Agilent 3396 Series III Integrator

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1 Agilent 3396 Series III Integrator Operating Manual Agilent Technologies

2 Agilent 3395/3396 Integrators Manuals These manuals may contain references to HP or Hewlett-Packard. Please note that Hewlett-Packard s former test and measurement, semiconductor products and chemicals analysis businesses are now part of Agilent Technologies. The HP 3395/3396 Integrator referred to throughout this document is now the Agilent 3395/3396 Integrator.

18 * LIST:

19 *HELP ANALYZE ASSIGN BASIC BX COPY CREATE DATE * > * * # * TIME.5 CHT SP

20 * LIST: CHT SP = 1.0

22 * DATR E 4/14/95 = DATE 4/14/95 INVALID SYSTEM COMMAND *

30 * REPORT RUN# 65 OCT 5, :01:32 SIGNAL FILE: M:SIGNAL.BNC TECH PROPIONIC ACID SAMPLE# 7 [CTRL D] * REPORT RUN# 65 OCT 5, :01:32 SIGNAL FILE: M:SIGNAL.BNC TECH PROPIONIC ACID SAMPLE# 7

31 * OP # 5 PRINT & POST-RUN LIST OPTIONS Large font [Y*/N]:

34 * DATE 3/28/95 MAR 28, :00:20 * TIME 08:35:30 MAR 28, :35:30

35 * PLOT STOP

36 * RUN # 1 MAR 28, :46:51 START STOP

37 START :

38 INTEGRATION PLOT TYPE (Source/Filtered/Unigram/No Plot) ENTER PLOT TYPE [S/F*/U/N]: * * Source Plot Filtered Plot Unigram Plot

39 No Plot INTEGRATION PLOT TYPE (Source/Filtered/Unigram/No Plot) ENTER PLOT TYPE [S/F*/U/N]: Presentation plot [Y/N*]:

40 * LIST: ZERO = 0, * ZERO START

42 * ATT 2^ START * ATT 2^ START

43 * CHT SP * CHT SP

45 *

46 * OP # 5 PRINT & POST-RUN LIST OPTIONS Large font [Y*/N]: Store post-run report [Y/N*]: External post-run report [Y/N*]: List run parameters [Y/N*]: List timetable [Y/N*]: List calibration [Y/N*]: List remote method [Y/N*]: Form-feed before report [Y/N*]: Form-feed after report [Y/N*]: Skip perforations in report [Y/N*]: Skip perforations in plot [Y/N*]:

47 ZE ^ZE AT CS PW TH AR IF EX ST

48 * TIME.5 CHT SP * LIST: CHT SP = 7.0

49 * EDIT METH 1 = RUN PARAMETERS 2 = TIMETABLE EVENTS 3 = CALIBRATION FILE SECTION TO BE EDITED: TIMETABLE EVENTS SELECT EVENTS FROM THE FOLLOWING MENU: [IF/EX/ZE/^Z/AT/CS/AR/TH/PW/ST] TIME: EVENT: VALUE:

50 * LIST: INTG # = AR REJ = CHT SP = INTG # = INTG # = 8 * DELETE TIME INTG # * LIST: AR REJ = CHT SP = 7.0 EMPTY

51 * LIST: AR REJ = 66 * TIME.032 AR REJ * LIST: AR REJ = 100

55 * LIST: LIST PEAK CAPACITY: 1244 ZERO = 0, ATT 2^ = 0 CHT SP = 1.0 AR REJ = 0 THRSH = 0 PK WD = 0.04 * LIST: PK WD = 0.01

57 * PK

58 * TIME 1.00 PK

59 * TIME 1.00 PK * TIME 1.01 PK

60 * THRSH

61 * AR REJ

63 IF IF

64 * TIME.3 INTG # * TIME.55 INTG # IF IF 0.574

65 * LIST: INTG # = INTG # = INTG # = 5

66 Error storing signal; FILE ALREADY OPEN

68 INVALID MUTE HOST CONVERSATION

69 * OP # 4 REPORT OPTIONS Suppress local report [Y/N*]: * OP # 7 DEFAULT SAMPLE INFORMATION USE SAMPLE TABLE IN MANUAL RUN [Y/N*]: ISTD AMT [0.0000E+00 ]: SAMPLE AMT [0.0000E+00 ]: MUL FACTOR [1.0000E+00 ]:

70 * OP # 4 REPORT OPTIONS Suppress local report [Y/N*]: * PREP E = EXTERNAL STANDARD I = INTERNAL STANDARD N = NORMALIZATION CALIB PROCEDURE [E*/I/N]: REF % RTW [ 5.000]: NON-REF % RTW [ 5.000]: RF BASED ON AREA OR HEIGHT [A*/H]: CAL# RT AMT NAME 1 :

73 4 UnderstandingHow the Integrator Integrates 4-2 Data Acceptance 4-4 Data Preparation 4-5 Peak Recognition 4-8 Optimizing Peak Recognition 4-12 Peak Measurement 4-17 ChromatographicBaselineConstruction 4-19 BaselineCorrections 4-26 Peak Data Storage 4-27 The Integration FunctionDescriptions 4-28 Understanding Integration

81 ÇÇÉÉÉ ÇÇÉÉÉÇÇ ÇÇÉÉÉÇÇ ÇÇÉÉÉÇÇ ÇÇÉÉÉÇÇ

89 ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉ ÉÉÉ

92 É ÉÉ ÉÉ ÉÉ ÉÉ

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110 É ÉÉ ÉÉ ÉÉÉ ÉÉÉ ÉÉÉ ÉÉÉ

111 É ÉÉ ÉÉ ÉÉÉ É ÉÉÉ ÉÉÉ ÉÉÉ ÉÉÉ ÉÉÉÉÉÉ É É ÉÉ ÉÉ ÉÉÉ ÉÉÉ ÉÉÉ

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125 ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁ ÁÁÁÁ ÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁ ÁÁÁÁ ÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁ ÁÁÁÁ ÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁ ÁÁÁÁ ÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁ

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127 Single level calibration

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132 Point-to-point

133 Linear Non-linear (quadratic)

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137 RUN #10 July 5, :47:06 METHOD NAME: SIGNAL FILE: M:NORM.MET L:Q8A4A08E.BNC AREA % ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ RT AREA TYPE WIDTH AREA% ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ.250 ÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ.134 ÁÁÁÁ ÁÁÁÁ.750 ÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ.134 ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ.134 ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ PB.134 TOTAL AREA= MUL FACTOR= E

138 E = EXTERNAL STANDARD I = INTERNAL STANDARD N = NORMALIZATION CALIB PROCEDURE [E*/I/N] REF % RTW [5.000] NON-REF % RTW [5.000] RF BASED ON AREA OR HEIGHT [A*/H] ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ CAL # ÁÁÁÁÁÁÁÁ RT ÁÁÁÁÁÁÁÁ AMT ÁÁÁÁÁÁÁÁ NAME* ÁÁÁÁ 1 ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁ 2 ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁ 3 ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁ 4 ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁ 5 ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ

139 REF PK CAL #: REF PK CAL #: REF PK CAL #: GROUP PEAKS [Y/N*]: RF of Uncalibrated Peaks [0.0000E+00]: Replace calibration fit [Y/N*]: Disable post-run RT update [Y/N*]: SAMPLE AMT [0.0000E+00]: MUL FACTOR [1.0000E+00]:

140 RUN #139 July 5, :12:06 METHOD NAME: SIGNAL FILE: M:SAVEL.MET L:Q8A4A857.BNC NORM-AREA ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ RT AREA TYPE CAL# AMOUNT ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ.249 ÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ 1R ÁÁÁÁÁ ÁÁÁÁ.749 ÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ 2 ÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁ 3139 ÁÁÁÁÁ BB ÁÁÁÁÁ 3R ÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ PB TOTAL AREA= MUL FACTOR= E00

141

142 RUN #10 July 5, :47:06 METHOD NAME: SIGNAL FILE: M:ESTD.MET L:Q8A4A08E.BNC AREA % ÁÁÁÁ RT ÁÁÁÁÁ AREA ÁÁÁÁÁ TYPE ÁÁÁÁÁ WIDTH ÁÁÁÁ AREA% ÁÁÁÁ.250 ÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ.134 ÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁÁ BB ÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ PB.134 TOTAL AREA= MUL FACTOR=1.0000E E = EXTERNAL STANDARD I = INTERNAL STANDARD N = NORMALIZATION CALIB PROCEDURE [E*/I/N] REF % RTW [5.000] NON-REF % RTW [5.000] RF BASED ON AREA OR HEIGHT [A*/H]

143 ÁÁÁÁÁ CAL # ÁÁÁÁÁÁÁÁ RT ÁÁÁÁÁÁÁÁ AMT* ÁÁÁÁÁÁÁÁ NAME** ÁÁÁÁÁ 1 ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ 2 ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁ 3 ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁ ÁÁÁÁÁ 4 ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ GROUP PEAKS [Y/N*]: RF of Uncalibrated Peaks [0.0000E+00] Replace calibration fit [Y/N*]:

144 P = point-to-point L = linear N = non-linear (quadratic) Calibration fit [N/L/P*]: Disable post-run RT update [Y/N*]: SAMPLE AMT [0.0000E+00]: ISTD AMT MUL FACTOR [1.000E+00]:

145 RUN #10 July 5, :47:06 METHOD NAME: SIGNAL FILE: M:ESTD.MET L:Q8A4A68E.BNC ESTD - AREA ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ RT AREA TYPE CAL # NG* ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ.250 ÁÁÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ 1 ÁÁÁÁÁÁÁ ÁÁÁÁ.750 ÁÁÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ 2 ÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ PB ÁÁÁÁÁ 3R ÁÁÁÁÁÁÁ TOTAL AREA= MUL FACTOR=1.0000E+00

146 RUN #11 July 5, :47:06 METHOD NAME: SIGNAL FILE: M:ESTD.MET L:Q8A4A68E.BNC ESTD - AREA ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ RT AREA TYPE CAL # NG* ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ.250 ÁÁÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ 1 ÁÁÁÁÁÁÁ ÁÁÁÁ.750 ÁÁÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ 2 ÁÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁ PB ÁÁÁÁÁ 3R ÁÁÁÁÁÁÁ TOTAL AREA= MUL FACTOR=1.0000E+00 ÁÁÁÁ CAL # ÁÁÁÁÁÁ RT ÁÁÁÁÁÁÁÁÁÁÁ AMT ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ 3 ÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ

147 ESTD REF % RTW: NON-REF % RTW: LEVEL: 1 RECALIBRATIONS: 1 LEVEL: 2 RECALIBRATIONS: 1 ÁÁÁÁ CAL # ÁÁÁÁÁÁ RT ÁÁÁÁ LV ÁÁÁÁÁÁÁ AMT ÁÁÁÁÁÁÁ AMT/AREA ÁÁÁÁ 1R ÁÁÁÁÁÁ ÁÁÁÁ 1 ÁÁÁÁÁÁÁ E+02 ÁÁÁÁÁÁÁ E-05 ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ E E-05 ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ E E-03 ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁ ÁÁÁÁ 2 ÁÁÁÁÁÁÁ E+02 ÁÁÁÁÁÁÁ E-03 ÁÁÁÁ 3 ÁÁÁÁÁÁ ÁÁÁÁ 1 ÁÁÁÁÁÁÁ E+02 ÁÁÁÁÁÁÁ E-05 ÁÁÁÁÁÁÁÁÁÁÁÁ 2 ÁÁÁÁÁÁÁ E+02 ÁÁÁÁÁÁÁ E-05

148 RUN #12 July 5, :18:00 METHOD NAME: SIGNAL FILE: M:estd.MET L:Q8B3939E.BNC ESTD-AREA ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ RT AREA TYPE CAL# NG ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁ.249 ÁÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ 1R ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ 2 ÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ 3 ÁÁÁÁÁÁÁ TOTAL AREA= MUL FACTOR=1.0000E+00

149 ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁ CAL # ÁÁÁÁÁ RT ÁÁÁÁÁÁÁÁÁÁÁ AMT ÁÁÁÁÁÁ 1 ÁÁÁÁÁ.249 ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁ 2 ÁÁÁÁÁ.749 ÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ

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151 RUN #1 July 25, :07:06 METHOD NAME: SIGNAL FILE: M:IST.MET L:Q8A4A19E.BNC AREA % ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ RT AREA TYPE WIDTH AREA% ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ.250 ÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ.134 ÁÁÁÁ ÁÁÁÁ.750 ÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ.134 ÁÁÁÁ ÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁ PB.134 ÁÁÁÁ TOTAL AREA:= MUL FACTOR=1.00E+00 E = EXTERNAL STANDARD I = INTERNAL STANDARD N = NORMALIZATION CALIB PROCEDURE [E*/I/N] REF % RTW [5.000] NON-REF % RTW [5.000] RF BASED ON AREA OR HEIGHT [A*/H] ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ CAL # ÁÁÁÁÁÁÁÁ RT ÁÁÁÁÁÁ AMT ÁÁÁÁÁÁÁÁÁÁ NAME ÁÁÁÁ 1 ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ 4 ÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ 7

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153 REF PK CAL #: REF PK CAL #: ISTD CAL #: GROUP PEAKS [Y/N*]: RF of Uncalibrated Peaks [0.0000E+00]: Replace calibration fit [Y/N*]: P = point-to-point L = linear N = non-linear (quadratic) Calibration fit [N/L/P*]: Disable post-run RT update [Y/N*]:

154 SAMPLE AMT [0.0000E+00]: ISTD AMT MUL FACTOR [1.000E+00]: Run # 1 Jul 25, :07:06 METHOD NAME: SIGNAL FILE: M:IST.MET L:Q8A419E.BNC ISTD-AREA ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ RT ÁÁÁÁÁ AREA ÁÁÁÁÁ TYPE ÁÁÁÁÁ CAL # ÁÁÁÁÁÁ AMOUNT ÁÁÁÁ.249 ÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ 1& ÁÁÁÁÁÁ ÁÁÁÁ.749 ÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ 2 ÁÁÁÁÁÁ TOTAL AREA= MUL FACTOR=1.0000E+00 ISTD AMT= E+00

155 Run # 2 Jul 25, :51:42 METHOD NAME: SIGNAL FILE: M:IST.MET L:Q8A710BC ISTD-AREA ÁÁÁÁ RT ÁÁÁÁÁ AREA ÁÁÁÁÁ TYPE ÁÁÁÁÁ CAL # ÁÁÁÁÁÁ AMOUNT ÁÁÁÁ.249 ÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ 1&* ÁÁÁÁÁÁ ÁÁÁÁ.749 ÁÁÁÁÁ TOTAL AREA= ÁÁÁÁÁ BB 2 MUL FACTOR=1.0000E+00 ISTD AMT= E+00 ÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ CAL # LEVEL AMT ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ 1 2

156 Run # 4 Jul 25, :45:42 METHOD NAME: SIGNAL FILE: M:IST.MET L:Q8A608BC ISTD-AREA ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ RT AREA TYPE CAL # AMOUNT ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ.249 ÁÁÁÁÁÁ ÁÁÁÁÁÁ BB ÁÁÁÁÁ 1& ÁÁÁÁÁÁ ÁÁÁÁ.749 ÁÁÁÁÁÁ ÁÁÁÁÁÁ BB ÁÁÁÁÁ 2 ÁÁÁÁÁÁ TOTAL AREA= MUL FACTOR=1.0000E+00 ISTD AMT= E+00 Run # 5 Jul 25, :01:42 METHOD NAME: SIGNAL FILE: M:IST.MET L:Q8A608BC ISTD-AREA ÁÁÁÁ RT ÁÁÁÁÁ AREA ÁÁÁÁÁ TYPE ÁÁÁÁÁ CAL # ÁÁÁÁÁÁ AMOUNT ÁÁÁÁÁÁÁÁ ÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁ BB 1& ÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ.749 TOTAL AREA= ÁÁÁÁÁ BB 2 MUL FACTOR=1.0000E+00 ISTD AMT= E

157 Run # 6 Jul 25, :15:42 METHOD NAME: SIGNAL FILE: M:IST.MET L:Q8A608BC ISTD-AREA ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ RT ÁÁÁÁÁ AREA ÁÁÁÁÁ TYPE ÁÁÁÁÁ CAL # ÁÁÁÁÁÁ AMOUNT ÁÁÁÁ.249 ÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ 1& ÁÁÁÁÁÁ ÁÁÁÁ.749 ÁÁÁÁÁ ÁÁÁÁÁ BB ÁÁÁÁÁ 2 ÁÁÁÁÁÁ TOTAL AREA= MUL FACTOR=1.0000E+00 ISTD AMT= E+00

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161 NO RUN PEAKS STORED. CALIB EXISTS E = EXTERNAL STANDARD I = INTERNAL STANDARD N = NORMALIZATION CALIB PROCEDURE (E*/I/N):

162 E REF % RTW [5.000]: REF % RTW [ 5.000]:

163 ÈÈÈ ÈÈÈ ÈÈÈ ÈÈÈ NON-REF % RTW [ 5.000]: RF BASED ON AREA OR HEIGHT [A*/H]: CAL# RT AMT NAME 1 :

164 CAL# RT AMT NAME 1 :.082 :10 : S1 2 :.173 :5 : S2 3 :.498 NO MATCH S REF PK CAL#: ISTD CAL#:

165 GROUP PEAKS [Y/N*]: CALIBRATION OPTIONS GRP# CAL# NAME 1 : NAME GRP# CAL# NAME 1 :7,9,10 :BUTENE

166 CALIBRATION OPTIONS RF of uncalibrated peaks [0.0000E+00 ]: Replace calibration fit [Y/N*]: Disable post-run RT update [Y/N*]: ISTD AMT [0.0000E+00 ]: SAMPLE AMT [0.0000E+00 ]: MUL FACTOR [1.0000E+00 ]: ISTD AMT SAMPLE AMT MUL FACTOR SAMPLE AMT MUL FACTOR

167 MUL FACTOR MUL FACTOR

168 CALIBRATION OPTIONS RF of uncalibrated peaks [0.0000E+00 ]: Replace calibration fit [Y/N*]: P = point-to-point L = linear N = non-linear (quadratic) Calibration fit [N/L/P*]:

169 Point-to-point Linear Non-linear (quadratic)

170 CAL# RT AMT 1 : rr.rrr :

171

172

173 AMT/AREA AMT/HEIGHT

174 * EDIT CALIB 1 = CALIB PROCEDURE 2 = RETENTION TIME WINDOWS 3 = TABLE ENTRIES 4 = PEAK GROUPS 5 = CALIB options SECTION TO BE EDITED:

175 * OP() CALIBRATION OPTIONS RF of uncalibrated peaks [0.0000E+00 ]: Replace calibration fit [Y/N*]: P = point-to-point L = linear (least square) N = non-linear (quadratic) Calibration fit [N/L/P*]: Disable post-run RT update [Y/N*]: ISTD peak #: ISTD AMT [1.0000E+00 ]: SAMPLE AMT [0.0000E+00 ]: MUL FACTOR [1.0000E+00 ]: Replace calibration fit Calibration fit ISTD peak # ISTD CAL#

176 NO CALIB TBL. * LIST: CALIB ISTD REF % RTW: NON-REF % RTW: LEVEL: 1 RECALIBRATIONS: 1 CAL# RT LV AMT AMT/AREA 1& E E CAL# 1 NAME CALIBRATION options RF of uncalibrated peaks E+00 Calibration fit... P Disable post-run RT update.. NO ISTD peak #... 1 ISTD AMT... 1 SAMPLE AMT E+00 MUL FACTOR E+00

177 DELETE ALL [Y/N*]: * DELETE CALIB

178 * EDIT CALIB 1 = CALIB PROCEDURE 2 = RETENTION TIME WINDOWS 3 = TABLE ENTRIES 4 = PEAK GROUPS 5 = CALIB OPTIONS SECTION TO BE EDITED: CAL#:

179

180 * OP() DEFAULT SAMPLE INFORMATION USE SAMPLE TABLE IN MANUAL RUN [Y/N*]: ISTD AMT [0.0000E+00 ]: SAMPLE AMT [0.0000E+00 ]: MUL FACTOR [1.0000E+00 ]: RECALIBRATION [Y/N*]:

181 LEVEL [0 ]: NAME: REPORT MEMO:

182 * OP # 7 * LIST: OP # 7 DEFAULT SAMPLE INFORMATION USE SAMPLE TABLE IN MANUAL RUN ISTD AMT SAMPLE AMT MUL FACTOR RECALIBRATION NO E E E+00 NO SAMPLE NAME REPORT MEMO

183

184

185

186

187

188

189

190

191

192

193

194

195

196

197

198

199 ÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁ ADDRESS DEVICE ID ÁÁÁÁÁÁÁÁÁÁÁ ACCESSORY ID & CLASS ÁÁÁÁ 8 ÁÁÁÁÁÁÁÁÁÁÁÁ HP82169A ÁÁÁÁÁÁÁÁÁÁÁ 43H INTERFACE ÁÁÁÁ 1 7 ÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁ RESERVED FOR HPIB DEVICES ÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ SLOT1 ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ 2MB-SRAM ÁÁÁÁ SLOT2 512KB-FLASH ÁÁÁÁÁÁ DISC NAME ÁÁÁÁÁÁ ADDRESS ÁÁÁÁÁ DRIVE# ÁÁÁÁÁÁÁ VOLUME ID ÁÁÁÁÁ MEDIA ÁÁÁÁÁÁ A ÁÁÁÁÁÁ 7 ÁÁÁÁÁÁÁÁÁÁÁ EPA1 ÁÁÁÁÁ ÁÁÁÁÁÁ B ÁÁÁÁÁÁ 7 ÁÁÁÁÁÁÁÁÁÁÁ WATER ÁÁÁÁÁ ÁÁÁÁÁÁ C ÁÁÁÁÁÁ SLOT1 ÁÁÁÁÁÁÁÁÁÁÁ CLWAT ÁÁÁÁÁ FLASH ÁÁÁÁÁÁ D ÁÁÁÁÁÁ SLOT1 ÁÁÁÁÁÁÁÁÁÁÁ METHOD ÁÁÁÁÁ FLASH ÁÁÁÁÁÁ F ÁÁÁÁÁÁ SLOT1 ÁÁÁÁÁÁÁÁÁÁÁ AUG ÁÁÁÁÁ FLASH ÁÁÁÁÁÁ G ÁÁÁÁÁÁ SLOT1 ÁÁÁÁÁÁÁÁÁÁÁ SAVE ÁÁÁÁÁ FLASH ÁÁÁÁÁÁ I ÁÁÁÁÁÁ SLOT2 ÁÁÁÁÁÁÁÁÁÁÁ TEMP ÁÁÁÁÁ SRAM ÁÁÁÁÁÁ ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ J SLOT2 RS-232-C SWITCH SETTINGS Baud 4800 TEMP2 SRAM Timeout Handshake Delay Hardware Handshake 15 sec Disabled Enabled

200

201 ADDRESSÁÁÁÁÁÁÁÁÁÁÁÁ DEVICE ID ÁÁÁÁÁÁÁÁÁÁÁ ACCESSORY ID & CLASS ÁÁÁÁ 8 ÁÁÁÁÁÁÁÁÁÁÁÁ HP82169A ÁÁÁÁÁÁÁÁÁÁÁ 43H INTERFACE ÁÁÁÁ 1 7 ÁÁÁÁÁÁÁÁÁÁÁÁ RESERVED FOR HPIB DEVICESÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ SLOT1 ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ 2MB-SRAM ÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁÁ ÁÁÁÁ SLOT2 512KB-FLASH ÁÁÁÁÁÁ DISC NAME ÁÁÁÁÁÁ ADDRESS ÁÁÁÁÁ DRIVE# ÁÁÁÁÁÁÁ VOLUME ID ÁÁÁÁÁ MEDIA ÁÁÁÁÁÁ A ÁÁÁÁÁÁ SLOT1 ÁÁÁÁÁÁÁÁÁÁÁ CLWAT ÁÁÁÁÁ FLASH ÁÁÁÁÁÁ B ÁÁÁÁÁÁ SLOT1 ÁÁÁÁÁÁÁÁÁÁÁ METHOD ÁÁÁÁÁ FLASH ÁÁÁÁÁÁ C ÁÁÁÁÁÁ SLOT1 ÁÁÁÁÁÁÁÁÁÁÁ AUG ÁÁÁÁÁ FLASH ÁÁÁÁÁÁ D ÁÁÁÁÁÁ SLOT1 ÁÁÁÁÁÁÁÁÁÁÁ SAVE ÁÁÁÁÁ FLASH ÁÁÁÁÁÁ F ÁÁÁÁÁÁ SLOT2 ÁÁÁÁÁÁÁÁÁÁÁ TEMP ÁÁÁÁÁ SRAM ÁÁÁÁÁÁ G ÁÁÁÁÁÁ SLOT2 ÁÁÁÁÁÁÁÁÁÁÁ TEMP2 ÁÁÁÁÁ ÁÁÁÁÁÁ I ÁÁÁÁÁÁ 7 ÁÁÁÁÁÁÁÁÁÁÁ EPA1 ÁÁÁÁÁ ÁÁÁÁÁÁ J ÁÁÁÁÁÁ 7 ÁÁÁÁÁÁÁÁÁÁÁ WATER ÁÁÁÁÁ RS-232-C SWITCH SETTINGS Baud 4800 Timeout Handshake Delay Hardware Handshake 15 sec Disabled Enabled

202

203

204 FORMAT WANTS: DISK, NAME, MAX FILES, (S)

205 * *A:

206

207

208 * OP # 2 RUN DATA STORAGE Store signal data [Y/N* Device [M*]: Bunched or raw data [B/R*]:] Local run-time storage [Y/N*]: Keep run-time storage [Y/N*]: Store processed peaks [Y/N*]: * OP # 2 RUN DATA STORAGE Store signal data [Y/N* Device [M*]: M:SIGNAL.BNC

209 Bunched or raw data [B/R*]:

210 Store processed peaks Local run-time storage [Y/N*]: Copying signal file to host Keep run-time storage [Y/N*]: Deleting local signal file

211 Store processed peaks [Y/N*]:

212 * [STORE] [METH] C:METH20.MET * OP # 5 PRINT & POST-RUN LIST OPTIONS Large font [Y*/N]: Store post-run report [Y/N*]: Device [M*]:

213 *DI VOLUME NAME: MDISK DRIVE: M DATE: JAN 8, :20:13 FILE NAME LENGTH CREATED/VERSION SIG_BUFF.RAW /05/90 14:48:02 LU1.MET /03/90 18:04:45 PROG.BAS /05/90 15:07:35 USED FREE MAX FILES BYTES

214 FREE MAX FREE USED MAX LENGTH FREE MAX FREE USED MAX USED FREE MAX VOLUME NAME: ADisk DRIVE: A DATE: June 10, 1994 SRAM BATTERY SLOT 1 (OK, REPLACE, or DEAD)

215

216 SYSTEM CONFIGURATION ADDRESS DEVICE ID ACCESSORY ID & CLASS 8 HP6890A 71H INET 9 HP82169A 43H Interface 1 7 (Reserved for HPIB devices) SLOT1 SLOT2 1MB SRAM 1MB SRAM DISC NAME ADDRESS DRIVE # VOLUME ID MEDIA A B C SLOT1 0 TEMP SRAM D SLOT1 1 DDISK SRAM F SLOT1 2 FDISK SRAM G SLOT1 3 GDISK SRAM I SLOT1 4 IDISK SRAM J SLOT1 5 JDISK SRAM K SLOT1 6 KDISK SRAM L SLOT1 7 LDISK SRAM X SLOT2 0 XDISK SRAM Y SLOT2 1 YDISK SRAM RS 232 C SWITCH SETTINGS Baud 9600 Timeout 15 sec Handshake Delay Hardware Handshake Disabled Off *

217 *COPY M:CA1.CAL,A:CA1.CAL *RENAME M:SIGNAL.BNC,M:RUN5.BNC

218 *PURGE A:METH1.MET *PACK A:

219

220

221

222

223 * HEIGHT% report [Y/N*]: ENTER PLOT TYPE [S/F*/U/N]:

224 * PREP METH RUN PARAMETERS ZERO [ 0 ]: ATT 2^ [ 0 ]: CHT SP [ 1.0 ]: AR REJ [ 0 ]: THRSH [ 0 ]: PK WD [ 0.04 ]:

225 TIMETABLE EVENTS DELETE CURRENT TABLE [Y/N*]: TIMETABLE EVENTS SELECT EVENTS FROM THE FOLLOWING MENU [IF/EX/ZE/^Z/AT/CS/AR/TH/PW/ST] TIME: EVENT:

226 VALUE: TIME:

227 TIME:.30 EVENT: PW ] VALUE: 05 TIME: 8 [ EVENT: ST VALUE: TIME: 240 EVENT: EX VALUE: 3?

228 REPLACE CURRENT CALIBRATION [Y/N*]: CALIBRATION FILENAME: CALIBRATION FILENAME: CALIBRATION FILENAME:

229 INTEGRATION PLOT TYPE (Source/Filtered/Unigram/No Plot) ENTER PLOT TYPE [S/F*/U/N]: Presentation plot [Y/N*]: RUN DATA STORAGE Store signal data [Y/N*]:

230 Device [M*]: CAUTION: Previous signal data will be lost Bunched or raw data [B/R*]: Store processed peaks [Y/N*]: REPORT OPTIONS Suppress local report [Y/N*]: HEIGHT% report [Y/N*]: Replace report title [Y/N*]: Report title: Replace amount label [Y/N*]: Report uncalibrated peaks [Y/N*] Extended report [Y/N*]:

231 PRINT & POST-RUN LIST OPTIONS Large font [Y*/N]: Store post-run report [Y/N*]: Device [M*]: External post-run report [Y/N*]: List run parameters [Y/N*]: List time table [Y/N*]: List calibration table [Y/N*]: List remote method [Y/N*]: Form feed before report [Y/N*]: Form feed after report [Y/N*]: Skip perforations in report [Y/N*]:

232 C1 Range [5] Buffer Range [5] [ENTER] [ENTER]

233 [LIST] [OP()] 8 [ENTER] Range: C1, Buffer 4!4!

234 * STORE METH ATTEMPTED WRITE PAST END OF FILE. DISK FULL.

235 * LOAD METH INSTRUMENT AT ADDRESS 8 REJECTED SETPOINTS METH NOT CHANGED

236 * [LOAD] [METH] A: labmet1 INSTRUMENT AT ADDRESS 8 REJECTED PARAMETERS Back Det Type Mismatch ALS Back Tower Oven Max Mismatch Col Length

237 *[LOAD] [METH] A: labmet1 INSTRUMENT AT ADDRESS 8 REJECTED PARAMETERS Back Det Type Mismatch ALS Back Tower Oven Max Mismatch SHOULD ADDRESS 8 ADAPT PARAMETERS? [Y/N*] SHOULD ADDRESS 8 ADAPT PARAMETERS? [Y/N*] * N [ENTER] METH NOT CHANGED

238 * EDIT METH 1 = RUN PARAMETERS 2 = TIMETABLE EVENTS 3 = CALIBRATION FILE 4 = INTEGRATION PLOT TYPE 5 = RUN DATA STORAGE OPTIONS 6 = REPORT OPTIONS 7 = POST-RUN LIST OPTIONS 8 = REMOTE DEVICE ACCESS SECTION TO BE EDITED: SECTION TO BE EDITED:

239 REMOTE DEVICE ACCESS

240 FILE NOT FOUND.

241 DEVICE ADDRESS:

242 COMMAND STRING: DEVICE ADDRESS: COMMAND STRING: DEVICE ADDRESS:

243 * LIST METH RUN PARAMETERS ZERO = 0 ATT 2^ = 2 CHT SP = 1.0 AR REJ = 0 THRSH = 2 PK WD = 0.01 TIMETABLE EVENTS PK WD = STOP CALIBRATION NORM REF % RTW: NON-REF % RTW: LEVEL: 1 RECALIBRATIONS: 1 CAL# RT LV AMT AMT/HEIGHT 1R E E E E 06 3R E E E E 03 5R E E 04 CAL# NAME 1 PK1 2 PK2 3 PK3 4 PK4 5 PK5 GRP# CAL# NAME 1 2, 4, GRP1 2 3, 5, GRP2 3 4, 5, GRP3 4 2, 4, 5, GRP4 5 1, 3, 5, GRP3

244 INTEGRATION PLOT TYPE... FILTERED Presentation plot... NO RUN DATA STORAGE Store signal data... YES Device... M Bunched or raw data... BUNCHED Store processed peaks... NO CALIBRATION OPTIONS RF of uncalibrated peaks E+00 Calibration fit... P Disable post run RT update.. NO MUL FACTOR E+00 REPORT OPTIONS Suppress local report... NO Height% report... NO Report title: SLUDGE Amount label... GMS Report uncalibrated peaks... YES Extended report... YES PRINT & POST RUN LIST OPTIONS Large font... YES Store post run report... NO External post run report... NO List run parameters... YES List timetable... YES List calibration table... NO List remote method... NO Form feed before report... NO Form feed after report... NO Skip perforations in report. NO Skip perforations in plot... NO RANGE: C1,BUFFER...5!5! 19405B IECM CONTROL MODULE LOOP ADDRESS: 9

245 EXTERNAL EVENT TABLES NO AUTO RESET TIME TABLE: TIME EXT # STATE ON

246 * LIST METH HP 5890A GAS CHROMATOGRAPH LOOP ADDRESS: 8 OVEN TEMP = 204 SETPT = 204 EQUIB TIME = 0.00 CRYO OFF OVEN MAXIMUM = 400 INITIAL TEMP = 204 INITIAL TIME = RUN LENGTH = MIN INJ A TEMP = 50 SETPT = 50 INJ B TEMP = 50 SETPT = 50 DET A TEMP = 203 SETPT = 203 DET B TEMP = 207 SETPT = 207 SIGNAL 1 = A INET FULL RANGE DATA ON RANGE = 0 ZERO = 0.0 ATTN = 4 SIGNAL 2 = B RANGE = 0 ZERO = ATTN = 10 DETECTOR A = FID (ON) DETECTOR B = TCD (ON) POLARITY = + PURGE A = OFF PURGE B = ON List remote method

247 * DELETE METH

248

249

250 * LIST: RUN PARAMETERS ZERO = 0 ATT 2^ = 0 CHT SP = 1.0 AR REJ = 0 THRSH = 0 PK WD = 0.04 TIMETABLE EVENTS EMPTY CALIBRATION NO CALIB TBL INTEGRATION PLOT TYPE... FILTERED Presentation plot... NO RUN DATA STORAGE Store signal data... NO Store processed peaks... NO REPORT OPTIONS Suppress local report... NO HEIGHT% report... NO Report uncalibrated peaks... NO Extended report... NO PRINT & POST-RUN LIST OPTIONS Large font... YES Store post-run report... NO External post-run report... NO List run parameters... NO List timetable... NO List calibration table... NO List remote method... NO Form-feed before report... NO Form-feed after report... NO Skip perforations in report. NO Skip perforations in plot... NO RANGE: C1,BUFFER 5!5!

251

252

253

254

255

256

257

258

259 INET SAMPLER CONTROL [Y/N*] BOTTLE OR RUN SAMPLE INDEXED [R/B*]:

260 * [PREP] [SEQ] ALS INFORMATION INET SAMPLER CONTROL [Y/N*] Y [ENTER] 6890A GAS CHROMATOGRAPH: LOOP ADDRESS: 8 Sequence Type (1= FRONT ALS, 2=BACK ALS, 3=BOTH ALS, 4=VALVE) INJECTIONS PER VIAL: 1 > FIRST BOTTLE NUMBER: 1 > LAST BOTTLE NUMBER: 1 > (FRONT) INJECTIONS PER VIAL: 1 > (FRONT) FIRST BOTTLE NUMBER: 1 > (FRONT) LAST BOTTLE NUMBER: 1 >

261 (BACK) INJECTIONS PER VIAL: 1 > (BACK) FIRST BOTTLE NUMBER: 1 > (BACK) LAST BOTTLE NUMBER: 1 > # OF INJECTIONS: 1 > INJECTIONS PER POSITION: 1 > POSITION RANGE: 1 > TIMES THROUGH RANGE: 1 > Post Sequence GC Method # 0 > Repeat Sequence? 1 = Yes, 0 = No 0 > POSITION <1=FRONT, 2=REAR> INET CHANNEL 1 1 > [ENTER]

262 EQUILIBRATION TIME IN SECONDS [0] Delete Sample Table [Y/N*]: BOTTLE OR RUN SAMPLE INDEXED [R/B*]: INET SAMPLER CONTROL [Y*/N]:

263 FIRST BOTTLE [1 ]: FIRST RUN [1 ]: LAST BOTTLE [1 ]: LAST RUN [1 ]: BOTTLE # : RUN # : ISTD AMT: SAMPLE AMT: MUL FACTOR:

264 RECALIBRATION [Y/N*]: LEVEL: NAME REPORT MEMO BOTTLE #: RUN #:

265 NEXT SEQUENCE:[*] Caution: Cannot get sequence file.

266 MUL FACTOR SAMPLE AMT FIRST BOTTLE #LAST BOTTLE # INVALID SAMPLE NUMBER

267 * LIST: OP # 7 DEFAULT SAMPLE INFORMATION USE SAMPLE TABLE IN MANUAL RUN NO ISTD AMT E+00 SAMPLE AMT0.0000E+00 MUL FACTOR E+00 RECALIBRATION NO

268 FIRST BOTTLE # LAST BOTTLE # 7673A SAMPLER* LOOP ADDRESS: 9 INVALID BOTTLE NUMBER FIRST BOTTLE # LAST BOTTLE # LAST BOTTLE # INET SAMPLE CONTROL [Y/N*]:

269 5890 SERIES II GAS CHROMATOGRAPH LOOP ADDRESS: C AUTOMATIC SAMPLER LOOP ADDRESS: 9 ENABLE TRAY (1=YES, 2=NO) 1 > ENABLE BAR CODE 1 > FRONT INJECTOR INJ/BOTTLE 1 > FIRST BOTTLE 1 > LAST BOTTLE 1 > # OF SAMPLE WASHES 0 > # OF PUMPS 6 > VISCOSITY 0 > VOLUME 1 > # OF SOLVENT A WASHES 0 > # OF SOLVENT B WASHES 0 >

270 PRIORITY SAMPLE (1=YES) > CAPILLARY ON COLUMN 0 > REAR INJECTOR INJ/BOTTLE 1 > FIRST BOTTLE 1 > LAST BOTTLE 1 > # OF SAMPLE WASHES 0 > # OF PUMPS 6 > VISCOSITY 0 > VOLUME 1 > # OF SOLVENT A WASHES 0 > # OF SOLVENT B WASHES 0 > PRIORITY SAMPLE (1=YES) > CAPILLARY ON COLUMN 0 > POSITION (1=FRONT, 2=REAR) INET CHANNEL 1 1 > INET CHANNEL 2 1 > AUXILIARY CHANNEL 1 > EQUILIBRATION TIME IN SECONDS:

271

272

273 *PREP SEQ ALS INFORMATION INET SAMPLER CONTROL [Y/N*]: RUNS WAIT FOR START_INPUT: [Y/N*] REMOTE_START_RELAY: PRERUN/RUN [P/R*]

274 EQUILIBRATION TIME IN SECONDS [0]

275 REMOTE READY SENSING [C/S*]

276 BOTTLE # USE SAMPLE TABLE IN MANUAL RUN [Y/N*]:

277 *PREP SEQ ALS INFORMATION INET SAMPLER CONTROL [Y/N*]: RUN # FIRST RUN # LAST RUN # USE SAMPLE TABLE IN MANUAL RUN [Y/N*]: FIRST RUN #

278 * EDIT SEQ 1 = ALS INFORMATION 2 = EQUILIBRATION TIME DELAY 3 = METHOD FILE SPECIFICATION 4 = SAMPLE INFORMATION TABLE 5 = NEXT SEQUENCE SECTION TO BE EDITED: SAMPLE INFORMATION TABLE BOTTLE OR RUN NUMBER INDEXED [R/B*]: FIRST RUN [1 ]: LAST RUN [1 ]:... * OP # 7 DEFAULT SAMPLE INFORMATION USE SAMPLE TABLE IN MANUAL RUN [Y/N*]: ISTD AMT [1.0000E+O1 ]: *SET RUNNUM

279

280 10 START SEQ_LATER FIRST BOTTLE # RUN # LAST BOTTLE # RUN # FIRST RUN # LAST RUN # INVALID INDEX; ABORTED. WAITING FOR SYSTEM READINESS EQUILIBRATION DELAY IN PROGRESS FILE NOT FOUND NOT LOADED

281 DISC DOES NOT EXIST HPIL DOWN DISK FULL. PRESS I, S, R, STOP TO IGNORE, SUSPEND, RESUME, OR STOP

282

283 FILE NOT FOUND SEQ NOT CHANGED SEQ NOT CHANGED DEFAULT SEQ INVOKED

284

285 1 = ALS INFORMATION 2 = EQUILIBRATION TIME DELAY 3 = METHOD FILE SPECIFICATION 4 = SAMPLE INFORMATION TABLE 5 = NEXT SEQUENCE SECTION TO BE EDITED: BOTTLE # RUN #

286 RUN #:

287 FILE NOT FOUND * LIST: SEQ ALS INFORMATION INET SAMPLER CONTROL... NO RUNS WAIT FOR START_INPUT: [Y/N] Y REMOTE_START_RELAY: PRERUN/RUN [P/R*]...P EQUILIBRATION TIME IN SECONDS... 5 REMOTE READY SENSING...SEPARATE METHOD... METH1.MET SAMPLE INFORMATION TABLE BOTTLE OR RUN SAMPLE INDEXED... R FIRST RUN... 5 LAST RUN... 10

288 RUN #... 5 ISTD AMT E+00 SAMPLE AMT E+00 MUL FACTOR E+00 RECALIBRATION... NO NAME... GROUP A NEXT SEQUENCE... NEXT.SEQ

289

290

291 EX

292

293 * LIST: TIME EXT 19405B EVENT CONTROL MODULE LOOP ADDRESS: 9 EXTERNAL EVENT TABLES AUTO RESET: EXT # STATE 1 OFF 2 OFF 3 OFF 4 OFF 5 OFF 6 OFF 7 OFF 8 OFF EQUILIBRATION TIME 0.10 TIME TABLE TIME EXT # STATE OFF OFF ON ON OFF OFF OFF OFF

294 * EXT # * EXT # * TIME.1 EXT

295

296

297 * AREA% RUN# 65 OCT 5, :01:32 SAMPLE# 7 SIGNAL FILE: M:SIGNAL.BNC TECH PROPIONIC ACID AREA% RT AREA TYPE WIDTH AREA% PP PB PB SBB BV VB BB TOTAL AREA=1.4477E+07 MUL FACTOR=1.0000E+00

298 * LIST: OP # 4 REPORT OPTIONS Suppress local report..... HEIGHT% report Report uncalibrated peaks. Extended report NO NO NO NO

299 * AREA% * OP # 4 REPORT OPTIONS Suppress local report [Y/N*]: HEIGHT% report [Y/N*]: Replace report title [Y/N*]: RUN# 5 OCT 5, :01:32 SAMPLE# 5 SIGNAL FILE: M:SIGNAL.BNC PEAK FILE : M:Q1EBBE6F.PRO REPORT #5 HEIGHT% RT HEIGHT TYPE WIDTH HEIGHT% BB I BH TOTAL HEIGHT= MUL FACTOR=1.0000E+00

300

301

302 * OP # 4 REPORT OPTIONS Suppress local report [Y/N*]:

303 HEIGHT% report [Y/N*]: Replace report title [Y/N*]: Report title: Replace amount label [Y/N*]:

304 Report uncalibrated peaks [Y/N*]: Extended report [Y/N*]: RT TYPE AREA WIDTH HEIGHT CAL# AMOUNT NAME RT AREA TYPE CAL# AMOUNT

305 * OP # 5 PRINT & POST-RUN LIST OPTIONS Large font [Y*/N]: ] Store post-run report [Y/N*]: Device [M*]: External post-run report [Y/N*]:

306 Printer Address [0 ]: List run parameters [Y/N*]: List timetable [Y/N*]: EMPTY List calibration table [Y/*N]: List remote method [Y/*N]: Form-feed before report [Y/N*]:

307 Form-feed after report [Y/N*]: Skip perforations in report [Y/N*]: Skip perforations in plot [Y/N*]:

308 * (USE BREAK OR CONTROL Y TO END) Testing column conditioning; First pass-operator is Kate * BREAK * ID Flavors Lab1 * REPORT RUN# 19 FEB 18, :24:00 IDENTIFIER : Flavors Lab1

309 Store post-run report [Y/N*]: Device [M*]:

310

311 RUN# 7 JAN 15, :22:08 SAMPLE NAME: SAMPLE NAME REPORT MEMO IDENTIFIER: LAB1 GC3 SIGNAL FILE: M:SIGNAL.RAW REPORT FILE: M:Q1FE0F80.RPT REPORT TITLE ISTD PEAK NOT MATCHED SAMPLE# 90

312

313

314 MUL FACTOR WIDTH AREA% HEIGHT% WIDTH RUN# 65 JUL 5, :01:32 SIGNAL FILE: M:SIGNAL.BNC TECH PROPIONIC ACID SAMPLE# 7 ESTD AREA RT AREA TYPE CAL# AMOUNT BV VB BB.3R TOTAL AREA=1.4477E+07 MUL FACTOR=1.0000E+00

315

316 RUN# 65 JUL 5, :01:32 SIGNAL FILE: M:SIGNAL.BNC TECH PROPIONIC ACID SAMPLE# 7 ESTD AREA RT AREA TYPE CAL# AMOUNT BV VB BB.3R TOTAL AREA=1.4477E+07 MUL FACTOR=1.0000E+00 RUN# 65 JUL 5, :01:32 SIGNAL FILE: M:SIGNAL.BNC TECH PROPIONIC ACID SAMPLE# 7 ESTD AREA RT TYPE AREA WIDTH HEIGHT CAL# AMOUNT NAME.138 PP PB PB SBB BV PPA VB IBTA BB R BTA TOTAL AREA=1.4477E+07 MUL FACTOR=1.0000E+04

317

318 * RUN # 18 JAN 1, :53:11 START IF CS8@ : AT TIMETABLE STOP

319 TIMETABLE STOP

320

321

322

323

324

325

326

327

328

329

330

331

332 Agilent Technologies Agilent Technologies, Inc. 08/97 Part Number

Agilent 3395 Integrator

Agilent 3395 Integrator Operating Manual Agilent Technologies Agilent 3395/3396 Integrators Manuals These manuals may contain references to HP or Hewlett-Packard. Please note that Hewlett-Packard s former