IR Group 1 - carbonyl compounds (R = alkyl branch, Ar = aromatic branch)
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1 I Problem Set Identify a functional group for each I below (write a generic structure from the choices in each group next to each I). Identify distinguishing absorption bands to demonstrate the logic of your choices, but be aware that not every band is diagnostic and sometimes typical bands are missing. I spectra are not 100% reliable. These are real spectra, not simulated. I Group 1 - carbonyl compounds ( = alkyl branch, Ar = aromatic branch) Ar Cl Ar Ar Ar Ar Ar Ar Ar Cl N 2 N N Ar N 2 Ar Ar Ar Ar N I Group 2 - hydrocarbon compounds, alkanes, alkenes, alkynes and aromatics ( = alkyl branch, Ph = phenyl) ' Ph Ph I Group 3 - Miscellaneous functional groups ( = alkyl branch, Ar = aromatic) S N 2 N N S Cl Br ' N N Ph N N ' Cl Y:\files\classes\00 fall 2016 files\is from database problems.doc
2 I Problem Set Group 1 1 structure Important wavenumbers 3430, , 2820, 2720, 1730, 1470, structure Important wavenumbers 3420, 3090, , 2740, 1700, 1660, 1600, 1580, 750, structure Important wavenumbers , 1690, 1600, 1580, 1460, 1290, 940, structure Important wavenumbers , 2970, 2870, 1710, 1470, 1370, 940, 730 Y:\files\classes\00 fall 2016 files\is from database problems.doc
3 I Problem Set Group 1 5 structure Important wavenumbers , 1650, 1460, structure Important wavenumbers 3360, 3190, , 1660, 1630, 1460, 1340, structure Important wavenumbers 3300, 3090, , 1650, 1550, 1470, 1380, structure Important wavenumbers 3330, 3070, 3050, , 1640, 1620, 1580, 1490, 720, 700, Y:\files\classes\00 fall 2016 files\is from database problems.doc
4 I Problem Set Group 1 9 structure Important wavenumbers 3460, , 1740, 1470, 1370, 1250, 1180, 1100, 1040, 10 structure Important wavenumbers 3430, 3090, 3040, , 1720, 1600, 1460, 1340, 1270, 1110, structure Important wavenumbers , , , structure Important wavenumbers 3450, 3060, 3040, 1730, 1600, 1490, 1260, 1200, 1060, 750, 700 Y:\files\classes\00 fall 2016 files\is from database problems.doc
5 I Problem Set Group 1 13 structure Important wavenumbers 3640, 3560, , 1820, 1760, 1460, 1380, structure Important wavenumbers 3090, 3050, 1790, 1730, 1600, 1450, 1210, 1180, 1040, 780, 700, structure Important wavenumbers 3490, 3070, 1780, 1600, 1580, 1450, 1210, 1180, 870, 780, structure Important wavenumbers 3680, , , 1380, Y:\files\classes\00 fall 2016 files\is from database problems.doc
6 I Problem Set Group 1 17 structure Important wavenumbers 3400, 3090, 3030, , 1690, 1600, 1550, 1460, 1350, 1220, 750, structure Important wavenumbers 3420, , 1720, 1470, 1360, 1170, 19 structure Important wavenumbers , 1550, structure Important wavenumbers 3070, 1670, 1590, 1450, 1280, 700, 640 Y:\files\classes\00 fall 2016 files\is from database problems.doc
7 I Problem Set Group 2 1 structure Important wavenumbers , structure Important wavenumbers 3 structure Important wavenumbers , structure Important wavenumbers , , Cis-4-octene Y:\files\classes\00 fall 2016 files\is from database problems.doc
8 I Problem Set Group 2 5 structure Important wavenumbers 3080, , 1480, , structure Important wavenumbers , structure Important wavenumbers 3090, structure Important wavenumbers , Y:\files\classes\00 fall 2016 files\is from database problems.doc
9 I Problem Set Group 2 9 structure Important wavenumbers 3060, , structure Important wavenumbers , , , structure Important wavenumbers , 1380, 1370 (2 peaks) structure Important wavenumbers 3050, , Y:\files\classes\00 fall 2016 files\is from database problems.doc
10 I Problem Set Group 2 13 structure Important wavenumbers , structure Important wavenumbers , structure Important wavenumbers , , 780, structure Important wavenumbers Y:\files\classes\00 fall 2016 files\is from database problems.doc
11 I Problem Set Group 2 17 structure Important wavenumbers , structure Important wavenumbers , ,690 1-phenyl-1-butyne Y:\files\classes\00 fall 2016 files\is from database problems.doc
12 I Problem Set Group 3 1 structure Important wavenumbers , structure Important wavenumbers 3080, m 1600m , m structure Important wavenumbers , 1550, structure (M+2 M+) Important wavenumbers , Y:\files\classes\00 fall 2016 files\is from database problems.doc
13 I Problem Set Group 3 5 structure Important wavenumbers 3640, impurity , structure Important wavenumbers , structure Important wavenumbers 3070, , structure Important wavenumbers , Y:\files\classes\00 fall 2016 files\is from database problems.doc
14 I Problem Set Group 3 9 structure Important wavenumbers , M+2 = 4.5% of M+ structure Important wavenumbers , structure Important wavenumbers 3370, structure Important wavenumbers , Y:\files\classes\00 fall 2016 files\is from database problems.doc
15 I Problem Set Group 3 hilarious 13 M+2 = 4.5% of M+ structure Important wavenumbers , 1440, structure Important wavenumbers 3490 impurity (wet?) ?? , structure Important wavenumbers , M+2 = 32% of M+ structure Important wavenumbers , Y:\files\classes\00 fall 2016 files\is from database problems.doc
16 I Problem Set Group 3 17 structure Important wavenumbers 3640, 3560, , 1820, 1760, 1460, 1380, structure Important wavenumbers 3680, , , 1380, 19 structure Important wavenumbers 3460, , 1740, 1470, 1370, 1250, 1180, 1100, 1040, 20 structure Important wavenumbers , 2970, 2870, 1710, 1470, 1370, 940, 730 Y:\files\classes\00 fall 2016 files\is from database problems.doc
17 I Problem Set Group 3 21 structure Important wavenumbers 3430, , 2820, 2720, 1730, 1470, structure Important wavenumbers 3420, , 1720, 1470, 1360, 1170, 23 structure Important wavenumbers 3360, 3190, , 1660, 1630, 1460, 1340, structure Important wavenumbers , Y:\files\classes\00 fall 2016 files\is from database problems.doc
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