Wir schaffen Wissen heute für morgen. Paul Scherrer Institut X10SA Partner Training Workshop 2014 (New) Features at X10SA
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1 Wir schaffen Wissen heute für morgen Paul Scherrer Institut X10SA Partner Training Workshop 2014 (New) Features at X10SA PSI, 1. April 2014
2 Major Developments Since Last Training (2009) Pilatus X10SA Monochromator Upgrade Cryoshutter D3 Endstation DA+, V1.0 New Microsocope Diffraction Based Alignment Discrete Helical Scan single photon detector faster energy changes remote sample anealing reliability, speed, precision new GUI ultra fast zoom and FPS raster scanning reduc radiation damage
3 SLS PX Beamlines Beamline X06SA X10SA X06DA Station / operation High resolution 2001 Micro-focussing Source U19 Undulator U19 Undulator 2.9T Superbend Energy range kev ( Å) kev kev Energy resolution 2 x 10-4 kev 2 x 10-4 kev 1.4 x 10-4 kev Flux (12.4 kev) >2 x ph/s 1.0 (0.3) x >2 x ph/s 5 x ph/s Focused beam 85 x 15 µm 2 25(15) x 10 µm 2 50 x 12 µm 2 80 x 60 µm 2 Beam divergency 0.35 x0.06 mrad x 0.3 mrad x 0.15 mrad x 0.3 mrad 2 Detector PILATUS 6M 25 Hz MAR225 PILATUS 6M 25 Hz PILATUS 2M 60 Hz Time / dataset min 5-10 min min 3-20 min Sample changer IRELEC CATS CATS CATS
4 Evolution of SLS PX Beamline Diffractometers X10SA X06SA X06DA
5 Motivation for the D3 project Make best developments available on all beamlines Full translations X, Y, Z for goniometer axes (X06DA) Move sample into X-ray and optical focus rather than refocus Retractable beam shaping apertures (X10SA K-box) Smaller variable beam, reduced background scatter Consolidate / improve previous developments Optimized on axis microscope Retractable small beamstop More space for sample-mounting, less broken beamstops Z Y ω Z Retraction X X06DA goniometer, Aerotech Crystal sizes 5µm Beam spots 50 x 10 µm 2, 80 x 45 µm 2 X06SA optics upgrade: Beam spot 1x1 µm 2
6 D3
7 SRI2012 Before Diffractometer
8 SRI2012 After Diffractometer
9 PRIGo Multi-axis Goniometer integration Parallel Robotics Inspired Goniometer Collision avoidance Potential collisions with lamp, microscope, beam shaping devices Integration studies during D3 construction phase Final modification to orion table required for integration
10 Beam Shaping Apertures D3 includes user-selectable beam shaping devices: 150 µm aperture: 50 x 12 µm beam 100% flux 30 µm aperture: 33 x 12 µm beam ~40% flux 10 µm aperture: 13 x 12 µm beam ~ 9% flux
11 Microscope Upgrade Better DOF Higher frame rate Ultrafast zoom LED-ring back-light easier to visualize and center larger crystals improved image quality and feedback near-instant change of zoom-levels illumination of crystal surface
12 DA+ - Data Acquisition Plus Team: Main GUI/Framework: MAD GUI CATS GUI Simon Ebner Zac Panepucci Jose Gabadinho Xioxiang Wang
13 DA+ - Data Acquisition Plus Why? Before every function required own GUI Clutered screens Not intuitive Hard to maintain Features All-in-one solution Daq Screening shortcuts Collecting Special modes Interleaved Discrete helical Bookmarks Still images Sample alignment Easy 3-click Toggle modes Sample Changer Spreadsheet Mode switching from GUI MAD MAD easy-mode Rastering
14 DA+ - Data Acquisition Plus Ultra Fast Zoom:
15 DA+ Screening & Data Acquistition (DAQ)
16 Beam-Center Alignment
17 Beamstop Centering by Eye
18 CATS Sample Changer
19 Diffraction Based Alignment PSI, Seite 20
20 Discrete Helical Scan
21 MAD Experiments / Energy Changes
22 Interleaved Experiments
23 X10SA CryoShutter Based on BESSY 3D model (Dr. Uwe Müller) Pneumatic actuator (FESTO) Material cryo-stable 3D printed Harp, J. M., B. L. Hanson, et al. (1999). Acta D55:
24 Acknowledgements MX-Group Vincent Thominet Martin Fuchs Claude Pradervand Jörg Schneider Roman Schneider Ezequiel Panepucci Takashi Tomizaki Clemens Schulze-Briese Meitian Wang & the whole team Construction & Manufacturing Uli Frommherz Jörg Welte Controls & IT Marcel Grunder Jose Gabadinho Xiaoqiang Wang Rene Kapeller Collin Higgs and all our partners and users PSI, 1. April 2014 Seite 25
25 Thank you. PSI, 1. April 2014 Seite 26
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