NUSRAT HUSSAIN/DR.IQBAL/NH-ST-1 1H
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1 Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2018
2
3 EXPNO 1 Date_ Time PROBHD 5 mm CPTCI - PULPROG zg30 TD NS 32 DS Hz Hz sec RG usec K sec TD0 1 W O MHz SI MHz W EM LB 0.50 Hz PC ppm
4 BB ppm EXPNO 6 Date_ Time 8.32 PROBHD 5 mm CPTCI - PULPROG zgpg TD NS 7314 DS Hz Hz sec RG usec K sec sec TD C usec db W W O MHz ======== CHANNEL f2 ======== CPDPRG[2 waltz16 NUC2 PCPD usec PL db PL2W 2W W 3W W O MHz SI MHz W EM LB 1.00 Hz PC 1.00
5 deptsp135 EXPNO ppm Date_ Time PROBHD 5 mm CPTCI - PULPROG deptsp135 TD NS 823 DS Hz Hz sec RG usec K CNST sec D sec sec TD0 6 13C usec usec PL db db PL0W 0 W W W O MHz SP db SPNAM[2] Crp60comp.4 SPOAL SPOFFS2 0 Hz ======== CHANNEL f2 ======== CPDPRG[2 waltz16 NUC2 P3 P usec PCPD usec PL2 2 2 PL2W 2W W O MHz SI MHz W EM LB 0.50 Hz PC 1.40
6 deptsp 90 EXPNO ppm Date_ Time PROBHD 5 mm CPTCI - PULPROG deptsp90 TD NS 240 DS Hz Hz sec RG usec K CNST sec D sec sec TD0 4 13C usec usec PL db db PL0W 0 W W W O MHz SP db SPNAM[2] Crp60comp.4 SPOAL SPOFFS2 0 Hz ======== CHANNEL f2 ======== CPDPRG[2 waltz16 NUC2 P3 P usec PCPD usec PL2 2 2 PL2W 2W W O MHz SI MHz W EM LB 0.50 Hz PC 1.40
7 hsqc ppm ppm EXPNO 4 Date_ Time PROBHD 5 mm CPTCI - PULPROG hsqcetgpsi TD 1024 NS 32 DS Hz Hz sec RG usec K CNST D sec sec D sec sec sec sec D sec IN sec ZGOPTNS P usec P usec W O MHz ======== CHANNEL f2 ======== CPDPRG[2 garp NUC2 13C P usec P usec PCPD usec PL db db PL2W W 2W W O MHz ====== GRADIENT CHANNEL ===== GPNAM[1] SINE.100 GPNAM[2] SINE.100 GPZ % GPZ % usec F1 - Acquisition parameters TD 256 O MHz Hz SW ppm FnMO Echo-Antiecho MHz W PC 4.00 F1 - Processing parameters MC2 echo-antiecho MHz W
8 hmbc ppm ppm EXPNO 5 Date_ Time 2.33 PROBHD 5 mm CPTCI - PULPROG hmbcgplpndqf TD 2048 NS 32 DS Hz Hz sec RG usec K CNST CNST D sec sec D sec D sec sec IN sec P usec W O MHz ======== CHANNEL f2 ======== NUC2 13C P usec PL db PL2W W O MHz ====== GRADIENT CHANNEL ===== GPNAM[1] SINE.100 GPNAM[2] SINE.100 GPNAM[3] SINE.100 GPZ % GPZ % GPZ % usec F1 - Acquisition parameters TD 256 O MHz Hz SW ppm FnMO QF SI MHz W SINE PC 4.00 F1 - Processing parameters MC2 QF MHz W SINE
9 cosy ppm ppm EXPNO 2 Date_ Time PROBHD 5 mm CPTCI - PULPROG cosydfqf TD 2048 NS 8 DS Hz Hz sec RG usec K D sec sec sec D sec IN sec W O MHz F1 - Acquisition parameters TD 128 O MHz Hz SW ppm FnMO QF MHz W PC 4.00 F1 - Processing parameters MC2 QF MHz W
10
11 Rabia / Dr. Iqbal / NH-ST-1 / C3D6O NOESY ppm ppm NAME COM EXPNO 3 Date_ Time PROBHD 5 mm PATXI / PULPROG noesygpph TD 1024 Acetone NS 32 DS Hz Hz sec RG usec K D sec sec D sec sec IN sec 7.24 usec P usec 0 db W W O MHz ====== GRADIENT CHANNEL ===== GPNAM[1] SINE.100 GPNAM[2] SINE.100 GPZ % GPZ % usec F1 - Acquisition parameters TD 256 O MHz Hz SW ppm FnMO States-TPPI MHz W PC 1.40 F1 - Processing parameters MC2 States-TPPI MHz W
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