Cat. # Lot #'s A & A058670
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1 Analytical Reference Materials Retention Time Marker Standard Cat. # Lot #'s A5895 & A Benner Circle Bellefonte, PA (81) FOR LABORATORY USE ONLY. READ MSDS PRIOR TO USE. MANUFACTURED UNDER RESTEK'S ISO 91 REGISTERED QUALITY SYSTEM
2 Certificate of Analysis 11 Benner Circle Bellefonte, PA Tel: (8) Fax: (81) FOR LABORATORY USE ONLY-READ MSDS PRIOR TO USE. Catalog No. : Lot No.: A5867 Description : Retention Time Marker Standard Expiration Date : March 15 Storage: Room Temperature Handling: Warm & Sonicate prior to use Elution Order Solvent: Compound CAS # Percent Purity Concentration (weight/volume) 3 Percent Uncertainty 1 n-decane (C1) % 1,. ug/ml +/-.1 % n-pentacosane (C5) % 1,. ug/ml +/-.1 % 3 n-hexatriacontane (C36) % 1,. ug/ml +/-.1 % Hexane % Column: 3m x.5mm x.5um Rtx-5 (cat.#13) Carrier Gas: cm/sec. Temp. Program: C (hold min.) to 33 5 C/min. Inj. Temp: 5 C Det. Temp: 3 C Det. Type: FID Balance
3 Chemical Standard Batch Sheet Lot #: A5867 Catalog #: Target: 1 ug/ml Description: Retention Time Marker Standard Solvent: Hexane Solvent Lot: E9E1 Final Volume: 5. ml Made by: Rebecca Lauver Date: /6/8 8:55:31AM Tested by: Diane Shaffer Pass Date: /7/8 1::7AM By: Sara Eyster Date: 3/1/8 1:19:5PM Packaged by: / Date: /6/8 11:3:AM No. Units: 31 Pkg Size: 1 ml Balance Used: ARMBALPC3 XP5 Serial #: Compound CAS Storage Location Lot # Target Purity Conc(ug/ml) Target Weight Actual Weight Calc Conc(ug/ml) n-decane (C1) RA1C11D 87MD.99 1, ,. n-pentacosane (C5) RA1D13C 38DD.99 1, ,. n-hexatriacontane (C36) RA1G1C 1HH.99 1, ,.
4 Certificate of Analysis 11 Benner Circle Bellefonte, PA Tel: (8) Fax: (81) FOR LABORATORY USE ONLY-READ MSDS PRIOR TO USE. Catalog No. : Lot No.: A5895 Description : Retention Time Marker Standard Expiration Date : April 15 Storage: Room Temperature Handling: Warm & Sonicate prior to use Elution Order Solvent: Compound CAS # Percent Purity Concentration (weight/volume) 3 Percent Uncertainty 1 n-decane (C1) % 1,. ug/ml +/-.1 % n-pentacosane (C5) % 1,. ug/ml +/-.1 % 3 n-hexatriacontane (C36) % 1,. ug/ml +/-.1 % Hexane % Column: 3m x.5mm x.5um Rtx-5 (cat.#13) Carrier Gas: cm/sec. Temp. Program: C (hold min.) to 33 5 C/min. Inj. Temp: 5 C Det. Temp: 3 C Det. Type: FID Balance
5 Chemical Standard Batch Sheet Lot #: A5895 Catalog #: Target: 1 ug/ml Description: Retention Time Marker Standard Solvent: Hexane Solvent Lot: E9E1 Final Volume: 5. ml Made by: Michael Maye Date: 3/5/8 :8:PM Tested by: Diane Shaffer Pass Date: 3/6/8 9:15:AM By: Sara Eyster Date: 3/1/8 1::7PM Packaged by: / Date: 3/6/8 7::59AM No. Units: 31 Pkg Size: 1 ml Balance Used: ARMBALPC1 XP5 Serial #: Compound CAS Storage Location Lot # Target Purity Conc(ug/ml) Target Weight Actual Weight Calc Conc(ug/ml) n-decane (C1) RA1C11D 87MD.99 1, ,. n-pentacosane (C5) RA1D13C 38DD.99 1, ,. n-hexatriacontane (C36) RA1G1C 1HH.99 1, ,.
6 QA Report: Retention Time Marker Standard (Cat.#31637) Peak Area in 1: Runs of Lot # A5895 Runs of Lot # A5867 COMPONENT 1 3 AVG StdDev %RSD 1 3 AVG Std... %RSD %D ME n-decane Phenanthrene (IS) Pentacosane Hexatriacontane Retention Time: n-decane Phenanthrene (IS) Pentacosane Hexatriacontane Relative Response Factors: n-decane Phenanthrene (IS) Pentacosane Hexatriacontane
7 Area % Report Page 1 of 1 Data File: \\Morty\Ezchrom\Projects\standards\Data\n-Decane (C1) Lot#87MD Method: \\Morty\Ezchrom\Projects\standards\Method\31885.met Acquired: 11/8/7 6:19:39 PM Printed: 11/9/7 8:36:3 AM n-decane (C1) Lot#87MD HP Minutes FID Results Retention Time Area Area Percent Totals
8 File :\\Morty\Ezchrom\Projects\standards\Data\87MD.D Operator : ARM QA Acquired : 8 Nov 7 15:3 using AcqMethod SVRAW.M Instrument : Instrument #1 Sample Name: Decane Lot#87MD Misc Info : Vial Number: 3 Abundance 57 Scan 11 (8.81 min): 87MD.D\data.ms m/z--> Abundance #55: Decane m/z-->
9 Area % Report Page 1 of 1 Data File: \\Morty\Ezchrom\Projects\standards\Data\n-Hexatriacontane -Lot#1HH Method: \\Morty\Ezchrom\Projects\standards\Method\3195.met Acquired: 8/8/7 9:16: AM Printed: 8/8/7 1:1:9 AM n-hexatriacontane Lot#1HH HP Minutes. FID Results Retention Time Area Area Percent Totals
10 Area % Report Page 1 of 1 Data File: \\Morty\Ezchrom\Projects\standards\Data\Pentacosane Lot#38DD Method: \\Morty\Ezchrom\Projects\standards\Method\svraw.met Acquired: 1/3/5 6::1 AM Printed: 1/7/5 3:56:1 PM Pentacosane Lot#38DD C (hold min.) to 33 1 C/min. (hold 1 min.) Rtx-5 3m x.5mm x.5um Cat.#138 Injector 5 C Split cc/ min. Detector 3 C Carrier gas cm/sec Minutes FID Results Retention Time Area Area Percent Totals
11 File : G:\MSDATA\38DD.D Operator : SEE Acquired : 7 Dec 5 :7 pm using AcqMethod SVRAW Instrument : GC/MS Ins Sample Name: Pentacosane Misc Info : Lot#38Dd Vial Number: Abundance 9 57 Scan 6893 (.991 min): 38DD.D m/z-->
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