Feed Check Sample No Preconditioning/Receiving Chow, Med Association of American Feed Control Officials

Transcription

1 Feed Check Sample No Preconditioning/Receiving Chow, Med Association of American Feed Control Officials - Pass 1 Results for 212 Labs - - Pass 2 Results for 211 Labs - No. Average No. Average AOAC Method of Grand Std. Range of Grand Std. Range Method 18th Code Labs Avg. Dev. of Dups Labs Avg. Dev. of Dups NPN, Urea + Am, Urease Method NPN, Automated Urea, Misc Method Group 000.XX PCT Loss on Drying, Vac 95 deg 5 hr Loss on Drying, ISO Loss on Drying, LECO Loss on Drying, 104 deg 3 hr, in malt Loss on Drying, 102 deg 16 hr, in meat Loss on Drying, Misc Method Group 001.XX PCT Protein, Crude Protein, Auto Kjel-Foss Protein, Semiauto Autoanalyzer Protein, Hach Method Protein, Copper Cat Protein, Copper, Boric Acid Protein, Combustion Nitrogen Analyzer Protein, Cu/Ti Protein, Block dig/distillation Protein, NIR Protein, Misc Method Group 002.XX PCT Fat, Eth Ext, Direct Fat, Ind Eth Ext (13th ed), Indirect Fat, Pet Ether Fat, Soxtec, Eth Ext Fat, Soxtec, Pet Ether Fat, NIR Fat, Hexane Ext Fat, Soxtec, Hexane Ext Fat, Ankom Fat, Misc Method Group 003.XX PCT Fiber, Crude Asbestos Free Fiber, Sing Filt Fiber, Fritted Glass Fiber, Fibertec Fiber, ANKOM Sample October 24, 2009 Page 1

2 Feed Check Sample No Preconditioning/Receiving Chow, Med Association of American Feed Control Officials - Pass 1 Results for 212 Labs - - Pass 2 Results for 211 Labs - No. Average No. Average AOAC Method of Grand Std. Range of Grand Std. Range Method 18th Code Labs Avg. Dev. of Dups Labs Avg. Dev. of Dups Fiber, NIR Fiber, Misc Method Group 004.XX PCT Ash, Ash, Sugars & Syrups Ash, LECO Ash, NIR Ash, Misc Method Group 005.XX PCT Fiber, Acid Detergent Fiber, Acid Detergent-Hach Fiber, Acid Detergent by ANKOM Fiber, Acid Detergent Misc Method Group 008.XX PCT Fiber, Neutral Det-No ENZ Pretreat Fiber, Neutral Det-ENZ Pretreat Fiber, Neutral Detergent by ANKOM Fiber, Neutral Det Misc Method Group 009.XX PCT Moisture, Karl-Fischer Moisture, NIR Moisture, Misc Method Group 010.XX PCT Loss on Drying, 135 deg 2 hr Loss on Drying, High Temp Methods, Misc Method Group 011.XX PCT Starch, Polarimetric (Ewers) Starch, Megazyme Starch, Enzymatic Starch, YSI Analyzer Starch, NIR Method Group 012.XX PCT Fat, Mojonnier, Bak Ext Fat, Roese-Gottlieb Modified Fat, Soxtec-Acid Hydrolysis Fat, Super Critical Fluid Extraction Fat, NIR-Acid Hydrolysis Fat, Ankon-Acid Hydrolysis Fat, Pretreat or extended ext, misc Sample October 24, 2009 Page 2

3 Feed Check Sample No Preconditioning/Receiving Chow, Med Association of American Feed Control Officials - Pass 1 Results for 212 Labs - - Pass 2 Results for 211 Labs - No. Average No. Average AOAC Method of Grand Std. Range of Grand Std. Range Method 18th Code Labs Avg. Dev. of Dups Labs Avg. Dev. of Dups Method Group 013.XX PCT Aluminum, ICP Method Group 015.XX PPM Arsenic, AA, Hydride Boron, ICP Boron, Misc Method Group 017.XX PPM Cadmium, ICP Method Group 018.XX PPM Calcium, Ox-Mn04 Vol Calcium, At Abs Spect Calcium, Semiauto (Autoanalyzer) Calcium, ICP, Dry Ash Calcium, EDTA Calcium, ICP, Wet Ash Calcium, Misc Method Group 019.XX PCT Chromium, AA Chromium, ICP Chromium, Misc Method Group 020.XX PPM Cobalt, AA Cobalt, ICP Cobalt, Misc Method Group 021.XX PPM Copper, AA Copper, ICP, Dry Ash Copper, ICP, Wet Ash Copper, Misc Method Group 022.XX PPM Fluorine, Ion Sel Elect Iron, AA Iron, ICP, Dry Ash Iron, ICP, Wet Ash Iron, Misc Method Group 025.XX PPM Lead, Lead, Misc Method Group 026.XX PPM Sample October 24, 2009 Page 3

4 Feed Check Sample No Preconditioning/Receiving Chow, Med Association of American Feed Control Officials - Pass 1 Results for 212 Labs - - Pass 2 Results for 211 Labs - No. Average No. Average AOAC Method of Grand Std. Range of Grand Std. Range Method 18th Code Labs Avg. Dev. of Dups Labs Avg. Dev. of Dups Magnesium, AA Magnesium, ICP, Dry Ash Magnesium, ICP, Wet Ash Magnesium, Misc Method Group 027.XX PCT Manganese, AA Manganese, Em Spect Manganese, ICP, Dry Ash Manganese, ICP, Wet Ash Manganese, Misc Method Group 028.XX PPM Mercury, Mercury, Misc Method Group 029.XX PPM Phosphorus, Photometric Phosphorus, GQMP (2.028) Phosphorus, Autoanalyzer Phosphorus, ICP Phosphorus, Hach Method Phosphorus, Misc Method Group 031.XX PCT Potassium, AA Potassium, Flame Emission Potassium, Em Spect Potassium, ICP Potassium, Misc Method Group 032.XX PCT Salt, Sol Cl Salt, Poten Cl Salt, Quantab Salt, Ion Sel Electrode Salt, Misc Method Group 033.XX PCT Selenium, Fluor Selenium, AA, Hydride Selenium, ICP Selenium, Misc Method Group 034.XX PPM Sodium, AA Sample October 24, 2009 Page 4

5 Feed Check Sample No Preconditioning/Receiving Chow, Med Association of American Feed Control Officials - Pass 1 Results for 212 Labs - - Pass 2 Results for 211 Labs - No. Average No. Average AOAC Method of Grand Std. Range of Grand Std. Range Method 18th Code Labs Avg. Dev. of Dups Labs Avg. Dev. of Dups Sodium, Ion Sel Electrode Sodium, Em Spect Sodium, ICP Sodium, Flame Emission Sodium, Misc Method Group 035.XX PCT Sulfur, (Gravimetric) Sulfur, ICP Sulfur, LECO Method Group 036.XX PCT Zinc, AA Zinc, ICP, Dry Ash Zinc, ICP, Wet Ash Zinc, Misc Method Group 037.XX PPM Molybdenum, ICP Molybdenum, Misc Method Group 038.XX PPM Nickel, AA Nickel, ICP Method Group 039.XX PPM Barium, ICP Vanadium, ICP Chlorotetracycline, Plate Chlorotetracycline, HPLC Chlorotetracycline, Misc Method Group 051.XX G/TON Sulfamethazine, Sulfamethazine, HPLC Sulfamethazine, HPLC-PCD Method Group 082.XX PCT Thiamine, HPLC Vitamin A, UV Vitamin A, HPLC Vitamin A, Misc Method Group 106.XX KU/LB Vitamin D3, HPLC Method Group 108.XX KU/LB Vitamin E, HPLC Sample October 24, 2009 Page 5

6 Feed Check Sample No Preconditioning/Receiving Chow, Med Association of American Feed Control Officials - Pass 1 Results for 212 Labs - - Pass 2 Results for 211 Labs - No. Average No. Average AOAC Method of Grand Std. Range of Grand Std. Range Method 18th Code Labs Avg. Dev. of Dups Labs Avg. Dev. of Dups Method Group 109.XX MG/KG Alanine, Post-col Ninhydrin Der Alanine, Pre-col AQC Der Method Group 120.XX PCT Arginine, Post-col Ninhydrin Der Arginine, Pre-col AQC Der Method Group 121.XX PCT Aspartic, Post-col Ninhydrin Der Aspartic, Pre-col AQC Der Method Group 122.XX PCT Cysteine/Cystine, PAO Post-col Ninhydri Cysteine/Cystine, PAO Post-col OPA Der Cysteine/Cystine, PAO Pre-col AQC Der Method Group 124.XX PCT Glutamic, Post-col Ninhydrin Der Glutamic, Pre-col AQC Der Method Group 125.XX PCT Glycine, Post-col Ninhydrin Der Glycine, Pre-col AQC Der Method Group 126.XX PCT Histidine, Post-col Ninhydrin Der Histidine, Pre-col AQC Der Method Group 127.XX PCT Isoleucine, Post-col Ninhydrin Der Isoleucine, Pre-col AQC Der Method Group 128.XX PCT Leucine, Post-col Ninhydrin Der Leucine, Pre-col AQC Der Method Group 129.XX PCT L-Lysine, Post-col Ninhydrin Der L-Lysine, Pre-col AQC Der Method Group 130.XX PCT Methionine, PAO Post-col Ninhydrin Der Methionine, PAO Post-col OPA Der Methionine, PAO Pre-col AQC Der Method Group 131.XX PCT Phenylalanine, Post-col Ninhydrin Der Phenylalanine, Pre-col AQC Der Method Group 132.XX PCT Sample October 24, 2009 Page 6

7 Feed Check Sample No Preconditioning/Receiving Chow, Med Association of American Feed Control Officials - Pass 1 Results for 212 Labs - - Pass 2 Results for 211 Labs - No. Average No. Average AOAC Method of Grand Std. Range of Grand Std. Range Method 18th Code Labs Avg. Dev. of Dups Labs Avg. Dev. of Dups Proline, Post-col Ninhydrin Der Proline, Pre-col AQC Der Method Group 133.XX PCT Serine, Post-col Ninhydrin Der Serine, Pre-col AQC Der Method Group 134.XX PCT Threonine, Post-col Ninhydrin Der Threonine, Pre-col AQC Der Method Group 135.XX PCT Tryptophan, Alka-Hydrol Post-col Ninhyd Tryptophan, Alka-Hydrol Rev Phase LC UV Tryptophan, Alka Hydrol+IS Rev Phase LC Method Group 136.XX PCT Tyrosine, Post-col Ninhydrin Der Tyrosine, Pre-col AQC Der Method Group 137.XX PCT Valine, Post-col Ninhydrin Der Valine, Pre-col AQC Der Method Group 138.XX PCT Taurine, Post-col Ninhydrin Der Sample October 24, 2009 Page 7

8 -- Method Method Method Method R Avg Method Avg R Method Method s s R Avg A s s s Method Method Avg R s Method Avg Method Method Avg Method s R Avg Method Method Avg Method R Method Avg Method s R R Sample October 24, 2009 Page 8

9 -- Method Method Avg Method R R A Method R Avg Method Method Avg R Method Avg R S Method Avg Method s Method Avg R R Method Method Sample October 24, 2009 Page 9

10 -- Method Avg R s Method Avg Method Method s s A R Avg s Method Avg Method Avg Method Avg Method R Method Avg Method Avg A Method R R Method Avg Method Method Avg Method S R Sample October 24, 2009 Page 10

11 -- Method Avg Method Method Avg R s Method R Avg S Method Avg Method s R R Method R R R Method Avg Sample October 24, 2009 Page 11

12 -- Method R Method R s Method Method Method S S S S S Avg Method Avg Method Method R Avg s Method Method s s Method Avg X R R s Method s Avg Method Method Avg Method Method s Avg R Method Avg R Method Avg S S Sample October 24, 2009 Page 12

13 -- Method s Avg Method s Avg S Method s R Method R R Avg Method R R s s Method Method Avg Method Avg Method Avg Method R Avg Method Avg Method S Method s Avg Method Method s Sample October 24, 2009 Page 13

14 -- Method Avg Method Method Avg Method Avg Method Avg Method s Avg Method Method Method s Avg s Method Method Avg Method R Avg Method S Method s R Avg Method Method S Method Avg Method s s Method Avg R Method R Avg Sample October 24, 2009 Page 14

15 -- Method Method S S Avg R s Method S Avg Method Avg Method Avg Method Avg Method Avg Method s Avg s Method Method Avg Method R R R Method R Avg Method Method R Avg Sample October 24, 2009 Page 15

16 -- Method R Method Avg Method Method R Avg Method s s s R R Avg s Method s s Avg R Method S Avg Method Method Method s R Avg Method s s s Method Avg Sample October 24, 2009 Page 16