ERC REFRACTOMAX 520. Clarity Control Module. Code/Rev.: M190/70C Date: 8/23/2018
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1 ERC REFRACTOMAX 520 Clarity Control Module ENG Code/Rev.: M190/70C Date: 8/23/2018 Phone: DataApex Ltd. Fax: Petrzilkova 2583/ Prague 5 The Czech Republic
2 Clarity, DataApex and are trademarks of DataApex Ltd. Microsoft and Windows TM are trademarks of Microsoft Corporation. DataApex reserves the right to make changes to manuals without prior notice. Updated manuals can be downloaded from Author: DM
3 Table of Contents Contents 1 ERC Refractomax 520 Control Module 1 2 Requirements 2 3 Installation Procedure ERC Refractomax 520 detector communication Clarity Configuration 4 4 Using the control module Method Setup - Acquisition Method Setup - Advanced Hardware Configuration Device Monitor DataApex UNI Setup 12 5 Report Setup 13 6 Troubleshooting 14 - i -
4 Table of Contents Clarity Control Module To facilitate the orientation in the ERC Refractomax 520 manual and Clarity chromatography station, different fonts are used throughout the manual. Meanings of these fonts are: Instrument (blue text) marks the name of the window to which the text refers. Open File (italics) describes the commands and names of fields in Clarity, parameters that can be entered into them or a window or dialog name (when you already are in the topic describing the window). WORK1 (capitals) indicates the name of the file and/or directory. ACTIVE (capital italics) marks the state of the station or its part. The bold text is sometimes also used for important parts of the text and the name of the Clarity station. Moreover, some sections are written in format other than normal text. These sections are formatted as follows: Note: Notifies the reader of relevant information. Caution: Warns the user of possibly dangerous or very important information. Marks the problem statement or trouble question. Description: Presents more detailed information on the problem, describes its causes, etc. Solution: Marks the response to the question, presents a procedure how to remove it. - ii -
5 1 ERC Refractomax 520 Control Module 1 ERC Refractomax 520 Control Module This manual describes the setting of the ERC Refractomax 520 detector. The control module enables direct control of the instrument over serial line. Fig 1: ERC Refractomax 520 detector Direct control means that the detector can be completely controlled from the Clarity environment. The Instrument method controlling the analysis conditions will be saved in the measured chromatograms. The control is performed via the UNI Ruby control module and the ERC Refractomax 520 script
6 2 Requirements 2 Requirements Clarity Installation USB with LC Control (p/n A24) or GC Control module (p/n A23) license Free serial COM port in the PC. Note: Modern computers usually have only one (if any) serial (COM) port installed. To use more devices requiring the RS232 port, the MultiCOM adapter (p/n MC01) is available. Serial DB9F-DB9M straight cable (p/n SK02). Note: Cables are not part of Clarity Control Module. It is strongly recommended that you order the required cables together with the Control Module
7 3 Installation Procedure 3 Installation Procedure 3.1 ERC Refractomax 520 detector communication The ERC Refractomax 520 is controlled by serial (RS232) communication. It uses a standard serial DB9F-DB9M straight cable (p/n SK02) described in the picture below. Fig 2: Serial DB9F-DB9M straight cable - 3 -
8 3 Installation Procedure Clarity Control Module 3.2 Clarity Configuration Fig 3: How to Add ERC Refractomax 520 module Start the Clarity station by clicking on the icon on the desktop. Invoke the System Configuration dialog accessible from the Clarity window using the System - Configuration... command. Press the Add button (1 on Fig 3 on pg 4.) to invoke the Available Control Modules dialog. You can specify the search filter 2 to simplify the finding of the driver
9 3 Installation Procedure Select the correct item and press the Add (3 on Fig 3 on pg 4.) button. Each device with already created UNI profile should have its own item named accordingly in the Available Control Modules dialog. The DataApex UNI Setup dialog will appear. Fig 4: DataApex UNI Setup Set the correct communication Port and click on the AutoDetect button to establish communication with the device. You may fill in the custom Device Name. Note: The DataApex UNI Setup dialog is described in detail in the chapter "DataApex UNI Setup" on pg 12. The ERC Refractomax 520 item 4 will appear in the Setup Control Modules list of the System Configuration dialog. Drag the appropriate item from the Setup Control Modules list on the left side to the desired Instrument tab 5 on the right side 6, or click on the button
10 4 Using the control module 4 Using the control module After adding and setting up the detector a new Acquisition tab will appear in the Method Setup dialog. A new ERC Refractomax 520 detector section enabling the monitoring of the current detector state will be also created in the Device Monitor window
11 4 Using the control module Clarity Control Module 4.1 Method Setup - Acquisition The Method Setup - Acquisition tab serves for setting the common parameters of the ERC Refractomax 520 detector. If more than one detector is available, it is possible to select between them by using the Select Detector combobox on the top of the dialog. Fig 5: Method Setup - Acquisition Sampling Period [s] Defines the frequency of data being gathered in the detector. The frequency of the data being sent to Clarity from the detector is defined by Response Time parameter. Valid values for the ERC Refractomax 520 detector range from 0.1 to 2.0 s. Range for Integrator Output [µriu/v] Sets the output range for the Integrator Output analog output, as well as digital signal sent to Clarity. The available range is dependent on the Detector Model as set in the DataApex UNI Setup dialog. Range for Recorder Output [µriu/fs] Sets the output range for the Recorder Output analog output, as well as digital signal sent to Clarity. Polarity of the Output Signals Determines the polarity of the output signal. Balance of the Output Signals [mv] Defines the value to which the signal level will be reset when Autozero function is used
12 4 Using the control module Response Time [s] Sets the frequency of the data being sent to Clarity from the detector. Setting this parameter to other value than Sampling Period means that the detector will filter the data and only send averaged values to Clarity. Temperature [ C] Defines the working temperature of the ERC Refractomax 520 detector. Equilibration Temperature Tolerance [ C] Serves for the setting of the target temperature tolerance. When the temperature reaches the desired value with the tolerance set here, the detector gets to the READY state. Autozero before Run Sets whether the detector should be autozeroed at the beginning of the analysis run. From Det Loads the detector control parameters from the detector to Clarity. Det Status When invoked, opens the Hardware Configuration dialog showing the information regarding the connected detector
13 4 Using the control module Clarity Control Module 4.2 Method Setup - Advanced The Method Setup - Advanced tab serves for setting the usage of auxiliary signals of the ERC Refractomax 520 detector. Fig 6: Method Setup - Advanced The list of available auxiliary signals is shown in the table in the lower part of the dialog. By checking the checkbox in the Store column for the particular row, the given auxiliary signal will be stored into the measured chromatogram
14 4 Using the control module 4.3 Hardware Configuration The Hardware Configuration dialog (invoked by using the Det Status button from the Method Setup - Acquisition dialog) displays the configuration of the ERC Refractomax 520, namely the communication type and its parameters. Fig 7: Hardware Configuration
15 4 Using the control module Clarity Control Module 4.4 Device Monitor The window with the detector status can be invoked by the Monitor - Device Monitor command from the Instrument window or using the Device Monitor icon. Autozero Zeroes the connected detector. Fig 8: Device Monitor - Detector Valve Current Position Shows the state of the purge valve. The valve position can be changed using the Purge Valve row. Purge Valve Allows to set the purge valve on or off. The current state of the purge valve is visible in the Valve Current Position row. Such action can only be performed outside of the analysis run. Current Temperature [ C] Shows the current temperature of the detector cell. Set Temperature [ C] Shows the set temperature of the detector cell
16 4 Using the control module 4.5 DataApex UNI Setup The appearance of the DataApex UNI Setup dialog depends on the presence of the selected Ruby Script - if the script is not present, only the Ruby Script field is visible. Fig 9: DataApex UNI Setup Ruby Script Displays the selected Ruby Script. The correct ERCREFRACTOMAX520DET.RB script for the ERC Refractomax 520 detector can be found in the UTILS/UNI_ DRIVERS/ERC subdirectory (accessible through the button) of the Clarity installation folder (C:\CLARITY\BIN by default). Port Defines the communication port used, possible values dependent on the type of communication of the device and/or available ports in the PC. AutoDetect It is used for verifying the device communication over the serial port selected above. Detector Name Allows you to set the custom name of the detector. This name (entered into the Value column) will be used throughout the Clarity station. Detector Model Allows you to set the type of the detector. The selection influences several settings further in Method Setup - Acquisition dialog. Firmware Displays the firmware & model version string upon pressing the AutoDetect button
17 5 Report Setup 5 Report Setup The detector section on the method report can be enabled by checking the Instrument Control checkbox on the Method tab of the Report Setup dialog. Auxiliary signals setting made on Method Setup - Advanced tab will be also printed. Fig 10: Report Setup All of the parameters set in the Method Setup - Acquisition dialog are reported, as well as the custom Detector Name and other parameters set in the DataApex UNI Setup dialog
18 6 Troubleshooting 6 Troubleshooting When the solution to a problem cannot be found easily, a recording of the communication between Clarity and the detector will significantly help DataApex support. The data recording can be enabled by adding or amending the COMMDRV.INI file in the Clarity installation directory (C:\CLARITY\CFG by default). The file can be edited in any text editor (e.g. Notepad). The following section should be edited or added: [COM1] echo=on textmode=on filename=commdrvcom1_%d.txt reset=off Note: Instead of COM1, type the communication port used to communicate with the ERC Refractomax 520 detector. This port number is displayed when the Det Status button in the Method Setup - Acquisition dialog is invoked. Note: %D (or %d) in the filename parameter means that the log will be created separately for each day. The reset=off parameter disables deleting the content of the log each time the station is started during the same day. The created *.TXT files will be of great help in the diagnosis of not documented errors and communication issues
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