Agilent 3395 Integrator
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- Shavonne Leonard
- 5 years ago
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1 Agilent 3395 Integrator Operating Manual Agilent Technologies
2 Agilent 3395/3396 Integrators Manuals These manuals may contain references to HP or Hewlett-Packard. Please note that Hewlett-Packard s former test and measurement, semiconductor products and chemicals analysis businesses are now part of Agilent Technologies. The HP 3395/3396 Integrator referred to throughout this document is now the Agilent 3395/3396 Integrator.
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7 ÉÉ É ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ É É
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12 * LIST: *HELP ANALYZE ASSIGN BASIC BX COPY CREATE DATE
13 * # * TIME.5 CHT SP * LIST: CHT SP = 1.0
14 * DATR E 4/14/95 = DATE 4/14/95 INVALID SYSTEM COMMAND *
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21 * REPORT RUN# 65 OCT 5, :01:32 SIGNAL FILE: M:SIGNAL.BNC TECH PROPIONIC ACID [CTRL D] * REPORT SAMPLE# 7 RUN# 65 OCT 5, :01:32 SIGNAL FILE: M:SIGNAL.BNC TECH PROPIONIC ACID SAMPLE# 7 * OP # 5 PRINT & POST-RUN LIST OPTIONS Large font [Y*/N]:
22 DEVICE ADDRESS: COMMAND STRING: ASSIGN 1,E:USER_INT.BAS CREATE TEMP.DAT,2048
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25 * DATE 3/28/95 MAR 28, :00:20 * TIME 08:35:30 MAR 28, :35:30
26 * PLOT STOP * RUN # 1 MAR 28, :46:51 START STOP
27 START :
28 INTEGRATION PLOT TYPE (Source/Filtered/Unigram/No Plot) ENTER PLOT TYPE [S/F*/U/N]: * * Source Plot Filtered Plot Unigram Plot No Plot
29 INTEGRATION PLOT TYPE (Source/Filtered/Unigram/No Plot) ENTER PLOT TYPE [S/F*/U/N]: Presentation plot [Y/N*]:
30 * LIST: ZERO = 0, * ZERO START ZE@
31 * ATT 2^ START * ATT 2^ START
32 * CHT SP * CHT SP
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34 *
35 * OP # 5 PRINT & POST RUN LIST OPTIONS Large font [Y*/N]: Store post run report [Y/N*]: External post run report [Y/N*]: List run parameters [Y/N*]: List timetable [Y/N*]: List calibration [Y/N*]: List remote method [Y/N*]: Form feed before report [Y/N*]: Form feed after report [Y/N*]: Skip perforations in report [Y/N*]: Skip perforations in plot [Y/N*]:
36 ZE ZE AT CS PW TH AR IF ST
37 * TIME.5 CHT SP * LIST: CHT SP = 7.0 * EDIT METH 1 = RUN PARAMETERS 2 = TIMETABLE EVENTS 3 = CALIBRATION FILE. SECTION TO BE EDITED: TIMETABLE EVENTS SELECT EVENTS FROM THE FOLLOWING MENU: [IF/EX/ZE/^Z/AT/CS/AR/TH/PW/ST] TIME: EVENT: VALUE:
38 * LIST: INTG # = AR REJ = CHT SP = INTG # = INTG # = 8 * DELETE TIME INTG # * LIST: AR REJ = CHT SP = 7.0
39 EMPTY * LIST: AR REJ = 66 * TIME.032 AR REJ * LIST: AR REJ = 100
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42 * LIST: LIST PEAK CAPACITY: 1244 ZERO = 0, ATT 2^ = 0 CHT SP = 1.0 AR REJ = 0 THRSH = 0 PK WD = 0.04 * LIST: PK WD = 0.01
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44 * PK
45 * TIME 1.00 PK * TIME 1.00 PK * TIME 1.01 PK
46 * THRSH
47 * AR REJ
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49 IF IF
50 * TIME.3 INTG # * TIME.55 INTG # IF IF 0.574
51 * LIST: INTG # = INTG # = INTG # = 5
52 Error storing signal; FILE ALREADY OPEN
53 INVALID MUTE HOST CONVERSATION TIMETABLE
54 * OP # 4 REPORT OPTIONS Suppress local report [Y/N*]: * OP # 7 DEFAULT SAMPLE INFORMATION USE SAMPLE TABLE IN MANUAL RUN [Y/N*]: ISTD AMT [0.0000E+00 ]: SAMPLE AMT [0.0000E+00 ]: MUL FACTOR [1.0000E+00 ]: * OP # 4 REPORT OPTIONS Suppress local report [Y/N*]:
55 * PREP E = EXTERNAL STANDARD I = INTERNAL STANDARD N = NORMALIZATION CALIB PROCEDURE [E*/I/N]: REF % RTW [ 5.000]: NON-REF % RTW [ 5.000]: RF BASED ON AREA OR HEIGHT [A*/H]: CAL# RT AMT NAME 1 :
56 ÉÉ ÉÉ ÉÉ ÉÉ É ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ É É ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ É É ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ É É ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ É É
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63 ÉÉ ÇÇÇÉÉÇÇÇ ÇÇÇÉÉÇÇÇ ÇÇÇÉÉÇÇÇ ÇÇÇÉÉÇÇÇ ÇÇÇÉÉÇÇÇ
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70 ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉÉ
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72 É ÉÉ ÉÉ ÉÉ ÉÉ
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86 ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉÉÉ ÉÉÉÉ
87 É ÉÉ ÉÉ ÉÉÉÉÉ ÉÉÉÉÉ ÉÉÉÉÉ ÉÉÉÉÉÉ ÉÉ ÉÉ ÉÉ ÉÉÉ ÉÉÉ ÉÉÉ ÉÉÉ
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93 Response Factor:
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98 ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁ ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁ ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁ ÁÁÁÁ ÁÁÁÁ ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁ
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104 Point-to-point
105 Linear Non-linear (quadratic)
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107 ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁ
108 ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ
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110 ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ
111 ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ
112 ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ
113 ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ
114 ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ
115 ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ
116 ÁÁÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ
117 ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁ
118
119 ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ
120 ÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ
121 ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ
122 ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁ
123
124
125
126 NO RUN PEAKS STORED. CALIB EXISTS E = EXTERNAL STANDARD I = INTERNAL STANDARD N = NORMALIZATION CALIB PROCEDURE (E*/I/N): E
127 REF % RTW [ 5.000]: REF % RTW [ 5.000]: ÈÈÈ ÈÈÈ ÈÈÈ ÈÈÈ ÈÈÈ NON-REF % RTW [ 5.000]: RF BASED ON AREA OR HEIGHT [A*/H]:
128 CAL# RT AMT NAME 1 : CAL# RT AMT NAME 1 :.082 :10 :S1 2 :.173 :5 :S2 3 :.498 NO MATCH :S
129 REF PK CAL#: ISTD CAL#: GROUP PEAKS [Y/N*]: CALIBRA- TION options GRP# CAL# NAME 1 : NAME GRP# CAL# NAME 1 :7,9,10 :BUTENE
130 CALIBRATION OPTIONS RF of uncalibrated peaks [0.0000E+00 ]: Replace calibration fit [Y/N*]: Disable post-run RT update [Y/N*]: ISTD AMT [0.0000E+00 ]: SAMPLE AMT [0.0000E+00 ]: MUL FACTOR [1.0000E+00 ]: ISTD AMT SAMPLE AMT MUL FACTOR SAMPLE AMT MUL FACTOR MUL FACTOR MUL FACTOR
131 CALIBRATION OPTIONS RF of uncalibrated peaks [0.0000E+00 ]: Replace calibration fit [Y/N*]: P = point-to-point L = linear N = non-linear (quadratic) Calibration fit [N/L/P*]: Point-to-point
132 Linear Non-linear (quadratic) CAL# RT AMT 1 : rr.rrr :
133
134
135 AMT/AREA AMT/HEIGHT * EDIT CALIB 1 = CALIB PROCEDURE 2 = RETENTION TIME WINDOWS 3 = TABLE ENTRIES 4 = PEAK GROUPS 5 = CALIB options SECTION TO BE EDITED:
136 * OP() CALIBRATION OPTIONS RF of uncalibrated peaks [0.0000E+00 ]: Replace calibration fit [Y/N*]: P = point-to-point L = linear (least square) N = non-linear (quadratic) Calibration fit [N/L/P*]: Disable post-run RT update [Y/N*]: ISTD peak #: ISTD AMT [1.0000E+00 ]: SAMPLE AMT [0.0000E+00 ]: MUL FACTOR [1.0000E+00 ]: Replace calibration fit Calibration fit ISTD peak # ISTD CAL#
137 NO CALIB TBL. * LIST: CALIB ISTD REF % RTW: NON-REF % RTW: LEVEL: 1 RECALIBRATIONS: 1 CAL# RT LV AMT AMT/AREA 1& E E CAL# 1 NAME CALIBRATION options RF of uncalibrated peaks E+00 Calibration fit... P Disable post-run RT update.. NO ISTD peak #... 1 ISTD AMT... 1 SAMPLE AMT E+00 MUL FACTOR E+00
138 DELETE ALL [Y/N*]: * DELETE CALIB * EDIT CALIB 1 = CALIB PROCEDURE 2 = RETENTION TIME WINDOWS 3 = TABLE ENTRIES 4 = PEAK GROUPS 5 = CALIB OPTIONS SECTION TO BE EDITED: CAL#:
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141 * OP() DEFAULT SAMPLE INFORMATION USE SAMPLE TABLE IN MANUAL RUN [Y/N*]: ISTD AMT [0.0000E+00 ]: SAMPLE AMT [0.0000E+00 ]: MUL FACTOR [1.0000E+00 ]: RECALIBRATION [Y/N*]:
142 LEVEL [0 ]: NAME: REPORT MEMO: * OP # 7 * LIST: OP # 7 DEFAULT SAMPLE INFORMATION USE SAMPLE TABLE IN MANUAL RUN. NO ISTD AMT E+00 SAMPLE AMT E+00 MUL FACTOR E+00 RECALIBRATION NO SAMPLE NAME REPORT MEMO
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147 * *H:
148 *SY RS-232-C SWITCH SETTINGS Baud 9600 Timeout 15 sec Handshake Delay Off Hardware Handshake Disabled INTERNAL SERIAL NUMBER: 22390
149
150 * OP # 2 RUN DATA STORAGE Store signal data [Y/N* Device [M*]: Bunched or raw data [B/R*]: ] Local run-time storage [Y/N*]: Keep run-time storage [Y/N*]: Store processed peaks [Y/N*]: * OP # 2 RUN DATA STORAGE Store signal data [Y/N* Device [M*]: M:SIGNAL.BNC
151 CAUTION: Previous signal data will be lost Bunched or raw data [B/R*]: Store processed peaks Local run-time storage [Y/N*]: Copying signal file to host
152 Keep run-time storage [Y/N*]: Deleting local signal file Store processed peaks [Y/N*]:
153 * STORE M:METH20.MET * OP # 5 PRINT & POST-RUN LIST OPTIONS Large font [Y*/N]: Store post-run report [Y/N*]: Device [M*]:
154 *DI VOLUME NAME: MDISK DRIVE: M DATE: JAN 8, :20:13 FILE NAME LENGTH CREATED/VERSION SIG_BUFF.RAW /05/90 14:48:02 LU1.MET /03/90 18:04:45 PROG.BAS /05/90 15:07:35 USED FREE MAX FILES BYTES
155 FREE MAX FREE USED MAX LENGTH FREE MAX FREE USED MAX
156 *COPY M:CA1.CAL,M:CA1.CAL *RENAME M:SIGNAL.BNC,M:RUN5.BNC
157 *PURGE M:METH1.MET
158
159
160
161
162
163
164 * HEIGHT% report [Y/N*]: ENTER PLOT TYPE [S/F*/U/N]:
165 * PREP METH RUN PARAMETERS ZERO [ 0 ]: ATT 2^ [ 0 ]: CHT SP [ 1.0 ]: AR REJ [ 0 ]: THRSH [ 0 ]: PK WD [ 0.04 ]: TIMETABLE EVENTS DELETE CURRENT TABLE [Y/N*]:
166 TIMETABLE EVENTS SELECT EVENTS FROM THE FOLLOWING MENU [IF/EX/ZE/^Z/AT/CS/AR/TH/PW/ST] TIME: EVENT: VALUE: TIME:
167 TIME:.30 EVENT: PW ] VALUE:.05 TIME:.8 [ EVENT: ST VALUE:?
168 REPLACE CURRENT CALIBRATION [Y/N*]: CALIBRATION FILENAME: CALIBRATION FILENAME: CALIBRATION FILENAME:
169 INTEGRATION PLOT TYPE (Source/Filtered/Unigram/No Plot) ENTER PLOT TYPE [S/F*/U/N]: Presentation plot [Y/N*]: RUN DATA STORAGE Store signal data [Y/N*]: Device [M*]: CAUTION: Previous signal data will be lost Bunched or raw data [B/R*]: Store processed peaks [Y/N*]:
170 REPORT OPTIONS Suppress local report [Y/N*]: HEIGHT% report [Y/N*]: Replace report title [Y/N*]: Report title: Replace amount label [Y/N*]: Report uncalibrated peaks [Y/N*] Extended report [Y/N*]: PRINT & POST-RUN LIST OPTIONS Large font [Y*/N]: Store post-run report [Y/N*]: Device [M*]: List run parameters [Y/N*]: List time table [Y/N*]: List calibration table [Y/N*]: Form feed before report [Y/N*]: Form feed after report [Y/N*]: Skip perforations in report [Y/N*]:
171
172 * STORE METH * LOAD METH ATTEMPTED WRITE PAST END OF FILE. DISK FULL.
173 * EDIT METH 1 = RUN PARAMETERS 2 = TIMETABLE EVENTS 3 = CALIBRATION FILE 4 = INTEGRATION PLOT TYPE 5 = RUN DATA STORAGE OPTIONS 6 = REPORT OPTIONS 7 = POST-RUN LIST OPTIONS 8 = REMOTE DEVICE ACCESS SECTION TO BE EDITED: SECTION TO BE EDITED: REMOTE DEVICE ACCESS
174 FILE NOT FOUND.
175 * LIST METH RUN PARAMETERS ZERO = 0 ATT 2^ = 2 CHT SP = 1.0 AR REJ = 0 THRSH = 2 PK WD = 0.01 TIMETABLE EVENTS PK WD = STOP CALIBRATION NORM REF % RTW: NON-REF % RTW: LEVEL: 1 RECALIBRATIONS: 1 CAL# RT LV AMT AMT/HEIGHT 1R E E E E 06 3R E E E E 03 5R E E 04 CAL# NAME 1 PK1 2 PK2 3 PK3 4 PK4 5 PK5 GRP# CAL# NAME 1 2, 4, GRP1 2 3, 5, GRP2 3 4, 5, GRP3 4 2, 4, 5, GRP4 5 1, 3, 5, GRP3
176 INTEGRATION PLOT TYPE... FILTERED Presentation plot... NO RUN DATA STORAGE Store signal data... YES Device... M Bunched or raw data... BUNCHED Store processed peaks... NO CALIBRATION OPTIONS RF of uncalibrated peaks E+00 Calibration fit... P Disable post-run RT update.. NO MUL FACTOR E+00 REPORT OPTIONS Suppress local report... NO Height% report... NO Report title: SLUDGE Amount label... GMS Report uncalibrated peaks... YES Extended report... YES PRINT & POST-RUN LIST OPTIONS Large font... YES Store post-run report... NO List run parameters... YES List timetable... YES List calibration table... NO Form-feed before report... NO Form-feed after report... NO Skip perforations in report. NO Skip perforations in plot... NO
177 * DELETE METH
178
179 * LIST: RUN PARAMETERS ZERO = 0 ATT 2^ = 0 CHT SP = 1.0 AR REJ = 0 THRSH = 0 PK WD = 0.04 TIMETABLE EVENTS EMPTY CALIBRATION NO CALIB TBL INTEGRATION PLOT TYPE... FILTERED Presentation plot... NO RUN DATA STORAGE Store signal data... NO Store processed peaks... NO REPORT OPTIONS Suppress local report... NO HEIGHT% report... NO Report uncalibrated peaks... NO Extended report... NO PRINT & POST-RUN LIST OPTIONS Large font... YES Store post-run report... NO List run parameters... NO List timetable... NO List calibration table... NO Form-feed before report... NO Form-feed after report... NO Skip perforations in report. NO Skip perforations in plot... NO
180
181
182
183
184 * BOTTLE OR RUN SAMPLE INDEXED [R/B*]:
185 RUNS WAIT FOR START_INPUT: [Y/N*] REMOTE_START_RELAY: PRERUN/RUN [P/R*] Select the START mode you desire.
186 EQUILIBRATION TIME IN SECONDS [0 ]: REMOTE READY SENSING [C/S*]
187 METHOD [*]: CAUTION: Cannot get method file. FILE NOT FOUND NOT LOADED
188 Delete Sample Table [Y/N*]: 5. BOTTLE OR RUN SAMPLE INDEXED [R/B*]: USE SAMPLE TABLE IN MANUAL RUN [Y/N*]:.
189 FIRST BOTTLE [1 ]: FIRST RUN [1 ]: LAST BOTTLE [1 ]: LAST RUN [1 ]: BOTTLE # : RUN # : ISTD AMT: SAMPLE AMT: MUL FACTOR:
190 RECALIBRATION [Y/N*]: LEVEL: NAME REPORT MEMO BOTTLE #: RUN #: NEXT SEQUENCE: Caution: Cannot get sequence file.
191 WAITING FOR SYSTEM READINESS EQUILIBRATION DELAY IN PROGRESS FILE NOT FOUND NOT LOADED DISK DOES NOT EX- IST FIRST BOTTLE # RUN # LAST BOTTLE # RUN # FIRST RUN # LAST RUN # INVALID INDEX; ABORTED.
192
193
194 BOTTLE # USE SAMPLE TABLE IN MANUAL RUN [Y/N*]:
195 RUN # FIRST RUN # LAST RUN # USE SAMPLE TABLE IN MANUAL RUN [Y/N*]: FIRST RUN #
196 * EDIT SEQ 1 = EQUILIBRATION TIME DELAY 2 = METHOD FILE SPECIFICATION 3 = SAMPLE INFORMATION TABLE 4 = NEXT SEQUENCE SPECIFICATION SECTION TO BE EDITED: SAMPLE INFORMATION TABLE BOTTLE OR RUN NUMBER INDEXED [R/B*]: FIRST RUN [1 ]: LAST RUN [1 ]:... * OP # 7 DEFAULT SAMPLE INFORMATION USE SAMPLE TABLE IN MANUAL RUN [Y/N*]: ISTD AMT [1.0000E+O1 ]: *SET RUNNUM
197 FILE NOT FOUND SEQ NOT CHANGED SEQ NOT CHANGED DEFAULT SEQ INVOKED
198 1 = EQUILIBRATION TIME DELAY 2 = METHOD FILE SPECIFICATION 3 = SAMPLE INFORMATION TABLE 4 = NEXT SEQUENCE SPECIFICATION SECTION TO BE EDITED: BOTTLE # RUN # RUN #:
199 FILE NOT FOUND * LIST: SEQ RUNS WAIT FOR START_INPUT: [Y/N*]...Y REMOTE_START_RELAY: PRERUN/RUN[P/R*]..P EQUILIBRATION TIME IN SECONDS...5 METHOD... METH1.MET SAMPLE INFORMATION TABLE BOTTLE OR RUN SAMPLE INDEXED... R FIRST RUN... 5 LAST RUN RUN #... 5 ISTD AMT E+00 SAMPLE AMT E+00 MUL FACTOR E+00 RECALIBRATION... NO NAME... GROUP A NEXT SEQUENCE... SEQ2.SEQ
200
201
202
203 * AREA% RUN# 65 OCT 5, :01:32 SAMPLE# 7 SIGNAL FILE: M:SIGNAL.BNC TECH PROPIONIC ACID AREA% RT AREA TYPE WIDTH AREA% PP PB PB SBB BV VB BB TOTAL AREA=1.4477E+07 MUL FACTOR=1.0000E+00
204 * LIST: OP # 4 REPORT OPTIONS Suppress local report NO HEIGHT% report NO Report uncalibrated peaks NO Extended report NO
205 * OP # 4 REPORT OPTIONS Suppress local report [Y/N*]: HEIGHT% report [Y/N*]: Replace report title [Y/N*]: * AREA% RUN# 5 OCT 5, :01:32 SIGNAL FILE: M:SIGNAL.BNC PEAK FILE : M:Q1EBBE6F.PRO REPORT #5 SAMPLE# 5 HEIGHT% RT HEIGHT TYPE WIDTH HEIGHT% BB I BH TOTAL HEIGHT= MUL FACTOR=1.0000E+00
206
207 * OP # 4 REPORT OPTIONS Suppress local report [Y/N*]: HEIGHT% report [Y/N*]:
208 Replace report title [Y/N*]: Report title: Replace amount label [Y/N*]: Report uncalibrated peaks [Y/N*]: Extended report [Y/N*]: RT TYPE AREA WIDTH HEIGHT CAL# AMOUNT NAME
209 RT AREA TYPE CAL# AMOUNT * OP # 5 PRINT & POST-RUN LIST OPTIONS Large font [Y*/N]: Store post-run report [Y/N*]: Device [M*]: List run parameters [Y/N*]
210 List timetable [Y/N*]: EMPTY List calibration table [Y/*N]: Form-feed before report [Y/N*]: Form-feed after report [Y/N*]: Skip perforations in report [Y/N*]: Skip perforations in plot [Y/N*]:
211 * (USE BREAK OR CONTROL-Y TO END) Testing column conditioning; First pass operator is Kate * BREAK * ID Flavors Lab1 * REPORT RUN# 19 FEB 18, :24:00 IDENTIFIER : Flavors Lab1
212 Store post-run report [Y/N*]: Device [M*]:
213 RUN# 7 JAN 15, :22:08 SAMPLE NAME: SAMPLE NAME REPORT MEMO IDENTIFIER: LAB1 GC3 SIGNAL FILE: M:SIGNAL.RAW REPORT FILE: M:Q1FE0F80.RPT REPORT TITLE ISTD PEAK NOT MATCHED SAMPLE# 90
214
215
216 MUL FACTOR WIDTH AREA% HEIGHT% WIDTH RUN# 65 JUL 5, :01:32 SIGNAL FILE: M:SIGNAL.BNC TECH PROPIONIC ACID SAMPLE# 7 ESTD-AREA RT AREA TYPE CAL# AMOUNT BV VB BB 3R TOTAL AREA=1.4477E+07 MUL FACTOR=1.0000E+00
217
218 RUN# 65 JUL 5, :01:32 SIGNAL FILE: M:SIGNAL.BNC TECH PROPIONIC ACID SAMPLE# 7 ESTD-AREA RT AREA TYPE CAL# AMOUNT BV VB BB 3R TOTAL AREA=1.4477E+07 MUL FACTOR=1.0000E+00 RUN# 65 JUL 5, :01:32 SIGNAL FILE: M:SIGNAL.BNC TECH PROPIONIC ACID SAMPLE# 7 ESTD AREA RT TYPE AREA WIDTH HEIGHT CAL# AMOUNT NAME.138 PP PB PB SBB BV PPA VB IBTA BB R BTA TOTAL AREA=1.4477E+07 MUL FACTOR=1.0000E+04
219 * RUN # 18 JAN 1, :53:11 START IF CS8@ : AT TIMETABLE STOP
220 TIMETABLE STOP
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234 Agilent Technologies Agilent Technologies, Inc. 08/97 Part Number
Agilent 3396 Series III Integrator
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