CERTIFICATE OF ANALYSIS
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1 Attention:Marc St Germain Markham (DW) 600 Cochrane Dr Suite 500 Markham, ON Canada L3R 5K3 Your Project #: IMMACULATE CONCEPTION Your C.O.C. #: Report #: R Version: 1 - Final MAXXAM JOB #: B6B7050 Received: 2016/06/08, 14:15 Sample Matrix: Water # Samples Received: 2 Analyses Metals Analysis by ICPMS (as received) (1) CERTIFICATE OF ANALYSIS Date Quantity Extracted 2 Date Analyzed Laboratory Method 2016/06/ /06/13 CAM SOP Reference EPA 6020A m Reference Method suffix m indicates test methods incorporate validated modifications from specific reference methods to improve performance. * RPDs calculated using raw data. The rounding of final results may result in the apparent difference. (1) Metals analysis was performed on the sample 'as received'. Encryption Key Please direct all questions regarding this Certificate of Analysis to your Project Manager. James Aspin, Senior Project Manager JAspin@maxxam.ca Phone# (905) ==================================================================== Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page. Total Cover Pages : 1 Page 1 of 7
2 Maxxam ID Sampling Date COC Number Metals. Lead (Pb) ELEMENTS BY ATOMIC SPECTROSCOPY (WATER) UNITS ug/l MAC 10 CMO /06/08 05: S 23 (1) CMO /06/08 06: F RDL = Reportable Detection Limit QC Batch = Quality Control Batch MAC: Ontario Regulation 243/07 made under the Safe Drinking Water Act, (Released June 7, 2007) (1) POTENTIAL EXCEEDENCE FOR PARAMETER 6.2 RDL 0.50 QC Batch Page 2 of 7
3 TEST SUMMARY Maxxam ID: CMO778 Collected: 2016/06/08 Sample ID: S Shipped: Matrix: Water Received: 2016/06/08 Test Description Metals Analysis by ICPMS (as received) Instrumentation ICP/MS Batch Extracted 2016/06/09 Date Analyzed 2016/06/13 Analyst Prempal Bhatti Maxxam ID: CMO779 Collected: 2016/06/08 Sample ID: F Shipped: Matrix: Water Received: 2016/06/08 Test Description Metals Analysis by ICPMS (as received) Instrumentation ICP/MS Batch Extracted 2016/06/09 Date Analyzed 2016/06/13 Analyst Prempal Bhatti Page 3 of 7
4 GENERAL COMMENTS Each temperature is the average of up to three cooler temperatures taken at receipt Package C Results relate only to the items tested. Page 4 of 7
5 QUALITY ASSURANCE REPORT Site Location: Matrix Spike SPIKED BLANK Method Blank RPD QC Batch Parameter Date % Recovery QC Limits % Recovery QC Limits Value UNITS Value (%) Lead (Pb) 2016/06/ ND, RDL=0.50 ug/l NC Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement. Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference. Spiked Blank: A blank matrix sample to which a known amount of the analyte, usually from a second source, has been added. Used to evaluate method accuracy. Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination. NC (Duplicate RPD): The duplicate RPD was not calculated. The concentration in the sample and/or duplicate was too low to permit a reliable RPD calculation (one or both samples < 5x RDL). QC Limits 20 Page 5 of 7
6 VALIDATION SIGNATURE PAGE The analytical data and all QC contained in this report were reviewed and validated by the following individual(s). Cristina Carriere, Scientific Services Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page. Page 6 of 7
7 Page 7 of 7
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