MC Prochloraz, [phenyl- 14 C]- Lot A JH

Transcription

1

2 Prochloraz, [phenyl- 14 C]- Lot A JH A) All chromatograms were run using the HPLC method described on the Product Data Sheet. Concentrations and volumes: Standard solution concentration was 2. mg/ml. Prochloraz, [phenyl- 14 C]- concentration was 1 µci/ml. Volume of standard alone injection was 2. µl. Volume of Prochloraz, [phenyl- 14 C]- alone injection was 1. µl. Co-injection solution consisted of 1. µl Prochloraz, [phenyl- 14 C] µl standard. Volume of co-injection was 3. µl. Volume of blank injection was 1. µl. B) Mass spectrometry- Positive mode

3 /6/214 2: PM Chromatogram L:\int42176.PRM Lot A JH File : L:\int42176 File Created : /6/214 1:2:6 PM Origin : Acquired, Acquisition started 11/3/29 1::4 AM Acquired Date : 11/3/29 11::39 AM Method : Unit4-4minrun By : Administrator : Radiochemical trace of 14C material alone Created : 6/12/28 1:3 AM Modified : /6/214 2:14 PM Column : Detection : Radiochemical L:\ int Unit 4 Radio Result Table (Uncal - L:\int Unit 4 Radio) W Total

4 /6/214 2:13 PM Chromatogram L:\int42176.PRM Lot A JH File : L:\int42176 File Created : /6/214 1:2:6 PM Origin : Acquired, Acquisition started 11/3/29 1::4 AM Acquired Date : 11/3/29 11::39 AM Method : Unit4-4minrun By : Administrator : UV trace of 14C material alone Created : 6/12/28 1:3 AM Modified : /6/214 1:7 PM Column : Detection : UV 2nm 12 L:\ int Unit 4 UV Result Table (Uncal - L:\int Unit 4 UV) W Total

5 /6/214 2:17 PM Chromatogram L:\int42177.PRM Lot A JH File : L:\int42177 File Created : /6/214 1:2:7 PM Origin : Acquired, Acquisition started 11/3/29 11:3:26 AM Acquired Date : 11/3/29 12:1: PM Method : Unit4-4minrun By : Administrator : UV trace of standard material alone Created : 6/12/28 1:3 AM Modified : /6/214 2:16 PM Column : Detection : UV 2nm L:\ int Unit 4 UV Result Table (Uncal - L:\int Unit 4 UV) W Total

6 /6/214 2:21 PM Chromatogram L:\int42178.PRM Lot A JH File : L:\int42178 File Created : /6/214 1:2:7 PM Origin : Acquired, Acquisition started 11/3/29 12:37:2 PM Acquired Date : 11/3/29 1:17:1 PM Method : Unit4-4minrun By : Administrator : Radiochemical trace of 14C material co-injected with standard Created : 6/12/28 1:3 AM Modified : /6/214 2:21 PM Column : Detection : Radiochemical L:\ int Unit 4 Radio Result Table (Uncal - L:\int Unit 4 Radio) W Total

7 /6/214 2:21 PM Chromatogram L:\int42178.PRM Lot A JH File : L:\int42178 File Created : /6/214 1:2:7 PM Origin : Acquired, Acquisition started 11/3/29 12:37:2 PM Acquired Date : 11/3/29 1:17:1 PM Method : Unit4-4minrun By : Administrator : UV trace of 14C material co-injected with standard Created : 6/12/28 1:3 AM Modified : /6/214 2:2 PM Column : Detection : UV 2nm 6 L:\ int Unit 4 UV Result Table (Uncal - L:\int Unit 4 UV) W Total

8 /6/214 2:22 PM Chromatogram L:\int4217.PRM Lot A JH File : L:\int4217 File Created : /6/214 1:2:6 PM Origin : Acquired, Acquisition started 11/3/29 9:4:33 AM Acquired Date : 11/3/29 9:44:32 AM Method : Unit4-4minrun By : Administrator : UV trace of blank injection Created : 6/12/28 1:3 AM Modified : /6/214 2:3 PM Column : Detection : UV 2nm L:\ int Unit 4 UV Result Table (Uncal - L:\int Unit 4 UV) W No peak to report

9 C:\Xcalibur\data\MC JH 11/3/29 1:1:2 AM MC JH RT: NL: 4.11E9 TIC MS MC JH MC JH #1-387 RT: T: + c NSI Full ms [ ] = Intensity Relative (min) MC JH #1-387 RT: AV: 387 NL: 9.4E8 T: + c NSI Full ms [ ] MC JH #1-387 RT: AV: 387 NL: 9.4E8 T: + c NSI Full ms [ ]

10 C:\Xcalibur\data\PROCHLORAZ STD-MS 11/4/29 9:12:39 AM PROCHLORAZ STD RT: NL: 2.71E9 TIC MS PROCHLO RAZ STD-MS PROCHLORAZ STD-MS#1-188 RT:.1-2. AV: T: + c NSI Full ms [.-7.] = Intensity Relative (min) PROCHLORAZ STD-MS #1-188 RT:.1-2. AV: 188 NL:.6E8 T: + c NSI Full ms [.-7.] PROCHLORAZ STD-MS #1-188 RT:.1-2. AV: 188 NL:.6E8 T: + c NSI Full ms [.-7.]