 100 ml reactor 1 51191918 Magnetic stir bar, cross-shaped 1 34

100 ml Glass Reactor Set 51161620 100 ml glass reactor EasyMax Borosilicate glass Working Volume Max. 100 ml Temperature 40 C to 180 C Inner Ø 52 mm, height 90 mm, wall 2.5 mm 51161676 Reactor holder for 100 ml reactor PE 51191913 O-ring for 100 ml reactor Silicone rubber VQM, FEP-coated Temperature 60 C to 200 C Ø 56.82 mm x 2.62 mm; AS no. 140 51161670 Clamp chain for 100 ml reactor Stainless steel 1.4404, Glastherm HT 220 (Thermalite 220M) Note: A reactor cover is required: 51161709 6-port 100 ml glass cover set For details see page 40. 51191918 Magnetic stir bar, cross-shaped PTFE-coated Ø 38 mm x 15 mm 51161800 6-port PTFE cover set with standard tapered joints for 100 ml reactor. For details see page 44. 30090541 6-port PTFE cover set with compression fittings and standard tapered joints for 100 ml reactor. For details see page 48. 30090542 6-port PTFE cover set with compression fittings, standard tapered joints and 19 mm bore for 100 ml reactor For details see page 51. 35

100 ml Glass Reactor Set for EasyMax 402 100 ml Glass Reactor Set For EasyMax 402 30125690 100 ml glass reactor set The 100 ml reactor set has a starting volume of 15 ml, Working Volume of 100 ml and Nominal Volume of 150 ml for work up. EasyMax 100 ml glass reactor set consisting of Both magnetic and overhead stirring possibilities are available. Order Number Product Description Quantity 51161620 100 ml glass reactor 1 51161676 Reactor holder for 100 ml reactor 1 51191913 O-ring for 100 ml reactor 1 51161670 Clamp chain for 100 ml reactor 1 30086802 EasyMax 402 receptacle for 100 ml reactor 1 36

100 ml Glass Reactor Set for EasyMax 402 51161620 100 ml glass reactor EasyMax Borosilicate glass Working Volume Max. 100 ml Temperature 40 C to 180 C Inner Ø 52 mm, height 90 mm, wall 2.5 mm 51161676 Reactor holder for 100 ml reactor PE 51191913 O-ring for 100 ml reactor Silicone rubber VQM, FEP-coated Temperature 60 C to 200 C Ø 56.82 mm x 2.62 mm; AS no. 140 51161670 Clamp chain for 100 ml reactor Stainless steel 1.4404, Glastherm HT 220 (Thermalite 220M) Note: A reactor cover is required: 51161709 6-port 100 ml glass cover set For details see page 40. 30086802 EasyMax 402 receptacle for 100 ml reactor Thermostat sleeve Aluminium anodized 51161800 6-port PTFE cover set with standard tapered joints for 100 ml reactor. For details see page 44. 30090541 6-port PTFE cover set with compression fittings and standard tapered joints for 100 ml reactor. For details see page 48. 30090542 6-port PTFE cover set with compression fittings, standard tapered joints and 19 mm bore for 100 ml reactor For details see page 51. 37

100 ml High Workup Volume Glass Reactor Set EasyMax 100 ml High Workup Volume Glass Reactor Set 30111633 100 ml high workup volume glass reactor set The 100 ml high workup volume reactor set has a starting volume of 15 ml, Working Volume of 100 ml and Nominal Volume of 200 ml for work up. Both magnetic and overhead stirring possibilities are available. EasyMax 100 ml high workup volume glass reactor set consisting of Order Number Product Description Quantity 30111634 100 ml high workup volume glass reactor 1 51161676 Reactor holder for 100 ml reactor 1 51191913 O-ring for 100 ml reactor 1 51161670 Clamp chain for 100 ml reactor 1 51191918 Magnetic stir bar, cross-shaped 1 30111636 EasyMax 402 receptacle for 100 ml high workup volume reactor 1 38

100 ml High Workup Volume Glass Reactor Set 30111634 100 ml high workup volume glass reactor Borosilicate glass Working Volume Max. 100 ml Temperature 40 C to 180 C Inner Ø 52 mm, height 103 mm, wall 2.5 mm 51161676 Reactor holder for 100 ml reactor PE 51191913 O-ring for 100 ml reactor Silicone rubber VQM, FEP-coated Temperature 60 C to 200 C Ø 56.82 mm x 2.62 mm; AS no. 140 51161670 Clamp chain for 100 ml reactor Stainless steel 1.4404, Glastherm HT 220 (Thermalite 220M) Note: A reactor cover is required: 51161709 6-port 100 ml glass cover set For details see page 40. 51191918 Magnetic stir bar, cross-shaped PTFE-coated Ø 38 mm x 15 mm 51161800 6-port PTFE cover set with standard tapered joints for 100 ml reactor. For details see page 44. 30090541 6-port PTFE cover set with compression fittings and standard tapered joints for 100 ml reactor. For details see page 48. 30090542 6-port PTFE cover set with compression fittings, standard tapered joints and 19 mm bore for 100 ml reactor For details see page 51. 30111636 EasyMax 402 receptacle for 100 ml high workup volume reactor Thermostat sleeve Aluminium anodized 39

100 ml Glass Cover Set EasyMax 100 ml Glass Cover Set 51161709 6-port 100 ml glass cover set The 100 ml glass cover set with six ports is built for multiple applications without limitations for dosing, reflux, ph measurement, ReactIR, or turbidity. EasyMax 100 ml glass cover set consisting of The set includes all adapters, stoppers, and clamps needed for full operation. Order Number Product Description Quantity 51161619 6-port 100 ml glass reactor cover 1 51190878 Glass stopper ST14/23 4 51191167 Glass stopper ST10/19 2 51191505 Keck clamp ST14 4 51191504 Keck clamp ST10 2 51191515 Nut for UNF 1/4 28, 4 pcs in a set 1 51191514 Ferrule for tubing and sensors of outer Ø 3.2 mm, 4 pcs in a set 1 51161728 Adapter ST 10/19 with 1 UNF 1/4 28 port 2 51191428 Hose connection for purge gas tubing 2 51190317 Screw cap GL14, with aperture 2 51190319 Plastic hose, straight 2 51161029 Reflux condenser for ST14/23 port 1 40

100 ml Glass Cover Set ST10/19 Tr sensor, FEP-coated stainless steel Ø 3.2 mm ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser ST14 ST14/23 Overhead stirrer ST10/19 Tr sensor, FEP-coated stainless steel Ø 3.2 mm ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser ST14 ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser ST14 51161619 Glass cover for 100 ml reactor, 6 ports 2 x ST10/9, 3 x ST14/23, center ST14/23 Borosilicate glass Temperature 40 C to 180 C Inner Ø 52 mm 51190878 Glass stopper ST14/23 Glass 51191167 Glass stopper ST10/19 Glass 41

100 ml Glass Cover Set 51191505 Keck clamp ST14 POM 51191504 Keck clamp ST10 POM 51191515 Nut for UNF 1/4 28 threads ETFE Inner Ø max. 3.2 mm Quantity 4 pcs in a set 51191514 Ferrule for tubing and sensors of outer Ø 3.2 mm Quantity ETFE Inner Ø max. 3.2 mm 4 pcs in a set 51161728 Adapter ST10/19 with 1 UNF 1/4 28 port PTFE GF25 UNF 1/4, inner Ø 3.2 mm 51191428 Hose connection for purge gas tubing PP For tube inner Ø 4 mm 42

100 ml Glass Cover Set 51190317 Screw cap GL14, with aperture PBT Temperature Max. 200 C Aperture Ø 9.5 mm 51190319 Plastic hose, straight with silicone rubber seal, for screw cap GL14 PP, VQM For tube inner Ø 6 mm to 9 mm 51161029 Reflux condenser for ST14/23 port with 2 GL14 connectors for coolant Borosilicate glass Outer Ø 24 mm, height 140 mm 43

100 ml PTFE Cover Set Standard Taper Joints EasyMax 100 ml PTFE Cover Set Standard Taper Joints 51161800 6-port PTFE cover set with standard tapered joints for 100 ml reactor This version of a PTFE cover is equipped with a series of standard taper joints in order to accommodate standard ST adapters and lab equipment. EasyMax 100 ml PTFE cover set consisting of The PTFE cover can be used in combination with the standard O-rings and reactor clamp as used for the glass cover. Order Number Product Description Quantity 51161795 6-port PTFE cover for 100 ml reactor body (works only with the 50 ml stirrer shaft 51161756) 1 51191167 Glass stopper ST10/19 1 51190878 Glass stopper ST14/23 3 71517 Glass stopper ST19/26 2 51161821 Adapter PTFE for ParticleTrack probe, ST19/14 1 51191857 O-Ring FFKM 13.95 mm x 2.62 mm 1 51161817 Adapter PTFE for ReactIR probe, ST14-9.5mm 1 51192091 O-Ring FFKM 9.19 mm x 2.62 mm 1 51191515 Nut for UNF 1/4 28, 4 pcs in a set 1 51191514 Ferrule for tubing and sensors of outer Ø 3.2 mm, 4 pcs in a set 1 51161728 Adapter ST10/19 with 1 UNF 1/4 28 port 2 51190878 Glass stopper ST14/23 3 51190317 Screw cap GL14, with aperture 2 51190319 Plastic hose, straight 2 51161029 Reflux condenser for ST14/23 port 1 44

100 ml PTFE Cover Set Standard Taper Joints This PTFE reactor cover is an extremely robust alternative for the standard glass covers. It is the perfect choice if the reactor is equipped with heavy inserts and probes which bear the risk of breaking the glass version of the cover. The cover is mainly used to run crystallization experiments. Special care needs to be taken when the cover is used for reflux experiments since absolute solvent tightness cannot be guaranteed under all circumstances. Alternative 100 ml PTFE covers can be found on page 48 & 51. ST19/26 ParticleTrack probe S/G400 Ø 14 mm ST10/19 Tr sensor, FEP-coated stainless steel Ø 3.2 mm ST14/23 Overhead stirrer ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser ST14 ST19/26 ParticleTrack probe S/G400 Ø 14 mm ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser ST14 51161795 PTFE cover for 100 ml reactor, 6 ports 1 x ST10/9, 2 x ST14/23, 2 x ST19/26, center ST14/23 PTFE GF25 works only with the 50 ml stirrer shaft 51161756 71517 Glass stopper ST19/26 Glass 51190878 Glass stopper ST14/23 Glass 51191167 Glass stopper ST10/19 Glass 45

100 ml PTFE Cover Set Standard Taper Joints 51161821 Adapter PTFE for ParticleTrack probe, ST19/14 PTFE O-ring needed 51191857 Ø 14 mm 51191857 O-Ring for 51161821 ParticleTrack probe adapter FFKM Ø 13.95 mm x 2.62 mm, AS no. 113 51161817 Adapter PTFE for ReactIR probe, ST14-9.5mm PTFE O-ring needed 51192091 Ø 3/8 9.5 mm 51192091 O-Ring for 51161817 ReactIR probe adapter FFKM Ø 9.19 mm x 2.62 mm, AS no. 110 51191515 Nut for UNF 1/4 28 threads ETFE Inner Ø max. 3.2 mm Quantity 4 pcs in a set 51191514 Ferrule for tubing and sensors of outer Ø 3.2 mm Quantity ETFE Inner Ø max. 3.2 mm 4 pcs in a set 46

100 ml PTFE Cover Set Standard Taper Joints 51161728 Adapter ST10/19 with 1 UNF 1/4 28 port PTFE GF25 UNF 1/4, inner Ø 3.2 mm 51190317 Screw cap GL14, with aperture PBT Temperature Max. 200 C Aperture Ø 9.5 mm 51190319 Plastic hose, straight with silicone rubber seal, for screw cap GL14 PP, VQM For tube inner Ø 6 mm to 9 mm 51161029 Reflux condenser for ST14/23 port with 2 GL14 connectors for coolant Borosilicate glass Outer Ø 24 mm, height 140 mm 47

100 ml PTFE Cover Set for ParticleTrack and ReactIR EasyMax 100 ml PTFE Cover Set For ParticleTrack and ReactIR 30090541 6-port PTFE cover set with compression fittings and standard tapered joints for 100 ml reactor This cover is designed to be used in combination with METTLER TOLEDOs ReactIR and ParticleTrack probes up to 14 mm in diameter. The adapters with compression fittings are perfectly suited to hold the various probes and insert in an ideal and secure position. EasyMax 100 ml PTFE cover set consisting of The PTFE cover comes as full set with all the required adapters to accommodate typical combinations of probes and inserts. The cover can be used in combination with the standard O-rings and reactor clamp as used for the glass cover. Order Number Product Description Quantity PTFE cover for 100 ml reactor, 6 ports 1 Standard stirrer adapter, ST14/35 with 3/8 NPT 1 PC701.050.14 1/2 NPT x Ø 14 mm compression fitting 1 PC703.14 Sealing plug for Ø 14 mm compression fitting 1 PC701.050.375 1/2 NPT x Ø 3/8 9.525 mm compression fitting 1 PC703.375 Sealing plug for Ø 3/8 compression fitting 1 PC701.050.250 1/2 NPT x Ø 1/4 6.35 mm compression fitting 1 PC703.250 Sealing plug for Ø 1/4 compression fitting 1 PC711.1913 ST19/38 fitting x 1/2 NPT 2 Note: All the contained threaded adapters are standard parts from COWIE. In case replacement or additional adapters are required, please refer to www.cowie.com. All the COWIE part numbers are indicated with a PC as prefix. 48

100 ml PTFE Cover Set for ParticleTrack and ReactIR This PTFE reactor cover is an extremely robust alternative for the standard glass covers. It is the perfect choice if the reactor is equipped with heavy inserts and probes which bear the risk of breaking the glass version of the cover. The cover is mainly used to run crystallization experiments. Special care needs to be taken when the cover is used for reflux experiments since absolute solvent tightness cannot be guaranteed under all circumstances. Alternative 100 ml PTFE covers can be found on page 51. 1/2 NPT ParticleTrack probe S/G400 probe Ø 14 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm ST10/19 Tr sensor, FEP-coated stainless steel, Ø 3.2 mm ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser ST14 3/8 NPT Overhead stirrer 1/2 NPT ParticleTrack probe S/G400 probe Ø 14 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser ST14 PTFE cover for 100 ml reactor, 6 ports 1 x ST10, 2 x ST14, 2 x 1/2 NPT, center 3/8 NPT PTFE Standard stirrer adapter ST14/35 with 3/8 NPT PTFE Inner Ø 14 mm, 3/8 NPT, height 62 mm PC701.050.14 1/2 NPT x 14 mm compression fitting PTFE, PEEK Inner Ø 14 mm, 1/2 NPT Sealing plug needed PC703.14 PC703.14 Sealing plug for Ø 14 mm compression fitting PTFE 49

100 ml PTFE Cover Set for ParticleTrack and ReactIR PC701.050.375 1/2 NPT x 3/8 compression fitting PTFE, PEEK Inner Ø 3/8 9.525 mm, 1/2 NPT Sealing plug needed PC703.375 PC703.375 Sealing plug for Ø 3/8 compression fitting PTFE PC701.050.250 1/2 NPT x 1/4 compression fitting PTFE, PEEK Inner Ø 1/4 6.35 mm, 1/2 NPT Sealing plug needed PC703.250 PC703.250 Sealing plug for Ø 1/4 compression fitting PTFE PC711.1913 ST19/38 fitting x 1/2 NPT PTFE Inner Ø 15 mm, 1/2 NPT, height 50 mm 50

100 ml PTFE Cover Set for PVM V819 EasyMax 100 ml PTFE Cover Set For PVM V819, ParticleTrack, and ReactIR 30090542 6-port PTFE cover set with compression fittings, standard tapered joints and 19 mm bore for 100 ml reactor This cover is designed to be used in combination with METTLER TOLEDOs ReactIR and ParticleTrack probes up to 14 mm in diameter as well as the PVM V819 probe with 19 mm in diameter. The adapters with compression fittings are perfectly suited to hold the various probes and insert in an ideal and secure position. EasyMax 100 ml PTFE cover set consisting of The PTFE cover comes as full set with all the required adapters to accommodate typical combinations of probes and inserts. The cover can be used in combination with the standard O-rings and reactor clamp as used for the glass cover. Order Number Product Description Quantity PTFE cover for 100 ml reactor, 6 ports 1 Standard stirrer adapter, ST14/35 with 3/8 NPT 1 PC701.050.14 1/2 NPT x 14 mm compression fitting 1 PC703.14 Sealing plug for Ø 14 mm compression fitting 1 010.03.19 Number 19 flask stopper for 19.25 mm port 1 7451 PTFE sleeves for 19.25 mm port 10 Note: All the contained threaded adapters are standard parts from COWIE. In case replacement or additional adapters are required, please refer to www.cowie.com. All the COWIE part numbers are indicated with a PC as prefix. 51

100 ml PTFE Cover Set for PVM V819 This PTFE reactor cover is an extremely robust alternative for the standard glass covers. It is the perfect choice if the reactor is equipped with heavy inserts and probes which bear the risk of breaking the glass version of the cover. The cover is mainly used to run crystallization experiments. Special care needs to be taken when the cover is used for reflux experiments since absolute solvent tightness cannot be guaranteed under all circumstances. 1/2 NPT ParticleTrack probe S/G400 probe Ø 14 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm ST10/19 Tr sensor, FEP-coated stainless steel Ø 3.2 mm ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser St14 3/8 NPT Overhead stirrer 19.25 mm PVM V819 Ø 19.25 mm ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser St14 PTFE cover for 100 ml reactor, 6 ports 1 x ST10, 2 x ST14, 1 x 1/2 NPT, 1 x 19.25 mm, center 3/8 NPT PTFE Standard stirrer adapter ST14/35 with 3/8 NPT PTFE Inner Ø 14 mm, 3/8 NPT, height 62 mm PC701.050.14 1/2 NPT x 14 mm compression fitting PTFE, PEEK Inner Ø 14 mm, 1/2 NPT Sealing plug needed PC703.14 PC703.14 Sealing plug for Ø 14 mm compression fitting PTFE 52

100 ml PTFE Cover Set for PVM V819 010.03.19 Number 19 flask stopper for 19.25 mm port PTFE 7451 PTFE sleeve for 19.25 mm port PTFE 53

5-Port 100 ml One-Piece Glass Reactor Set 5-Port 100 ml One-Piece Glass Reactor Set 51161805 5-port 100 ml one-piece glass reactor set The one-piece reactor is developed to meet round bottom flask requirements so that standard lab material and handling can be used. The reactor has a starting volume of 15 ml, maximum working volume of 100 ml and a Nominal Volume of 180 ml. Magnetic and overhead stirring (only with dedicated glass stirrer and blade) possibilities are available. The ST14 port can be used for inserting analytical probes EasyMax 5-port 100 ml one-piece glass reactor set consisting of Order Number Product Description Quantity 51161786 5-port 100 ml one-piece glass reactor 1 51161676 Reactor holder for 100 ml reactor 1 51161813 Glass stirrer shaft for 100 ml one-piece reactor 1 51161749 Half-moon stirrer blade 1 51161822 Non-height adjustable stirrer adapter, ST19, including sealing ring 1 71517 Glass stopper ST19/26 3 51190878 Glass stopper ST14/23 1 51191167 Glass stopper ST10/19 1 51191515 Nut for UNF 1/4 28, 4 pcs in a set 1 51191514 Ferrule for tubing and sensors of outer Ø 3.2 mm, 4 pcs in a set 1 51191429 Keck clamp ST19 3 51191505 Keck clamp ST14 1 51191504 Keck clamp ST10 1 51161728 Adapter ST10/19 with 1 UNF 1/4 28 port 1 51191939 Magnetic stir bar 8 mm x 40 mm 1 54

5-Port 100 ml One-Piece Glass Reactor Set ST19/26 ParticleTrack probe S/G400 Ø 14 mm ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser ST14 ST19/26 ParticleTrack probe S/G400 Ø 14 mm ST19/26 Overhead stirrer ST10/19 Tr sensor, FEP-coated stainless steel Ø 3.2 mm 51161786 100 ml one-piece glass reactor, 5 ports 1x ST10/19, 1x ST14/23, 2x ST19/26, center ST19/26 Borosilicate glass Working Volume Max. 180 ml Temperature 40 C to 180 C Inner Ø 52 mm, height 150 mm, wall 2.5 mm 51161813 Glass stirrer shaft for 100/50 ml one-piece reactor Borosilicate glass Ø 8 mm, length 192 mm 51161749 Half-moon stirrer blade PTFE 15 mm x 40 mm 51161676 Reactor holder for 100 ml reactor PE 55

EasyMax 5-Port 100 ml One-Piece Glass Reactor Set *Note: Certain solvents like Methylene-chloride, DMSO, and THF may cause swelling in PEEK. We recommend to use the optional PTFE stirrer adapter 51161835 (see page 78) as an alternative to avoid breakage of the glass port. 51161822 Non-height adjustable stirrer adapter* ST19, including sealing ring PEEK adapter, PTFE/FPM sealing ring Available only as a set with sealing ring 51191375 51191375 Sealing ring for stirrer adapter BOLA-sealing PTFE/FPM 71517 Glass stopper ST19/26 Glass 51190878 Glass stopper ST14/23 Glass 51191167 Glass stopper ST10/19 Glass 51191515 Nut for UNF 1/4 28 threads ETFE Inner Ø max. 3.2 mm Quantity 4 pcs in a set 51191514 Ferrule for tubing and sensors of outer Ø 3.2 mm ETFE Inner Ø max. 3.2 mm Quantity 4 pcs in a set 56

EasyMax 5-Port 100 ml One-Piece Glass Reactor Set 51191429 Keck clamp ST19 POM 51191505 Keck clamp ST14 POM 51191504 Keck clamp ST10 POM 51161728 Adapter ST10/19 with 1 UNF 1/4 28 port PTFE GF25 UNF 1/4, inner Ø 3.2 mm 51191939 Magnetic stir bar 8 mm x 40 mm PTFE-coated Ø 8 mm, length 40 mm 57

400 ml Glass Reactor Set 400 ml Glass Reactor Set For EasyMax 402 30111619 400 ml glass reactor set The 400 ml reactor set has a starting volume of 75 ml, Working Volume of 400 ml and Nominal Volume of 425 ml for work up. EasyMax 400 ml glass reactor set consisting of Overhead stirring possibilities are available. Order Number Product Description Quantity 30072099 400 ml glass reactor 1 51162759 Reactor holder for 400 ml reactor 1 51191335 O-ring for 400 ml reactor 1 30111610 Clamp chain for 100 ml reactor 1 30125685 Adapter ST14/23 with 1 UNF 1/4 28 port 1 58

400 ml Glass Reactor Set 30072099 400 ml glass reactor EasyMax Borosilicate glass Working Volume Max. 400 ml Temperature 40 C to 180 C Inner Ø 67 mm, height 140 mm 51162759 Reactor holder for 400 ml reactor PE 51191335 O-ring for 400 ml reactor Silicone rubber VQM, FEP-coated Temperature 60 C to 200 C Ø 82 mm x 2.62 mm 30111610 Clamp chain for 100 ml reactor Stainless steel 1.4404, Glastherm HT 220 (Thermalite 220M) Note: A reactor cover is required: 30111632 6-port 400 ml glass cover set For details see page 60. 30125685 Adapter ST14/23 with 1 UNF 1/4 28 port PTFE 30111620 6-port PTFE cover set with compression fittings for 400 ml reactor. For details see page 63. 59

400 ml Glass Cover Set 400 ml Glass Cover Set For EasyMax 402 30111632 400 ml glass cover set The 400 ml glass cover set with 6 ports is built for multiple applications like dosing or ph measurement. The set includes all stoppers and clamps needed for normal operation. EasyMax 400 ml glass cover set consisting of Order Number Product Description Quantity 51161072 6-port 400 ml glass cover 1 71517 Glass stopper ST19/26 2 51190878 Glass stopper ST14/23 4 51191429 Keck clamp ST19 2 51191505 Keck clamp ST14 4 30125685 Adapter ST14/23 with 1 UNF 1/4 28 port 1 60

400 ml Glass Cover Set ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser ST14 ST19/26 ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST14/23 Overhead stirrer ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser ST14 ST14/23 ph electrode Ø 6 mm, turbidity probe Ø 6 mm, ReactIR Ø 1/4 6.35 mm, ReactIR Ø 3/8 9.525 mm, dropping funnel ST14, reflux condenser ST14 ST19/26 ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm 51161072 Glass cover for 400 ml reactor, 6 ports 3 x ST14/23, 2 x ST19/26, center ST14/23 Borosilicate glass Temperature 40 C to 180 C Inner Ø 67 mm 71517 Glass stopper ST19/26 Glass 51190878 Glass stopper ST14/23 Glass 61

400 ml Glass Cover Set 51191429 Keck clamp ST19 POM 51191505 Keck clamp ST14 POM 30125685 Adapter ST14/23 with 1 UNF 1/4 28 port PTFE 62

400 ml PTFE Cover Set 400 ml PTFE Cover Set For EasyMax 402 30111620 6-port PTFE cover set with standard NS19/38 fittings for 400 ml reactor This cover is designed for normal use and use with probes up to 14 mm in diameter 400 ml PTFE cover set consisting of The PTFE cover set comes with standard ST19 adapters to accommodate standard applications. The cover can be used with the same clamp and O-ring as used with the glass cover. Order Number Product Description Quantity PTFE cover for 400 ml reactor, 6 ports 1 Standard stirrer adapter, ST14/35 with 3/8 NPT 1 PC711.1913 ST19/38 fitting x 1/2 NPT 2 PC711.1919 ST19/38 fitting x 3/4 NPT 3 30125686 Adapter ST19/26 with 1 UNF 1/4 28 port 1 Note: All the contained threaded adapters are standard parts from COWIE. In case replacement or additional adapters are required, please refer to www.cowie.com. All the COWIE part numbers are indicated with a PC as prefix. This PTFE reactor cover is an extremely robust alternative for the standard glass covers. It is the perfect choice if the reactor is equipped with heavy inserts and probes which bear the risk of breaking the glass version of the cover. The cover is mainly used to run crystallization experiments. Special care needs to be taken when the cover is used for reflux experiments since absolute solvent tightness cannot be guaranteed under all circumstances. 63

400 ml PTFE Cover Set ST19/38 ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST19/38 ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST19/38 ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm 3/8 NPT Overhead stirrer ST19/38 ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST19/38 ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm PTFE cover for 100 ml reactor, 6 ports 3 x ST19/38 with 1/2 NPT, 2 x ST19/38 with 3/4 NPT, center 3/8 NPT PTFE Standard stirrer adapter ST14/35 with 3/8 NPT PTFE Inner Ø 14 mm, 3/8 NPT, height 62 mm PC711.1913 ST19/38 fitting x 1/2 NPT PTFE Inner Ø 15.2 mm, 1/2 NPT PC711.1919 ST19/38 fitting x 3/4 NPT PTFE Inner Ø 15.2 mm, 3/4 NPT 30125686 Adapter ST19/26 with 1 UNF 1/4 28 port PTFE 64

PTFE Lid Adapter Set for PTFE Covers PTFE Lid Adapter Set For EasyMax 102 and 402 PTFE Covers 30138934 Adapter set for PTFE covers The adapter set contains adapters that can be used with the EasyMax PTFE covers (30111620, 30090541, 30090542) for various applications like IR, FBRM, ph, dosing and temperature measurement. Adapter set consisting of Order Number Product Description Quantity PC701.050.125 1/2 NPT x Ø 1/8 3.175 mm compression fitting 2 PC703.125 Sealing plug for Ø 1/8 compression fitting 2 PC701.050.06 1/2 NPT x Ø 6 mm compression fitting 1 PC703.06 Sealing plug for Ø 6 mm compression fitting 1 PC701.050.250 1/2 NPT x Ø 1/4 6.35 mm compression fitting 1 PC703.250 Sealing plug for Ø 1/4 compression fitting 1 PC701.050.375 1/2 NPT x Ø 3/8 9.525 mm compression fitting 1 PC703.375 Sealing plug for Ø 3/8 compression fitting 1 PC701.050.14 1/2 NPT x Ø 14 mm compression fitting 1 PC703.14 Sealing plug for Ø 14 mm compression fitting 1 Note: All the contained threaded adapters are standard parts from COWIE. In case replacement or additional adapters are required, please refer to www.cowie.com. All the COWIE part numbers are indicated with a PC as prefix. 65

PTFE Lid Adapter Set for PTFE Covers PC701.050.125 1/2 NPT x Ø 1/8 3.175 mm compression fitting PTFE, PEEK Sealing plug needed PC703.125 Inner Ø 1/8 3.175 mm, 1/2 NPT PC703.125 Sealing plug for Ø 1/8 compression fitting PTFE PC701.050.06 1/2 NPT x Ø 6 mm compression fitting PTFE, PEEK Sealing plug needed PC703.06 Inner Ø 6 mm, 1/2 NPT PC703.06 Sealing plug for Ø 6 mm compression fitting PTFE PC701.050.250 1/2 NPT x Ø 1/4 6.35 mm compression fitting PTFE, PEEK Sealing plug needed PC703.250 Inner Ø 1/4 6.35 mm, 1/2 NPT PC703.250 Sealing plug for Ø 1/4 compression fitting PTFE 66

PTFE Lid Adapter Set for PTFE Covers PC701.050.375 1/2 NPT x Ø 3/8 9.525 mm compression fitting PTFE, PEEK Sealing plug needed PC703.375 Inner Ø 3/8 9.525 mm, 1/2 NPT PC703.375 Sealing plug for Ø 3/8 compression fitting PTFE PC701.050.14 1/2 NPT x Ø 14 mm compression fitting PTFE, PEEK Sealing plug needed PC703.14 Inner Ø 14 mm, 1/2 NPT PC703.14 Sealing plug for Ø 14 mm compression fitting PTFE Adapters applicable for Order Number Product Description Applicable for PC701.050.125 1/2 NPT x Ø 1/8 3.175 mm compression fitting Tr sensor FEP coated 3.2 mm, dosing tube 3.2 mm PC701.050.06 1/2 NPT x Ø 6 mm compression fitting Calibration heater, Tr sensor glass 6 mm, ph sensor PC701.050.250 1/2 NPT x Ø 1/4 6.35 mm compression fitting ReactIR calibration heater 1/4 6.35mm, Tr sensor Alloy C-22 1/4 6.35mm PC701.050.375 1/2 NPT x Ø 3/8 9.525 mm compression fitting ReactIR probe 3/8, ParticleTrack probe 3/8 PC701.050.14 1/2 NPT x Ø 14 mm compression fitting ParticleTrack probe 14 mm 67

50 ml Pressure Reactor EasyMax 50 ml Pressure Reactor Set 51161870 EasyMax 50 ml pressure reactor set The pressure reactor is for applications which need pressures from 0 bar to 200 bar abs. EasyMax 50 ml pressure reactor set consisting of The Alloy C-22 material allows customers to work with aggresive media. The reactor has a Working Volume between 25 ml and 50 ml, and a Nominal Volume up to 60 ml. Order Number Product Description Quantity Pressure reactor complete, 200 bar 1 51161875 Tr sensor for pressure reactor 1 Receptacle for 50 ml pressure reactor 1 51161718 Fixing ring for receptacle 1 51191452 O-ring for 50 ml reactor, FFKM 1 51191587 Gassing stirrer, Ø 18 mm with 4 grooves at gas entrainment impeller, Alloy C-22 1 51191331 Rupture disc, 200 bar, Alloy C-276 1 51161009 Flexible spiral tube, Ø 2 mm, stainless steel 1 51191348 Needle valve, 1/8 3.175 mm, Alloy C-22, Swagelok part in stainless steel 1 68

50 ml Pressure Reactor 51161875 Tr sensor for pressure reactor Stainless steel no direct contact with the reaction media Outer Ø 2.2 mm Receptacle for 50 ml reactor Thermostat sleeve Aluminium anodized only available in the set 51 161 718 Fixing ring for receptacle PTFE C25 51 191 452 O-Ring for 50 ml reactor FFKM Ø 31.42 mm x 2.62 mm, AS no. 124 51 191 587 Gassing stirrer with 4 grooves at gas entrainment impeller Alloy C-22 Ø 18 mm 51 191 331 Rupture disc for the 50 ml reactor Alloy C-276 Pressure Range 0 bar to 200 bar abs. ± 10% 51 161 009 Flexible spiral tube Stainless steel Inner Ø 2 mm 51 191 348 Needle valve Alloy C-22, Swagelok part in stainless steel 1/8 3.175 mm Note: All the external connectors and fittings are Swagelok compatible. 69

50 ml Pressure Reactor Accessories 50 ml Pressure Reactor Optional Accessories and Upgrade Set 51191588 Gassing stirrer with four grooves at gas entrainment impeller Alloy C-22 Ø 25 mm 51192161 Rupture disc for the 50 ml reactor Alloy C-276 Pressure Range 0 bar to 15 bar abs. ± 10% 51161876 EasyMax 50 ml pressure reactor upgrade set Pressure reactor upgrade set to upgrade a current MultiMax pressure reactor to an EasyMax pressure reactor. The set contains overhead stirrer motor, Tr probe, receptacle, and fixing ring. EasyMax 50 ml pressure reactor upgrade set consisting of Order Number Product Description Quantity 51161830 EasyMax stirrer motor without coupling 1 51161875 Tr sensor for pressure reactor 1 Receptacle for 50 ml pressure reactor, only available in the set 1 51161718 Fixing ring for receptacle 1 70

100 ml Pressure Reactor 100 ml Pressure Reactor Sets EM20-100-HC and EM60-100-HC 30030945 EM20-100-HC pressure reactor set The pressure reactor is for applications which need pressures from 0 up to 20 bar abs. 30030946 EM60-100-HC pressure reactor set The pressure reactor is for applications which need pressures from 0 up to 60 bar abs. EasyMax 100 ml pressure reactor sets consisting of The Alloy C-22 material allows customers to work with aggresive media. Both reactors have a Working Volume between 30 ml and 100 ml, and a nominal volume of 120 ml. Order Number EM20-100-HC pressure reactor set EM60-100-HC pressure reactor set Quantity Pressure reactor complete 1 51161875 Tr sensor for pressure reactor 1 30030952 O-ring for 100 ml reactor, FFKM 1 30030950 Gassing stirrer, Ø 30 mm, Alloy C-22 1 30030947 Rupture disc, 25 bar, Alloy C-276 1 Analog pressure gauge, 40 bar 1 30030948 Rupture disc, 65 bar, Alloy C-276 1 Analog pressure gauge, 100 bar 1 71

100 ml Pressure Reactor 51 161 875 Tr sensor for pressure reactor Stainless steel no direct contact with the reaction media Outer Ø 2.2 mm 30 030 952 O-Ring for 100 ml reactor FFKM Ø 50.47 mm x 2.62 mm 30 030 950 Gassing stirrer with 4 grooves at gas entrainment impeller Alloy C-22 Ø 30 mm 30 030 947 Rupture disc, 25 bar standard for the EM20-100-HC reactor Alloy C-276 Pressure Range 0 bar to 25 bar abs. ± 10% 30 030 948 Rupture disc, 65 bar standard for the EM60-100-HC reactor Alloy C-276 Pressure Range 0 bar to 65 bar abs. ± 10% Note: All the external connectors and fittings are Swagelok compatible. 100 ml Pressure Reactor Optional Accessories 30030950 Gassing stirrer with four grooves at gas entrainment impeller Alloy C-22 Ø 30 mm 30030951 Pitched-blade stirrer downwards, four impellers Alloy C-22 Ø 30 mm 72

100 ml Pressure Reactor Accessories 100 ml Pressure Reactor Optional Accessories 51192161 Rupture disc, 15 bar Alloy C-276 Pressure Range 0 bar to 15 bar abs. ± 10% 30030949 Rupture disc, 110 bar Alloy C-276 Pressure Range 0 bar to 110 bar abs. ± 10% 14474703 HP reactor fiber probe adapter kit for 1/4 6.35 mm fiber probe, includes extension tube 14474701 and adapter 14474406 Alloy C-22 Pressure Range 0 bar to 60 bar abs. ± 10% 14474704 HP reactor fiber probe adapter kit for 3/8 9.525 mm fiber probe, includes extension tube 14474701 and adapter 14474404 Alloy C-22 Pressure Range 0 bar to 60 bar abs. ± 10% 14474700 HP reactor port extension tube allows connection of a 1/4 or 3/8 high pressure adapter Stainless steel Pressure Range 0 bar to 60 bar abs. ± 10% 14474701 HP reactor port extension tube allows connection of a 1/4 or 3/8 high pressure adapter Alloy C-22 Pressure Range 0 bar to 60 bar abs. ± 10% 14474706 HP reactor fiber probe adapter for 1/4 6.35 mm fiber probe Alloy C-22 Pressure Range 0 bar to 60 bar abs. ± 10% 14474704 HP reactor fiber probe adapter for 3/8 9.525 mm fiber probe Alloy C-22 Pressure Range 0 bar to 60 bar abs. ± 10% 73

50 ml and 100 ml Pressure Reactor Accessories 100 ml Pressure Reactor Optional Accessories 30132810 Baffle for the 100 ml pressure reactor Alloy C-22 Outer Ø 45 mm, height 70 mm 30138105 Dip tube for Tr sensor Alloy C-22 Outer Ø 6 mm, height 75 mm 50 ml and 100 ml Pressure Reactor Optional Accessories 51191811 Digital manometer LEO 3, 30 bar Alloy C-276 Pressure Range 0 bar to 30 bar abs. ± 10% Resolution 10 mbar 51191349 Digital manometer LEO 3, 300 bar Alloy C-276 Pressure Range 0 bar to 300 bar abs. ± 10% Resolution 100 mbar 51161310 Analog cable to connect digital manometer to the UCB Position In inputs of the Universal Control Box, UCB 51161586 Analog cable to connect digital manometer to the UCB Position C In inputs of the Universal Control Box, UCB Note: To connect the digital manometer to the pressure reactor, the Swagelok spare parts set 51191707 is required. 74

50 ml and 100 ml Pressure Reactor Toolbox 50 ml and 100 ml Pressure Reactor Optional Accessories 51104377 Analog cable with integrated current supply for stand-alone connection of digital manometers Position In inputs of the Universal Control Box, UCB 50 ml and 100 ml Pressure Reactor Toolbox Toolbox consisting of 51161410 Toolbox Toolbox for the 100 ml and 50 ml pressure reactors. It contains a 12 mm hexagonal socket wrench and replacement parts. Order Number Product Description Quantity Toolbox, including a 12 mm hexagonal socket wrench 1 51191343 Friction bearing TK25, set of 4 pcs 1 51191344 Ball bearing, stainless steel, set of 4 pcs 1 51191347 Replacement cone 1/8 for needle valve, Alloy C-22, set of 2 pcs 1 51191388 Thrust disk TK25, set of 2 pcs 1 51191389 Grub screw M4x4 for stirrer, Alloy C-22, set of 2 pcs 1 51191390 Spacer sleeve for driven shaft, Alloy C-22, Ø 8/6 mm x 3 mm, set of 4 pcs 1 Front ferrule 2 mm, Swagelok, stainless steel, set of 4 pcs 1 Rear ferrule 2 mm, Swagelok, stainless steel, set of 4 pcs 1 30030952 O-ring, FFKM, Ø 50.47 mm x 2.62 mm 1 75

Overhead Stirrer Set EasyMax Overhead Stirrer Set EasyMax overhead stirrer set consisting of 51161700 Overhead stirrer set The overhead stirrer set with speed range from 50 rpm to 1000 rpm. The patented height adjustment allows the blade to be positioned at five different depths depending on the application need. Order Number Product Description Quantity 51161719 EasyMax stirrer motor with coupling 1 51161654 Height adjustment unit for stirrer adapter, incl. O-ring 1 51161731 Stirrer adapter ST14/23 1 51191375 Sealing ring for stirrer adapter (1 piece already fitted) 2 51161651 Chuck, PTFE C25 1 51161652 Clamping nut 1 51191376 Washer for stirrer adapter 2 76

Overhead Stirrer Set 51161719 EasyMax stirrer motor with coupling Aluminum anodized (flange), stainless steel (upper coupling) Speed 50 rpm to 1000 rpm 51161654 Height adjustment unit for stirrer adapter upper part for height adjustment, incl. O-ring PEEK available on special request only 51161731 Stirrer adapter ST14/23, lower part PEEK available on special request only 51191375 Sealing ring for stirrer adapter PTFE/FPM Ø 16 mm, thickness 5 mm, aperture 8 mm 51161652 Clamping nut Aluminum anodized 51161651 Chuck, PTFE C25 for stirrer shafts with outer Ø 8 mm PTFE C25 51191376 Washer for stirrer adapter PA Ø 16 mm, aperture 8 mm, thickness 2 mm 77

Overhead Stirrer Accessories EasyMax Overhead Stirrer Optional Accessories 51161830 EasyMax stirrer motor without coupling Stainless steel Speed 50 rpm to 1000 rpm 51161360 Set of upper stirrer coupling comprising upper coupling and 2 threaded pins Stainless steel, 1.4301 available on special request only 71652 O-ring for stirrer adapter FPM 21.89 mm x 2.62 mm, AS no. 118 Optional PTFE Stirrer Adapter For the 50 ml, 100 ml and 400 ml Reactors 51161835 PTFE stirrer adapter Certain solvents like Methylene-chloride, DMSO, and THF may cause swelling in PEEK. We recommend the use of this optional PTFE stirrer adapter as an alternative to the PEEK stirrer adapter 51161822 to avoid breakage of the glass port. 51161835 Non-height adjustable PTFE stirrer adapter with metal brace, ST19, including sealing ring Aluminium anodized with PTFE adapter, PTFE/FPM sealing ring Available only as a set with sealing ring 51191375 78

Magnetic Drive Sets EasyMax Overhead Stirrer Magnetic Drive Sets 30213866 Magnetic drive set for two-piece reactor for 50 ml of wetted parts Speed Alloy C-22, FFKM, PTFE C25 Stirrer shaft length 94 mm, stirrer blade outer Ø 25 mm 50 rpm to 1000 rpm 30213865 Magnetic drive set for one-piece reactor for 50 ml of wetted parts Speed Alloy C-22, FFKM, PTFE, PTFE C25, PTFE GF25 (adapter) Stirrer shaft length 83 mm, half-moon stirrer blade 15 mm x 26 mm, adapter ST19/ST14 50 rpm to 1000 rpm 30113925 Magnetic drive set for two-piece reactor for 100 ml of wetted Alloy C-22, FFKM, PTFE C25 parts Stirrer shaft length 129 mm, stirrer blade outer Ø 25 mm Speed 50 rpm to 1000 rpm 30113924 Magnetic drive set for one-piece reactor for 100 ml of wetted parts Speed Alloy C-22, FFKM, PTFE, PTFE C25, PTFE GF25 (adapter) Stirrer shaft length 118 mm, half-moon stirrer blade 15 mm x 40 mm, adapter ST19/ST14 50 rpm to 1000 rpm 79

Magnetic Drive Sets 30130319 Magnetic drive set for two-piece reactor for 400 ml of wetted parts Speed Alloy C-22, FFKM, PTFE C25 Stirrer shaft length 184 mm, stirrer blade outer Ø 25 mm 50 rpm to 1000 rpm 30125692 Magnetic drive set for one-piece reactor for 400 ml of wetted parts Speed Alloy C-22, FFKM, PTFE, PTFE C25, PTFE GF25 (adapter) Stirrer shaft length 165 mm, half-moon stirrer blade 15 mm x 40 mm, adapter ST19/ST14 50 rpm to 1000 rpm EasyMax Overhead Stirrer Magnetic Drive Upgrade Set 30092602 Magnetic drive upgrade set To upgrade an existing stirrer motor set-up. Available without stirrer motor (51161830). Stirrer shafts must be purchased separately. 30092602 Magnetic drive upgrade set magnetic coupling 20 Ncm ST14 of wetted Alloy C-22, FFKM, PTFE C25 parts Speed 50 rpm to 1000 rpm 80

Magnetic Drive Accessories EasyMax Magnetic Drive Accessories 51161830 EasyMax stirrer motor without coupling Stainless steel Speed 50 rpm to 1000 rpm 30130411 Driven Shaft for the magnetic drive Alloy C-22 Ø 6 mm x 125 mm 30138112 Magnet 20 Ncm without grub screw Alloy C-22 Ø 11.6 mm x 33.5 mm 51191214 O-ring (inside housing) FFKM Ø 23.4 mm x 3.53 mm 30092600 O-ring for ST14 part, upper FFKM Ø 10.82 mm x 1.78 mm 30092479 O-ring for ST14 part, lower FFKM Ø 9.25 mm x 1.78 mm 81

Magnetic Drive Accessories 51191388 Thrust disk for driven shaft PTFE/carbon Ø 11.5 mm x 1.2 mm Quantity 2 pcs in a set 51191343 Friction bearing driven shaft PTFE C25 Ø 12 mm x 6 mm Quantity 4 pcs in a set 30130576 Screw D11-M3 for half-moon blades Alloy C-22 Ø 11 mm x M3 30138089 Grub screw M4x3 Alloy C-22 M4 x 3 mm 82

Magnetic Drive Accessories EasyMax Magnetic Drive Optional Accessories 51191344 Ball bearing driven shaft Stainless steel Ø 12 mm x 3 mm Quantity 4 pcs in a set 51191390 Spacer sleeve driven shaft Alloy C-22 Ø 8 mm x 3 mm Quantity 4 pcs in a set 83

Available Glass Stirrers Available Glass Stirrers 100 ml and 400 ml Reactors 51161725 Pitched-blade stirrer upward, three impellers, 45, for 100 ml EasyMax reactor Glass Outer Ø 30 mm, length 261 mm 30111637 Pitched-blade stirrer upward, three impellers, 45, for 400 ml EasyMax reactor Glass Outer Ø 30 mm, length 298 mm 51161726 Pitched-blade stirrer downward, three impellers, 45, for 100 ml EasyMax reactor Glass Outer Ø 30 mm, length 261 mm 30111638 Pitched-blade stirrer downward, three impellers, 45, for 400 ml EasyMax reactor Glass Outer Ø 30 mm, length 298 mm 51161727 Anchor stirrer for 100 ml EasyMax reactor Glass Outer Ø 48 mm, height 55 mm, length 261 mm 30111639 Anchor stirrer for 400 ml EasyMax reactor Glass Outer Ø 65 mm, height 75 mm, length 298 mm 84

Available Stirrers Shafts Available Stirrer Shafts 50 ml, 100 ml and 400 ml Reactors 51161756 Stirrer shaft, length 218 mm Two-piece reactor, 50 ml Alloy C-22 Outer Ø 8/6 mm, length 218 mm 30130412 Stirrer shaft for magnetic drive Two-piece reactor, 50 ml Alloy C-22 Outer Ø 9.5/8 mm, length 94 mm 51161723 Stirrer shaft, length 258 mm Two-piece reactor, 100 ml Alloy C-22 Ø 8 mm, length 258 mm 30130575 Stirrer shaft for magnetic drive Two-piece reactor, 100 ml Alloy C-22 Outer Ø 9.5/8 mm, length 129 mm 30111611 Stirrer shaft, length 298 mm Two-piece reactor, 400 ml Alloy C-22 Ø 8 mm, length 298 mm 30138114 Stirrer shaft for magnetic drive Two-piece reactor, 400 ml Alloy C-22 Outer Ø 9.5/8 mm, length 184 mm 85

Available Stirrers Shafts 30130577 Stirrer shaft for magnetic drive One-piece reactor, 50 ml Alloy C-22 Outer Ø 9.5/8 mm, length 83 mm 30130413 Stirrer shaft for magnetic drive One-piece reactor, 100 ml Alloy C-22 Outer Ø 9.5/8 mm, length 118 mm 51161813 Glass stirrer shaft for 50/100 ml one-piece reactor Borosilicate glass Ø 8 mm, length 192 mm 30138113 Stirrer shaft for magnetic drive One-piece reactor, 400 ml Alloy C-22 Outer Ø 9.5/8 mm, length 165 mm 30111614 Glass stirrer shaft for 400 ml one-piece reactor Borosilicate glass Ø 8 mm, length 242 mm 86

Available Stirrers Blades Available Stirrer Blades 50 ml, 100 ml and 400 ml Reactors 51161356 Pitched-blade element upward, four impellers, 45, for 50 ml and 100 ml EasyMax reactors Alloy C-22 Outer Ø 25 mm 51161549 Pitched-blade element downward, four impellers, 45, for 50 ml and 100 ml EasyMax reactors Alloy C-22 Outer Ø 25 mm 51162442 Pitched-blade element upward, four impellers, 45, for 100 ml EasyMax reactor Alloy C-22 Outer Ø 38 mm 51162418 Pitched-blade element downward, four impellers, 45, for 100 ml EasyMax reactor Alloy C-22 Outer Ø 38 mm 30111616 Pitched-blade element upward, four impellers, 45, for 100 ml and 400 ml EasyMax reactors Alloy C-22 Outer Ø 38 mm 30111615 Pitched-blade element downward, four impellers, 45, for 100 ml and 400 ml EasyMax reactors Alloy C-22 Outer Ø 38 mm 87

Available Stirrers Blades 51161364 Rushton turbine blade for 50 ml and 100 ml EasyMax reactors Alloy C-22 Outer Ø 25 mm 51161724 Anchor blade for 100 ml EasyMax reactor Alloy C-22 Outer Ø 48 mm, height 55 mm 30111617 Anchor blade for 400 ml EasyMax reactor Alloy C-22 Outer Ø 65 mm, height 75 mm 51161814 Half-moon stirrer blade one-piece reactor, 50 ml PTFE 15 mm x 26 mm 51161749 Half-moon stirrer blade one-piece reactor, 100 ml PTFE 15 mm x 40 mm 51162684 Half-moon stirrer blade one-piece reactor, 400 ml PTFE 15 mm x 43 mm 51162683 Half-moon stirrer blade one-piece reactor, 400 ml PTFE 15 mm x 54 mm 88

Optional Accessories EasyMax Optional Accessories A variety of optional accessories expand the functionality of EasyMax. A number of spare parts and consumables are also available. 51191267 Glass adapter ST14/23-GL14 Glass Height 54 mm 51160827 Adapter ST14/23 to ST10/19 PTFE GF25 Height 30 mm 51190317 Screw cap GL14, with aperture PBT Temperature Max. 200 C Aperture Ø 9.5 mm 51161102 Silicone rubber sealing ring with vulcanized-on PTFE washers for GL14 caps and sensors with outer Ø 8 mm Silicone rubber VQM, PTFE-coated Ø 12 mm x 5 mm 51161547 Set of knurled screws with washers for 50 ml reactor clamp Stainless steel Quantity 8 pcs of each 89

Dosing Unit SP-50 Set Dosing Unit SP-50 Set 51161770 Dosing unit SP-50 set This unit allows the dosing of one reagent in two reactors completely independent and in parallel via touchscreen or PC software. Dosing unit SP-50 set consisting of Only available in the set. Order Number Product Description Quantity Dosing Unit SP-50, only available in the set 1 51191988 CAN cable 100 cm 1 51191306 PTFE dosing tube Ø 3.2 mm 3 51191304 PTFE dosing tube Ø 1.6 mm 2 51191515 Nut for UNF 1/4 28 threads, outer Ø max. 3.2 mm, 4 pcs in a set 1 51191514 Ferrule for tubing and sensors of outer Ø 3.2 mm, 4 pcs in a set 1 51191204 Plug for UNF 1/4 28 threads, 4 pcs in a set 1 51191203 Nut for UNF 1/4 28 threads, outer Ø max. 1.6 mm, 4 pcs in a set 1 51191202 Ferrule for tubing and sensors of outer Ø 1.6 mm, 4 pcs in a set 1 51191267 Glass adapter ST14/23-GL14 2 51190318 Screw cap GL14, closed 3 51191170 Silicone rubber seal (septum) 1 51191591 Bottle GL45 250 ml 1 51191972 Distributor cap GL45 2 x GL14 1 51161558 Adapter GL14-UNF 3 51190317 Screw cap GL14, with aperture 3 51103947 Silicone rubber sealing ring, outer Ø 12 mm, aperture 6 mm 6 51191687 Assorted heat-shrink tubings, 8 pcs in a set 1 51710710 EasyMax operating instructions 1 EasyMax factory test report 1 90

Dosing Unit SP-50 Set only available in the set Dosing unit SP-50 51191988 CAN cable 100 cm length 100 cm 51191306 PTFE dosing tube Ø 3.2 mm PTFE Ø 3.2 mm, length 2.5 m 51191304 PTFE dosing tube Ø 1.6 mm PTFE Ø 1.6 mm, length 2.5 m 51191515 Nut for UNF 1/4 28 threads ETFE Inner Ø max. 3.2 mm Quantity 4 pcs in a set 51191514 Ferrule for tubing and sensors of outer Ø 3.2 mm Quantity ETFE Inner Ø max. 3.2 mm 4 pcs in a set 51191204 Plug for UNF 1/4 28 threads ETFE Outer Ø max. 1.6 mm Quantity 4 pcs in a set 91

Dosing Unit SP-50 Set 51191203 Nut for UNF 1/4 28 threads ETFE Inner Ø max. 1.6 mm Quantity 4 pcs in a set 51191202 Ferrule for tubing and sensors of outer Ø 1.6 mm Quantity ETFE Inner Ø max. 1.6 mm 4 pcs in a set 51191267 Glass adapter ST14/23-GL14 Glass Height 54 mm 51190318 Screw cap GL14, closed with PTFE sealing PBT Temperature Max. 200 C 51191170 Silicone rubber seal (septum) for screw cap GL 14 Silicone rubber VQM Ø 12 mm, thickness 2 mm 51190317 Screw cap GL14, with aperture PBT Temperature Max. 200 C Aperture Ø 9.5 mm 51103947 Silicone rubber sealing ring with vulcanized-on PTFE washers for GL14 caps and sensors with outer Ø 6 mm Silicone rubber VQM, PTFE-coated Ø 12 mm, aperture 6 mm 92

Dosing Unit SP-50 Set 51191591 Bottle GL45 250 ml with cap Glass, PP 51191972 Distributor cap GL45 2 x GL14 PP 51161558 Adapter GL14-UNF PTFE GF25 36.14 mm x 2.62 mm 51191687 Assorted heat-shrink tubings 8 pcs in a set Polyolefin 51161710 EasyMax Operating Instructions Factory Test Report Quantity 1 of each 93

Dosing Unit SP-50 Syringes Dosing Unit SP-50 Syringes Flexible volumes from 1 ml, 10 ml, 25 ml, and 50 ml syringes Automatic refill of syringes possible with Dosing Unit SP-50 Interchangeable at all times during an experiment 51191793 Syringe 1 ml Glass, PTFE, metal Volume 1 ml 51191792 Syringe 10 ml Glass, PTFE, metal Volume 10 ml 51191794 Syringe 25 ml Glass, PTFE, metal Volume 25 ml 51191987 Syringe 50 ml Glass, PTFE, metal Volume 50 ml 94

3-Way Dosing Adapter Set EasyMax 3-Way Dosing Adapter Set EasyMax 3-way dosing adapter set consisting of 51161834 3-way dosing adapter set This adapter set allows the connection of three dosing channels to the reactor. Order Number Product Description Quantity 51162615 3-way glass adapter ST14/23-GL14 1 51190318 Screw cap GL14, closed 2 51161558 Adapter GL14-UNF 2 51190317 Screw cap GL14, with aperture 3 51103947 Silicone rubber sealing ring, outer Ø 12 mm, aperture 6 mm 3 51191203 Nut for UNF 1/4 28 threads, outer Ø max. 1.6 mm, 4 pcs in a set 1 95

3-Way Dosing Adapter Set 51162615 3-way glass adapter, ST14/23-GL14 Borosilicate glass Temperature 40 C to 180 C 51 161 558 Adapter GL14-UNF PTFE GF25 36.14 mm x 2.62 mm Sealing ring needed no. 51103947 51190317 Screw cap GL14, with aperture PBT Temperature Max. 200 C Aperture Ø 9.5 mm 51103947 Silicone rubber sealing ring with vulcanized-on PTFE washers for GL14 caps and sensors with outer Ø 6 mm Silicone rubber VQM, PTFE-coated Ø 12 mm, aperture 6 mm 51190318 Screw cap GL14, closed with PTFE sealing PBT Temperature Max. 200 C 51191203 Nut for UNF 1/4 28 threads ETFE Inner Ø max. 1.6 mm Quantity 4 pcs in a set 96

Accessories and Peripherals EasyMax Peripherals Optional Accessories Glass adapter set for Ø 1.6 8 mm consisting of 51161852 Adapter Set for probes, Ø 1.6 mm to 8 mm This adapter allows the connection of 1/4 ReactIR probes, 6 mm ph probes, 1.6 mm and 3.2 mm tubes to the reactor. Order Number Product Description Quantity 51191267 Glass adapter ST14/23-GL14 1 51190317 Screw cap GL14, with aperture 1 51161558 Adapter GL14-UNF 1 51103947 Silicone rubber sealing ring, outer Ø 12 mm, aperture 6 mm 1 51161037 Adapter for GL14 and 6.4 mm sensors 1 51161102 Silicone rubber sealing, outer Ø 12 mm, aperture 8 mm 1 97

Accessories and Peripherals 51191267 Glass adapter ST14/23-GL14 Glass Height 54 mm 51161558 Adapter GL14-UNF PTFE GF25 36.14 mm x 2.62 mm Sealing ring needed no. 51103947 51190317 Screw cap GL14, with aperture PBT Temperature Max. 200 C Aperture Ø 9.5 mm 51103947 Silicone rubber sealing ring with vulcanized-on PTFE washers for GL14 caps and sensors with outer Ø 6 mm Silicone rubber VQM, PTFE-coated Ø 12 mm, aperture 6 mm 51161037 Adapter for GL14 and 6.4 mm sensors PTFE Inner Ø 6.4 mm, outer Ø 12 mm, Sealing ring needed no. 51161102 51161102 Silicone rubber sealing ring with vulcanized-on PTFE washers for GL14 caps and sensors with outer Ø 8 mm Silicone rubber VQM, PTFE-coated Ø 12 mm x 5 mm, aperture 8 mm 98

Accessories and Peripherals Peripherals 51191952 50 ml dropping funnel, ST14/23 with PTFE stopcock and pressure equalizing tube Glass, PTFE Ø 35 mm, length 250 mm 51161029 Reflux condenser for ST14/23 port with 2 GL14 connectors for coolant Borosilicate glass Outer Ø 24 mm, height 140 mm 51162530 Reflux condenser for ST19/26 port Borosilicate glass Outer Ø 40 mm, height 250 mm 99

Upgrade Kit EasyMax HFCal Upgrade Kit EasyMax HFCal Upgrade Kit EasyMax HFCal consisting of 30090576 Upgrade Kit EasyMax HFCal A calorimetry Upgrade Kit for EasyMax contains all necessary parts to convert the workstation into a fully functional calorimeter. icontrol software is not included. It is Plug and Play. No service call is required for installation. Order Number Product Description Quantity 30090577 Module EasyMax HFCal 1 30099798 Temperature sensor, glass, 260 mm 2 30090579 Calibration heater, Alloy C-22, 260 mm 2 51162720 Adapter ST14, PTFE, with sealing ring 4 51191988 CAN cable 100 cm 1 30092605 EasyMax HFCal Quick Start Guide 1 icontrol HeatFlow License 1 100

Upgrade Kit EasyMax HFCal 30090577 Module EasyMax HFCal can be attached on the left or right side of the EasyMax 120 mm x 40 mm x 170 mm (w, d, h) 51191988 CAN cable 100 cm Length 100 cm 30090579 Calibration heater Alloy C-22 Ø 6.35 mm, 260 mm 30099798 Temperature sensor Glass Ø 6 mm, 260 mm 51162720 PTFE adapter, eccentric including 51162716 sealing ring PTFE GF25 Inner Ø 6 mm, ST14 Can also be used for Ø 1/4 6.35 mm inserts 51162716 Sealing ring for 51162720 PTFE adapter PTFE Inner Ø 6 mm Can also be used for Ø 1/4 6.35 mm inserts 30092605 EasyMax HFCal Quick Start Guide A4 101

Startet Kit EasyMax HFCal Starter Kit EasyMax HFCal 30090574 Starter Kit EasyMax HFCal The EasyMax HFCal Starter Kit applies heat flow based process safety screening. This quickly obtains heat information on a 100 ml scale. Thermostat and software are included. Reactor, cover, and stirrer must be purchased separately. Starter Kit EasyMax HFCal consisting of Order Number Product Description Quantity 51161711 EasyMax 102 thermostat system for details see page 5 1 51161099 Lab bar, stainless steel, Ø 14 mm x 600 mm 2 103472 Lab bar, stainless steel, Ø 14 mm x 300 mm 1 30090576 Upgrade Kit EasyMax HFCal 1 51161893 icontrol Single Instrument License for details see page 83 1 EasyMax Calorimetry Optional Parts 30090590 Temperature sensor Alloy C-22 Ø 6.35 mm, 260 mm 102

EasyMax Basic Upgrade Sets EasyMax Basic Upgrade Sets Optional Accessories 30133678 EasyMax Basic Plus Upgrade license Recorded experiment data can easily be exported and evaluated in Microsoft Excel A sequence of consecutive tasks can be programmed to safely run while unattended Data can be displayed and followed as trend graphs EasyMax Basic Plus Upgrade license consisting of Order Number Product Description Quantity USB 2.0 memory stick, contains software and manual 1 EasyMax Basic Plus license key 1 Product Information How to upgrade to EasyMax Basic Plus 1 30133679 EasyMax Advanced Upgrade license EasyMax Basic software and firmware upgrade to EasyMax Advanced functionalities Connectivity to optional icontrol PC Software ensures that experiments can be controlled using a PC without any touchscreen interaction All experimental events and data is automatically captured, prepared and shared, with a one-year ic Data Center license Controlling ph guarantees control through automating additions, of bases or acids EasyMax Advanced Upgrade license consisting of Order Number Product Description Quantity USB 2.0 memory stick, contains software and manual 1 EasyMax Advanced license key 1 icontrol DVD-Rom 1 icontrol Office License 1 ic Data Center CD-Rom 1 ic Data Center voucher one year free trial license 1 Product Information How to upgrade to EasyMax Advanced 1 103

icontrol Software for EasyMax icontrol Software for EasyMax Optional Accessories The software for experiment preparation, instrument control and data evaluation icontrol for single or multiple instruments icontrol for Office icare software maintenance icontrol Software for EasyMax icontrol provides the maximum amount of information from a single experiment. It uses a simple-tooperate user interface enabling EasyMax to be operated by either the PC software or in combination with the touchscreen. icontrol enables scientists to gain a comprehensive understanding of the chemical reaction under study. The combination of reactor data with information from METTLER TOLEDO analytical tools helps chemists in research and development reach appropriate conclusions from each experiment, enabling them to make better decisions and complete projects faster. Order Number License type Description 51161893 icontrol Single Instrument License Software license for experiment preparation, control and data evaluation for one instrument 51161894 icontrol Multiple Instrument Option Software license for experiment preparation, control and data evaluation for up to three instruments 51162613 icontrol Office License Software license for experiment preparation and experiment evaluation 51162629 icare for icontrol Instrument Software maintenance for instrument license 51162630 icare for icontrol Office Software maintenance for office license 104

Notes 105

106 Notes

Notes 107

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