Feed Check Sample No Chicken Starter/Grower, Medicated Association of American Feed Control Officials

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1 Feed Check Sample No Chicken Starter/Grower, Medicated Association of American Feed Control Officials - Pass 1 Results for 207 Labs - - Pass 2 Results for 206 Labs - No. Average No. Average AOAC Method of Grand Std. Range of Grand Std. Range Method 18th Code Labs Avg. Dev. of Dups Labs Avg. Dev. of Dups NPN, Urea + Am, Urease Method NPN, Automated Urea, Misc Method Group 000.XX PCT Loss on Drying, Vac 95 deg 5 hr Loss on Drying, ISO Loss on Drying, LECO Loss on Drying, 104 deg 3 hr, in malt Loss on Drying, 102 deg 16 hr, in meat Loss on Drying, Misc Method Group 001.XX PCT Protein, Crude Protein, Auto Kjel-Foss Protein, Semiauto Autoanalyzer Protein, Copper Cat Protein, Copper, Boric Acid Protein, Combustion Nitrogen Analyzer Protein, Cu/Ti Protein, Block dig/distillation Protein, NIR Protein, Misc Method Group 002.XX PCT Fat, Eth Ext, Direct Fat, Ind Eth Ext (13th ed), Indirect Fat, Pet Ether Fat, Soxtec, Eth Ext Fat, Soxtec, Pet Ether Fat, NIR Fat, Hexane Ext Fat, Soxtec, Hexane Ext Fat, Ankom Fat, Misc Method Group 003.XX PCT Fiber, Crude Asbestos Free Fiber, Sing Filt Fiber, Fritted Glass Fiber, Fibertec Fiber, ANKOM Fiber, NIR Sample July 26, 2009 Page 1

2 Feed Check Sample No Chicken Starter/Grower, Medicated Association of American Feed Control Officials - Pass 1 Results for 207 Labs - - Pass 2 Results for 206 Labs - No. Average No. Average AOAC Method of Grand Std. Range of Grand Std. Range Method 18th Code Labs Avg. Dev. of Dups Labs Avg. Dev. of Dups Fiber, Misc Method Group 004.XX PCT Ash, Ash, LECO Ash, NIR Ash, Misc Method Group 005.XX PCT Sugar, TSI, Lane-Eynon (12th) Sugar, Misc Method Group 006.XX PCT Fiber, Acid Detergent Fiber, Acid Detergent-Hach Fiber, Acid Detergent by ANKOM Fiber, Acid Detergent Misc Method Group 008.XX PCT Fiber, Neutral Det-ENZ Pretreat Fiber, Neutral Detergent by ANKOM Fiber, Neutral Det Misc Method Group 009.XX PCT Moisture, Karl-Fischer Moisture, NIR Moisture, Misc Method Group 010.XX PCT Loss on Drying, 135 deg 2 hr Method Group 011.XX PCT Starch, Polarimetric (Ewers) Starch, Megazyme Starch, Enzymatic Starch, YSI Analyzer Starch, NIR Method Group 012.XX PCT Fat, Mojonnier, Bak Ext Fat, Soxtec-Acid Hydrolysis Fat, Super Critical Fluid Extraction Fat, NIR-Acid Hydrolysis Fat, Ankon-Acid Hydrolysis Fat, Pretreat or extended ext, misc Method Group 013.XX PCT Aluminum, ICP Sample July 26, 2009 Page 2

3 Feed Check Sample No Chicken Starter/Grower, Medicated Association of American Feed Control Officials - Pass 1 Results for 207 Labs - - Pass 2 Results for 206 Labs - No. Average No. Average AOAC Method of Grand Std. Range of Grand Std. Range Method 18th Code Labs Avg. Dev. of Dups Labs Avg. Dev. of Dups Method Group 015.XX PPM Arsenic, AA, Hydride Boron, ICP Boron, Misc Method Group 017.XX PPM Cadmium, ICP Method Group 018.XX PPM Calcium, Ox-Mn04 Vol Calcium, At Abs Spect Calcium, Semiauto (Autoanalyzer) Calcium, ICP, Dry Ash Calcium, EDTA Calcium, ICP, Wet Ash Calcium, Misc Method Group 019.XX PCT Chromium, AA Chromium, ICP Chromium, Misc Method Group 020.XX PPM Cobalt, AA Cobalt, ICP Cobalt, Misc Method Group 021.XX PPM Copper, AA Copper, ICP, Dry Ash Copper, ICP, Wet Ash Copper, Misc Method Group 022.XX PPM Fluorine, Ion Sel Elect Iron, AA Iron, ICP, Dry Ash Iron, ICP, Wet Ash Iron, Misc Method Group 025.XX PPM Lead, Lead, Misc Method Group 026.XX PPM Magnesium, AA Magnesium, ICP, Dry Ash Sample July 26, 2009 Page 3

4 Feed Check Sample No Chicken Starter/Grower, Medicated Association of American Feed Control Officials - Pass 1 Results for 207 Labs - - Pass 2 Results for 206 Labs - No. Average No. Average AOAC Method of Grand Std. Range of Grand Std. Range Method 18th Code Labs Avg. Dev. of Dups Labs Avg. Dev. of Dups Magnesium, ICP, Wet Ash Magnesium, Misc Method Group 027.XX PCT Manganese, AA Manganese, ICP, Dry Ash Manganese, ICP, Wet Ash Manganese, Misc Method Group 028.XX PPM Mercury, Misc Phosphorus, Photometric Phosphorus, GQMP (2.028) Phosphorus, Autoanalyzer Phosphorus, ICP Phosphorus, Hach Method Phosphorus, Misc Method Group 031.XX PCT Potassium, AA Potassium, Flame Emission Potassium, ICP Potassium, Misc Method Group 032.XX PCT Salt, Sol Cl Salt, Poten Cl Salt, Quantab Salt, Ion Sel Electrode Salt, Misc Method Group 033.XX PCT Selenium, Fluor Selenium, AA, Flame Selenium, AA, Hydride Selenium, ICP Selenium, Misc Method Group 034.XX PPM Sodium, AA Sodium, Ion Sel Electrode Sodium, ICP Sodium, Flame Emission Sodium, Misc Method Group 035.XX PCT Sample July 26, 2009 Page 4

5 Feed Check Sample No Chicken Starter/Grower, Medicated Association of American Feed Control Officials - Pass 1 Results for 207 Labs - - Pass 2 Results for 206 Labs - No. Average No. Average AOAC Method of Grand Std. Range of Grand Std. Range Method 18th Code Labs Avg. Dev. of Dups Labs Avg. Dev. of Dups Sulfur, (Gravimetric) Sulfur, ICP Sulfur, LECO Method Group 036.XX PCT Zinc, AA Zinc, ICP, Dry Ash Zinc, ICP, Wet Ash Zinc, Misc Method Group 037.XX PPM Molybdenum, ICP Molybdenum, Misc Method Group 038.XX PPM Nickel, AA Nickel, ICP Method Group 039.XX PPM Barium, ICP Vanadium, ICP Method Group 041.XX PPM Amprolium, Color Amprolium, HPLC Method Group 045.XX PCT Monensin, HPLC Choline Chloride, Chem Choline Chloride, Misc Method Group 101.XX MG/LB Niacin, Chem Niacin, Micro Method Group 102.XX MG/LB Pantothenic Acid, Microbiological Method Group 103.XX MG/LB Riboflavin, Fluorometric Riboflavin, HPLC Method Group 104.XX MG/LB Thiamine, HPLC Vitamin A, Color Vitamin A, UV Vitamin A, HPLC Vitamin A, Misc Method Group 106.XX KU/LB Sample July 26, 2009 Page 5

6 Feed Check Sample No Chicken Starter/Grower, Medicated Association of American Feed Control Officials - Pass 1 Results for 207 Labs - - Pass 2 Results for 206 Labs - No. Average No. Average AOAC Method of Grand Std. Range of Grand Std. Range Method 18th Code Labs Avg. Dev. of Dups Labs Avg. Dev. of Dups Vitamin B12, Method Group 107.XX MCG/L Vitamin D3, HPLC Vitamin D3, HPLC Method Group 108.XX KU/LB Vitamin E, HPLC Vitamin E, Misc Method Group 109.XX MG/KG Pyridoxine, (Vitamin B6) Pyridoxine, Misc Method Group 112.XX MCG/G Folic Acid, Method Group 113.XX MG/KG Biotin, Microbiological Method Group 114.XX MG/KG Alanine, Post-col Ninhydrin Der Alanine, Pre-col AQC Der Method Group 120.XX PCT Arginine, Post-col Ninhydrin Der Arginine, Pre-col AQC Der Method Group 121.XX PCT Aspartic, Post-col Ninhydrin Der Method Group 122.XX PCT Cysteine/Cystine, PAO Post-col Ninhydri Cysteine/Cystine, PAO Post-col OPA Der Cysteine/Cystine, PAO Pre-col AQC Der Method Group 124.XX PCT Glutamic, Post-col Ninhydrin Der Glutamic, Pre-col AQC Der Method Group 125.XX PCT Glycine, Post-col Ninhydrin Der Glycine, Pre-col AQC Der Method Group 126.XX PCT Histidine, Post-col Ninhydrin Der Histidine, Pre-col AQC Der Method Group 127.XX PCT Isoleucine, Post-col Ninhydrin Der Isoleucine, Pre-col AQC Der Method Group 128.XX PCT Sample July 26, 2009 Page 6

7 Feed Check Sample No Chicken Starter/Grower, Medicated Association of American Feed Control Officials - Pass 1 Results for 207 Labs - - Pass 2 Results for 206 Labs - No. Average No. Average AOAC Method of Grand Std. Range of Grand Std. Range Method 18th Code Labs Avg. Dev. of Dups Labs Avg. Dev. of Dups Leucine, Post-col Ninhydrin Der Leucine, Pre-col AQC Der Method Group 129.XX PCT L-Lysine, Post-col Ninhydrin Der L-Lysine, Pre-col AQC Der Method Group 130.XX PCT Methionine, PAO Post-col Ninhydrin Der Methionine, PAO Pre-col OPA Der Methionine, PAO Post-col OPA Der Methionine, PAO Pre-col AQC Der Methionine, Misc Method Group 131.XX PCT Phenylalanine, Post-col Ninhydrin Der Phenylalanine, Pre-col AQC Der Method Group 132.XX PCT Proline, Post-col Ninhydrin Der Proline, Pre-col AQC Der Method Group 133.XX PCT Serine, Post-col Ninhydrin Der Serine, Pre-col AQC Der Method Group 134.XX PCT Threonine, Post-col Ninhydrin Der Threonine, Pre-col AQC Der Method Group 135.XX PCT Tryptophan, Alka-Hydrol Post-col Ninhyd Tryptophan, Alka-Hydrol Rev Phase LC UV Tryptophan, Misc Method Group 136.XX PCT Tyrosine, Post-col Ninhydrin Der Method Group 137.XX PCT Valine, Post-col Ninhydrin Der Valine, Pre-col AQC Der Method Group 138.XX PCT Taurine, Post-col Ninhydrin Der Sample July 26, 2009 Page 7

8 -- Method Method Method Avg Method s Avg R Method Avg Method Method Method Avg R R s s s Method Avg Method s R Avg Method S Avg Method Method Avg Method Avg Method Avg Method R Avg Method Method s s s R Sample July 26, 2009 Page 8

9 -- Method Avg Method Method R R R A A s s Method Avg S Method s R Method Avg s Method S S S Avg Method Avg S Method S S S S S R Avg R A Method Method s Sample July 26, 2009 Page 9

10 -- Method Avg s s s Method Avg Method R Method s A Avg s s Method Avg S Method Avg Method Avg Method s R Method Avg Method Avg R S S Method s s R Method Avg R Method S 3.31 Avg Method Avg Method R Sample July 26, 2009 Page 10

11 -- Method Avg R Method s Method Avg Method Avg Method Method s Avg Method s s R R R R R Method Method Avg R Sample July 26, 2009 Page 11

12 -- Method R R R R R Method Method S S Avg S S Method s Avg Method Method Method R Avg Method Method s X R Avg Method Method Avg S Method S Method Avg Method s Avg Method Method Avg Method S Avg S Method Avg s Sample July 26, 2009 Page 12

13 -- Method Avg s Method s s R R R Method Avg Method R R s Method Avg Method Avg Method Method Avg Method Avg Method S Method Avg Method s Method Avg Method Avg S Method Avg Sample July 26, 2009 Page 13

14 -- Method Avg Method Avg Method s s Avg Method Method Avg Method Method Method Avg Method R Avg R s Method s Method R Avg R R S Method Avg Method R Avg Method s Method Avg Method Sample July 26, 2009 Page 14

15 -- Method Avg R R Method S S S Avg Method Method Avg Method Method S Avg Method S Avg Method Avg Method Method s R R Avg s Method s s s S Method Avg R Method s s S A R R Method Avg s Method Avg Method Method s Sample July 26, 2009 Page 15

16 -- Method Avg s Method s R R Avg Method s Method R Avg Method s Method Avg Method Method Method s Avg Method Method s Avg R Method s Method Avg R R Method S Avg Sample July 26, 2009 Page 16

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